Quantitative Gas Chromatography For Laboratory Analyses And On Line Process Control
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Quantitative Gas Chromatography For Laboratory Analyses And On Line Process Control
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Author : G. Guiochon
language : en
Publisher: Elsevier
Release Date : 1988-06-01
Quantitative Gas Chromatography For Laboratory Analyses And On Line Process Control written by G. Guiochon and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 1988-06-01 with Science categories.
Here is an invaluable new book on quantitative gas chromatography which explains how the method can - or should - be used for accurate and precise analysis. Gas chromatography is firmly established as one of the few major methods for the quantitative analysis of complex mixtures. It is fast, accurate and inexpensive, with a broad range of applications. It has however become very complex and involved: over 200 stationary phases, more than 10 detector principles and several very different column types are available from among the catalogs of over 100 manufacturers and major retailers. The progressive changes in the nature of gas chromatography have created new needs for information which are not satisfied by the literature presently available. This book provides a complete discussion of all the problems involved in the achievement of quantitative analysis by gas chromatography, whether in the research laboratory, in the routine analysis laboratory or in process control. For this reason the presentation of theoretical concepts has been limited to the essential, while extensive explanations have been devoted to the various steps involved in the derivation of precise and accurate data. This starts with the selection of the instrumentation and column, continues with the choice of optimum experimental conditions, then calibration and ends with the use of correct procedures for data acquisition and calculations. Finally, there is almost always a way to reduce errors and an entire chapter deals with this single issue. Numerous relevant examples are presented. The first part of the book presents the theoretical background, simple enough to be understood by all analytical chemists, but still complete and up-to-date. It discusses the problems of flow dynamics, retention and band broadening. The changes in band profile associated with column overloading are explained without much recourse to mathematics. The second part describes the gas chromatograph and discusses the properties of each of its parts: gas flow and pressure controller sampling system, oven, column switching valves, detectors. The different implementations, their advantages and drawbacks are discussed and compared. In addition, three chapters present packed column technology, open tubular column technology and some sophisticated new phase systems, respectively. The new phase systems described use adsorbents, modified by coating or grafting organic phase, and carrier gases containing vapors which are sorbed by the stationary phase and modify it, such as steam. The third part discusses the applications in qualitative and quantitative analysis. Calibration, peak integration, sources of errors arising from the various parts of the instrument as well as from the measurement process itself are carefully described in four detailed chapters. Methods to carry out accurate and precise analysis are presented. A last chapter is devoted to process control analysis and gives a number of detailed examples of applications. A lexicon explaining the most important chromatographic terms and a detailed index complete the book. This is a book which no chemical analyst should be without. It should be on the library shelf of all universities, instrument companies and any laboratory and plant where gas chromatography is used.
Quantitative Gas Chromatography For Laboratory Analyses And On Line Process Control
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Author :
language : en
Publisher:
Release Date : 1988
Quantitative Gas Chromatography For Laboratory Analyses And On Line Process Control written by and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1988 with categories.
Process Gas Chromatography
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Author : Raymond Annino
language : en
Publisher:
Release Date : 1992
Process Gas Chromatography written by Raymond Annino and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1992 with Science categories.
A textbook on the principles and practices pertinent to the design, operation, and application of on-line gas chromatographs in an industrial environment, for instrument specification engineers, instrument maintenance personnel, internal support personnel, (such as laboratory chemists), technical sa
Instrument Engineers Handbook Volume One
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Author : Bela G. Liptak
language : en
Publisher: CRC Press
Release Date : 2003-06-27
Instrument Engineers Handbook Volume One written by Bela G. Liptak and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2003-06-27 with Technology & Engineering categories.
Unsurpassed in its coverage, usability, and authority since its first publication in 1969, the three-volume Instrument Engineers' Handbook continues to be the premier reference for instrument engineers around the world. It helps users select and implement hundreds of measurement and control instruments and analytical devices and design the most cost-effective process control systems that optimize production and maximize safety. Now entering its fourth edition, Volume 1: Process Measurement and Analysis is fully updated with increased emphasis on installation and maintenance consideration. Its coverage is now fully globalized with product descriptions from manufacturers around the world. Béla G. Lipták speaks on Post-Oil Energy Technology on the AT&T Tech Channel.
Trac Trends In Analytical Chemistry
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Author : U A Th Brinkman
language : en
Publisher: Elsevier
Release Date : 2013-09-24
Trac Trends In Analytical Chemistry written by U A Th Brinkman and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-09-24 with Science categories.
TRAC: Trends in Analytical Chemistry, Volume 8 provides information pertinent to the trends in the field of analytical chemistry. This book presents a variety of topics related to analytical chemistry, including protein purification, biotechnology, Raman spectroscopy in pharmaceutical field, electrokinetic chromatography, and flow injection analysis. Organized into 50 chapters, this volume begins with an overview of scientometric investigations that enable the quantitative study of the evolution of its various components and can thereby uncover how information is utilized to diffuse and generate knowledge. This text then discusses the economic significance of sensing and control as being the main factors in determining process economics and in offering products and business opportunities. Other chapters consider the important relationship between Raman spectroscopy and other analytical methods. This book discusses as well the interfaces between a gas chromatograph and a Fourier transform infrared spectrometer. The final chapter deals with chemometrics routines. This book is a valuable resource for analytical chemists, and biochemists.
