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Synthesis Of Aliphatic Nitrate Esters By Reaction Of Metal Nitrates With Phosphate Esters

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Synthesis Of Aliphatic Nitrate Esters By Reaction Of Metal Nitrates With Phosphate Esters

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Author : Willis Harford Baldwin
language : en
Publisher:
Release Date : 1979

Synthesis Of Aliphatic Nitrate Esters By Reaction Of Metal Nitrates With Phosphate Esters written by Willis Harford Baldwin and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1979 with Aliphatic compounds categories.

Synthesis Of Aliphatic Nitrate Esters By Reaction Of Metal Nitrates With Phosphate Esters

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Author :
language : en
Publisher:
Release Date : 1979

Synthesis Of Aliphatic Nitrate Esters By Reaction Of Metal Nitrates With Phosphate Esters written by and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1979 with categories.

A safe and simple method of synthesizing short-chain alkyl nitrates is described. This method, which should be of general utility, was found to be useful in preparing compounds for studies to determine the fate of organic materials in nuclear fuel reprocessing operations. Nitrate esters of short-chain alkyl alcohols can be conveniently obtained by distilling mixtures of the appropriate trialkyl phosphate with metallic nitrate salts. Runaway reactions are avoided by using only those metal nitrates that initially undergo an endothermic reaction with trialkyl phosphate. The nitrates of lithium, iron(III), and uranium among others, meet this criterion; lithium nitrate was found to be the most convenient. The purity of the product is more dependent on the temperature used and the purity of the nitrate salt than on the specific metal present in the salt. Details of the synthesis of n-butyl nitrate are given as an example of the method.

Energy Research Abstracts

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Author :
language : en
Publisher:
Release Date : 1979

Energy Research Abstracts written by and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1979 with Power resources categories.

Monthly Catalog Of United States Government Publications

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Author :
language : en
Publisher:
Release Date :

Monthly Catalog Of United States Government Publications written by and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on with Government publications categories.

Monthly Catalogue United States Public Documents

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Author :
language : en
Publisher:
Release Date : 1980

Monthly Catalogue United States Public Documents written by and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1980 with Government publications categories.

Monthly Catalog Of United States Government Publications

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Author : United States. Superintendent of Documents
language : en
Publisher:
Release Date : 1968

Monthly Catalog Of United States Government Publications written by United States. Superintendent of Documents and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1968 with Government publications categories.