200 And More Nmr Experiments
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200 And More Nmr Experiments
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Author : Stefan Berger
language : en
Publisher: John Wiley & Sons
Release Date : 2004-07-02
200 And More Nmr Experiments written by Stefan Berger and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2004-07-02 with Science categories.
This work-book will guide you safely, in step-by-step descriptions, through every detail of the NMR experiments within, beginning with 1D routine experiments and ending with a series of advanced 3D experiments on a protein: ? Which experiment can best yield the desired information? ? How must the chosen experiment be performed? ? How does one read the required information from the spectrum? ? How does this particular pulse sequence work? ? Which other experiments give similar information? This third edition of the book, following its two highly successful predecessors, has been revised and expanded to 206 experiments. They are organized in 15 chapters, covering test procedures and routine spectra, variable temperature measurements, the use of auxiliary reagents, 1D multipulse experiments, spectra of heteronuclides, and the application of selective pulses. The second and third dimensions are introduced using pulsed field gradients, and experiments on solid state materials are described. A key part describes 3D experiments on the protein ubiquitin with 76 amino acids. What is new in this third edition? 1. 24 new experiments have been inserted into the 14 chapters that were in the 2nd edition, e.g., alpha/beta-SELINCOR-TOCSY, WET, DOSY, ct-COSY, HMSC, HSQC with adiabatic pulses, HETLOC. J-resolved HMBC, (1,1)- and (1,n)-ADEQUATE, STD, REDOR, and HR-MAS. 2. 20 new protein NMR experiments have been specially devised and are collected in the newly added Chapter 15, ProteinNMR, for which one needs a special model sample: fully 13C- and 15N-labeled human ubiquitin. Techniques used include the constant time principle, the PEP method, filters, gradient selection, and the echo/anti-echo procedure. The guide has been written by experts in this field, following the principle of learning by doing: all the experiments have been specially performed for this book, exactly as described and shown in the spectra that are reproduced. Being a reference source and work-book for the NMR laboratory as well as a textbook, it is a must for every scientist working with NMR, as well as for students preparing for their laboratory courses
200 And More Nmr Experiments
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Author : Stefan Berger
language : en
Publisher:
Release Date : 2004
200 And More Nmr Experiments written by Stefan Berger and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2004 with categories.
50 And More Essential Nmr Experiments
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Author : Matthias Findeisen
language : en
Publisher: John Wiley & Sons
Release Date : 2013-07-30
50 And More Essential Nmr Experiments written by Matthias Findeisen and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-07-30 with Science categories.
This book is the perfect link for learning how to perform the experiments after only having studied theory. In eight chapters more than 50 essential NMR experiments are described in detail. Special focus is put on the organic set of NMR spectra (1H, 13C-APT, COSY, NOESY, HSQC and HMBC). Different chapters deal with advanced organic NMR, selective methods, heteronuclear NMR, relaxation and diffusion measurements, organic applications and maintenance. Every experiment has a section providing the reader with the purpose and scope of the specific experiment. Every experiment is concluded with the spectrum as it is obtained under the conditions described. Questions and comments enable the reader to check their understanding. The authors are very experienced and the whole book is in full color, which enhances the reading experience and makes the spectra and other figures easier to understand. This book is strongly recommended for all students and researchers who are involved in the structural elucidation of chemical compounds both in practical education and in pursuing research, in particular if they handle an NMR spectrometer.
100 And More Basic Nmr Experiments
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Author : Siegmar Braun
language : en
Publisher: Wiley-VCH
Release Date : 1996-01-25
100 And More Basic Nmr Experiments written by Siegmar Braun and has been published by Wiley-VCH this book supported file pdf, txt, epub, kindle and other format this book has been release on 1996-01-25 with Medical categories.
How do the pulse sequences of modern NMR work? Which experiment conveys the desired information? How can the maximal amount of information be retrieved from measured spectra? Have you ever been confronted with questions like these? Get the answers and explore the full productivity of your NMR equipment! This book is a reliable guide through the maze of modern NMR tools. Written by leading experts, it describes more than a hundred NMR experiments including selective pulses, field gradients and the second and third dimension. Being textbook as well as reference book for the laboratory, this book is a must for every scientist working with NMR as well as for students preparing for their lab courses.
150 And More Basic Nmr Experiments
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Author : Siegmar Braun
language : en
Publisher: Wiley-VCH
Release Date : 1998-09-10
150 And More Basic Nmr Experiments written by Siegmar Braun and has been published by Wiley-VCH this book supported file pdf, txt, epub, kindle and other format this book has been release on 1998-09-10 with Mathematics categories.
NMR is one of the most widely used analytical techniques in chemistry. This book gives a problem-oriented introduction to modern applications in a "how-to" format.