Process Gas Chromatographs
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Author : Tony Waters
language : en
Publisher: John Wiley & Sons
Release Date : 2020-07-13
Process Gas Chromatographs written by Tony Waters and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2020-07-13 with Technology & Engineering categories.
A guide to the fundamentals of applied gas chromatography and the process gas chromatograph, with practical procedures for design and troubleshooting This comprehensive resource provides the theory that underpins a full understanding of the fundamental techniques of gas chromatography and the process analyzer. Without relying on complex mathematics, the book addresses hands-on applications of gas chromatographs within process industries. The author – a noted expert on the topic – details both the scientific information needed to grasp the material presented and the practical applications for professionals working in the field. Process Gas Chromatographs: Fundamentals, Design and Implementation comprises 15 chapters, a glossary of terms and a series of self-assessment questions and quizzes. This important resource: Describes practical procedures for design and troubleshooting Contains concise chapters that provide a structured course for advanced students in process engineering Reviews the fundamentals of applied gas chromatography Details the operation and maintenance of process gas chromatographs Offers a summary, and self-assessment questions, for every chapter Is written by an international expert in the field with extensive industry knowledge and teaching experience in courses on process sampling systems and gas chromatography Written for process analyzer engineers and technicians, application engineers, and industrial environmental engineers, Process Gas Chromatographs: Fundamentals, Design and Implementation offers an essential guide to the basics of gas chromatography and reviews the applications of process gas chromatographs in industry today.
Practical Gas Chromatography
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Author : Katja Dettmer-Wilde
language : en
Publisher: Springer
Release Date : 2014-11-05
Practical Gas Chromatography written by Katja Dettmer-Wilde and has been published by Springer this book supported file pdf, txt, epub, kindle and other format this book has been release on 2014-11-05 with Science categories.
Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered.
Performance Tests For The Evaluation Of Computerized Gas Chromatography Mass Spectrometry Equipment And Laboratories
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Author : William L. Budde
language : en
Publisher:
Release Date : 1980
Performance Tests For The Evaluation Of Computerized Gas Chromatography Mass Spectrometry Equipment And Laboratories written by William L. Budde and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1980 with Gas chromatography categories.
Split And Splitless Injection For Quantitative Gas Chromatography
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Author : Konrad Grob
language : en
Publisher: John Wiley & Sons
Release Date : 2008-11-21
Split And Splitless Injection For Quantitative Gas Chromatography written by Konrad Grob and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2008-11-21 with Science categories.
This comprehensive and unique handbook of split and splitless injection techniques has been completely revised and updated. This new edition offers: - New insights concerning sample evaporation in the injector - Information about matrix effects - A new chapter on injector design The real processes within the injector are for the first time visualized and explained by the CD-ROM included in the book. Furthermore the reader will understand the concepts of injection techniques and get a knowledge of the sources of error. The handbook also includes many practical guidelines. From reviews of former editions: "This substantial book is on injection techniques alone, which ... demonstrates this can have many pitfalls ... no one should be allowed to direct a laboratory doing quantitative analysis by GC without first being thoroughly familar with this book ..." The Analyst "This is a detailed reference volume filled with practical suggestions and techniques for managing split and splitless injection in the day-to-day world of the working gas chromatographer. It will be useful ... for anyone who must work hands-on with GC." Journal of High Resolution Chromatography
Chromatographic Analysis Of The Environment Third Edition
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Author : Leo M.L. Nollet
language : en
Publisher: CRC Press
Release Date : 2005-11-29
Chromatographic Analysis Of The Environment Third Edition written by Leo M.L. Nollet and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2005-11-29 with Science categories.
Chromatographic Analysis of the Environment, Third Edition is a detailed handbook on different chromatographic analysis techniques and chromatographic data for compounds found in air, water, soil, and sludge. Taking on a new perspective from previous editions, this third edition discusses the parameters of each environmental compartment in a consistent format that highlights preparation techniques, chromatographic separation methods, and detection methods. Most of the data are compiled in tables and figures to elucidate the text as needed. Separate chapters approach specific aspects of sampling methods especially designed for environmental purposes, quantification of environmental analytes in difficult matrices, and data handling. The second part of the book focuses on the analysis of hazardous chemicals in the environment, including volatile organic carbons (VOCs), polycyclic aromatic hydrocarbons (PAHs), polychlorinated biphenyls (PCBs), and endocrine-disrupting chemicals (EDCs). In addition, the authors feature information on compounds such as phosphates, organic acids, halogenated VOCs, amines, and n-ntirosamines, isocyanates, phthalate esters, and humic substances. Presenting important theoretical and practical aspects from sample collection to laboratory analysis, Chromatographic Analysis of the Environment, Third Edition is a unique resource of chromatographic techniques, data, and references that are useful to all scientists involved in the analysis of environmental compounds.