Analytical Pyrolysis Handbook
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Analytical Pyrolysis Handbook
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Author : Karen D. Sam
language : en
Publisher: CRC Press
Release Date : 2021-03-23
Analytical Pyrolysis Handbook written by Karen D. Sam and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2021-03-23 with Science categories.
Analytical pyrolysis allows scientists to use routine laboratory instrumentation for analyzing complex, opaque, or insoluble samples more effectively than other analytical techniques alone. Analytical Pyrolysis Handbook, Third Edition is a practical guide to the application of pyrolysis techniques to various samples and sample types for a diversity of fields including microbiology, forensic science, industrial research, and environmental analysis. The much-anticipated third edition incorporates recent technological advances that increase the technique’s sensitivity to trace elements, improve its reproducibility, and expand its applicability. The book reviews the types of instrumentation available to perform pyrolysis and offers guidance for interfacing instruments and integrating other analytical techniques, including gas chromatography and mass spectrometry. Fully updated with new sample pyrograms, figures, references, and real-world examples, this edition also highlights new areas of application including cultural materials, forensic analysis, and environmental studies. This book illustrates how the latest advances make pyrolysis a practical, cost-effective, reliable, and flexible alternative for increasingly complex sample analyses. Analytical Pyrolysis Handbook, Third Edition is an essential, one-stop guide for determining if pyrolysis meets application-specific needs as well as performing pyrolysis and handling the data obtained.
Applied Pyrolysis Handbook
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Author : Thomas P. Wampler
language : en
Publisher: CRC Press
Release Date : 1995-02-08
Applied Pyrolysis Handbook written by Thomas P. Wampler and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 1995-02-08 with Science categories.
"Offers concise coverage of pyrolysis techniques in the analytical laboratory--concentrating on practical applications to real-world samples and sample types. Shows how pyrolysis can be used for a wide range of materials, including forensic evidence, paints, fibers, textiles, paper, ink, photocopies, art and museum pieces, synthetic polymers, and natural substances."
Pyrolysis Gc Ms Data Book Of Synthetic Polymers
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Author : Shin Tsuge
language : en
Publisher: Elsevier
Release Date : 2011-08-02
Pyrolysis Gc Ms Data Book Of Synthetic Polymers written by Shin Tsuge and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2011-08-02 with Science categories.
In this data book, both conventional Py-GC/MS where thermal energy alone is used to cause fragmentation of given polymeric materials and reactive Py-GC/MS in the presence of organic alkaline for condensation polymers are compiled. Before going into detailed presentation of the data, however, acquiring a firm grip on the proper understanding about the situation of Py-GC/MS would promote better utilization of the following pyrolysis data for various polymers samples. This book incorporates recent technological advances in analytical pyrolysis methods especially useful for the characterization of 163 typical synthetic polymers. The book briefly reviews the instrumentation available in advanced analytical pyrolysis, and offers guidance to perform effectually this technique combining with gas chromatography and mass spectrometry. Main contents are comprehensive sample pyrograms, thermograms, identification tables, and representative mass spectra (MS) of pyrolyzates for synthetic polymers. This edition also highlights thermally-assisted hydrolysis and methylation technique effectively applied to 33 basic condensation polymers. - Coverage of Py-GC/MS data of conventional pyrograms and thermograms of basic 163 kinds of synthetic polymers together with MS and retention index data for pyrolyzates, enabling a quick identification - Additional coverage of the pyrograms and their related data for 33 basic condensation polymers obtained by the thermally-assisted hydrolysis and methylation technique - All compiled data measured under the same experimental conditions for pyrolysis, gas chromatography and mass spectrometry to facilitate peak identification - Surveyable instant information on two facing pages dedicated to the whole data of a given polymer sample
Analytical Pyrolysis
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Author : Peter Kusch
language : en
Publisher: BoD – Books on Demand
Release Date : 2019-02-13
Analytical Pyrolysis written by Peter Kusch and has been published by BoD – Books on Demand this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019-02-13 with Science categories.