150 And More Basic Nmr Experiments
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Author : Siegmar Braun
language : en
Publisher: Wiley-VCH
Release Date : 1998-09-10
150 And More Basic Nmr Experiments written by Siegmar Braun and has been published by Wiley-VCH this book supported file pdf, txt, epub, kindle and other format this book has been release on 1998-09-10 with Science categories.
50 And More Essential Nmr Experiments
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Author : Matthias Findeisen
language : en
Publisher: John Wiley & Sons
Release Date : 2013-11-04
50 And More Essential Nmr Experiments written by Matthias Findeisen and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-11-04 with Science categories.
This book is the perfect link for learning how to perform the experiments after only having studied theory. In eight chapters more than 50 essential NMR experiments are described in detail. Special focus is put on the organic set of NMR spectra (1H, 13C-APT, COSY, NOESY, HSQC and HMBC). Different chapters deal with advanced organic NMR, selective methods, heteronuclear NMR, relaxation and diffusion measurements, organic applications and maintenance. Every experiment has a section providing the reader with the purpose and scope of the specific experiment. Every experiment is concluded with the spectrum as it is obtained under the conditions described. Questions and comments enable the reader to check their understanding. The authors are very experienced and the whole book is in full color, which enhances the reading experience and makes the spectra and other figures easier to understand. This book is strongly recommended for all students and researchers who are involved in the structural elucidation of chemical compounds both in practical education and in pursuing research, in particular if they handle an NMR spectrometer.
Hands On Nmr
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Author : William S. Price
language : en
Publisher:
Release Date : 2021-05-17
Hands On Nmr written by William S. Price and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2021-05-17 with Science categories.
Presenting important practical aspects of NMR spectroscopy, this book will be useful for explaining and facilitating the successful set up of a wide variety of NMR experiments. It will enlighten readers with the relevant information on the basic concepts in NMR, how it works, and how to trouble-shoot artefacts that may be encountered. A short introductory chapter on some basic theory and key concepts will precede chapters on more practical aspects e.g. instrumentation, sample preparation, experimentation and data processing. Several practical case experiments covering various fields and including details on the pitfalls, tips and recommendations are presented next. Lastly, detailed chapters on other important practical aspects such as artefacts, spectral prediction, databases and safety are included. Bringing books that present practical NMR up to date, this book fills a gap in the literature and provides a new comprehensive practical NMR book for teaching and research at all levels - graduates, postgraduates, industry and research.
Basic One And Two Dimensional Nmr Spectroscopy
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Author : Horst Friebolin
language : en
Publisher: John Wiley & Sons
Release Date : 2010-12-28
Basic One And Two Dimensional Nmr Spectroscopy written by Horst Friebolin and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2010-12-28 with Science categories.
This is the fifth edition of the highly successful, classic textbook for bachelor and master courses, with over 20 % new material and the contents completely revised and updated. Using a minimum of mathematics, it explains the underlying theory of this most important spectroscopic technique in a thorough, yet readily understandable way, covering instrumentation and interpretation of the spectra. It presents all students need to know about 1D, 2D-NMR, solid state and dynamic NMR spectroscopy, as well as NMR imaging, all illustrated by examples for maximum clarity. All the sections include sub-chapters that focus on applications taken from organic, macromolecular, polymer and biochemistry. A must for students and lecturers in chemistry, biochemistry, pharmacy, and life sciences, as well as for spectroscopists.
Understanding Nmr Spectroscopy
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Author : James Keeler
language : en
Publisher: John Wiley & Sons
Release Date : 2011-09-19
Understanding Nmr Spectroscopy written by James Keeler and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2011-09-19 with Science categories.
This text is aimed at people who have some familiarity with high-resolution NMR and who wish to deepen their understanding of how NMR experiments actually ‘work’. This revised and updated edition takes the same approach as the highly-acclaimed first edition. The text concentrates on the description of commonly-used experiments and explains in detail the theory behind how such experiments work. The quantum mechanical tools needed to analyse pulse sequences are introduced set by step, but the approach is relatively informal with the emphasis on obtaining a good understanding of how the experiments actually work. The use of two-colour printing and a new larger format improves the readability of the text. In addition, a number of new topics have been introduced: How product operators can be extended to describe experiments in AX2 and AX3 spin systems, thus making it possible to discuss the important APT, INEPT and DEPT experiments often used in carbon-13 NMR. Spin system analysis i.e. how shifts and couplings can be extracted from strongly-coupled (second-order) spectra. How the presence of chemically equivalent spins leads to spectral features which are somewhat unusual and possibly misleading, even at high magnetic fields. A discussion of chemical exchange effects has been introduced in order to help with the explanation of transverse relaxation. The double-quantum spectroscopy of a three-spin system is now considered in more detail. Reviews of the First Edition “For anyone wishing to know what really goes on in their NMR experiments, I would highly recommend this book” – Chemistry World “...I warmly recommend for budding NMR spectroscopists, or others who wish to deepen their understanding of elementary NMR theory or theoretical tools” – Magnetic Resonance in Chemistry