Analytical pyrolysis deals with the structural identification and quantitation of pyrolysis products with the ultimate aim of establishing the identity of the original material and the mechanisms of its thermal decomposition. The pyrolytic process is carried out in a pyrolyzer interfaced with analytical instrumentation such as gas chromatography (GC), mass spectrometry (MS), gas chromatography coupled with mass spectrometry (GC/MS), or with Fourier-transform infrared spectroscopy (GC/FTIR). By measurement and identification of pyrolysis products, the molecular composition of the original sample can often be reconstructed.This book is the outcome of contributions by experts in the field of pyrolysis and includes applications of the analytical pyrolysis-GC/MS to characterize the structure of synthetic organic polymers and lignocellulosic materials as well as cellulosic pulps and isolated lignins, solid wood, waste particle board, and bio-oil. The thermal degradation of cellulose and biomass is examined by scanning electron micrography, FTIR spectroscopy, thermogravimetry (TG), differential thermal analysis, and TG/MS. The calorimetric determination of high heating values of different raw biomass, plastic waste, and biomass/plastic waste mixtures and their by-products resulting from pyrolysis is described.
Analytical Pyrolysis Of Synthetic Organic Polymers
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Author : Serban C. Moldoveanu
language : en
Publisher: Elsevier
Release Date : 2005-01-20
Analytical Pyrolysis Of Synthetic Organic Polymers written by Serban C. Moldoveanu and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2005-01-20 with Science categories.
Analytical Pyrolysis of Synthetic Organic Polymers is a follow-up to Analytical Pyrolysis of Natural Organic Polymers, which is volume 20 of the series. The main focus of the book is on practical applications of analytical pyrolysis in synthetic organic polymer identification and characterization. The first part of the book has five chapters including an introduction, a discussion on physico-chemistry of thermal degradation of synthetic polymers and on instrumentation used in analytical pyrolysis, a chapter discussing what type of information can be obtained from analytical pyrolysis, and a chapter dedicated to the analysis and characterization of synthetic polymers.The second part systematically covers the analytical pyrolysis of various classes of synthetic polymers. Some theoretical background for the understanding of polymer structure using analytical pyrolysis is also discussed.* Includes broad coverage of organic synthetic macromolecules* Focuses on physico-chemistry of thermal degradation, and the analytical pyrolysis of various classes of synthetic polymers* Is well written and suitable for both researchers and chemists working in analytical chemistry or in synthetic polymers
Applied Pyrolysis Handbook
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Author : Thomas P. Wampler
language : en
Publisher: CRC Press
Release Date : 2006-12-13
Applied Pyrolysis Handbook written by Thomas P. Wampler and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2006-12-13 with Science categories.
Analytical pyrolysis allows scientists to use routine laboratory instrumentation for analyzing complex, opaque, or insoluble samples more effectively than other analytical techniques alone. Applied Pyrolysis Handbook, Second Edition is a practical guide to the application of pyrolysis techniques to various samples and sample types for a dive
Analytical Pyrolysis Of Natural Organic Polymers
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Author : S.C. Moldoveanu
language : en
Publisher: Elsevier
Release Date : 1998-11-11
Analytical Pyrolysis Of Natural Organic Polymers written by S.C. Moldoveanu and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 1998-11-11 with Science categories.
Analytical pyrolysis is one of the many tools utilized for the study of natural organic polymers. This books describes in three parts the methodology of analytical pyrolysis, the results of pyrolysis for a variety of biopolymers, and several practical applications of analytical pyrolysis on natural organic polymers and their composite materials. Analytical pyrolysis methodology covers two distinct subjects, the instrumentation used for pyrolysis and the analytical methods that are applied for the analysis of the pyrolysis products. A variety of pyrolytic techniques and of analytical instruments commonly coupled with pyrolysis devices are given.The description of the results of pyrolysis for biopolymers and some chemically modified natural organic polymers is the core of the book. The main pyrolysis products of numerous compounds as well as the proposed mechanisms for their pyrolysis are described. In this part an attempt is made to present as much as possible the chemistry of the pyrolytic process of natural organic polymers.The applications of analytical pyrolysis include topics such as polymer detection used for example in forensic science, structure elucidation of specific polymers, and identification of small molecules present in polymers (anti-oxidants, plasticizers, etc.). Also, the degradation during heating is a subject of major interest in many practical applications regarding the physical properties of polymers. The applications to composite polymeric materials are in the fields of classification of microorganisms, study of a variety of biological samples, study of fossil materials, etc. Analytical pyrolysis can also be used for obtaining information on the burning area generate pyrolysates that have complex compositions. Their analysis is important in connection with health issues, environmental problems, and taste of food and cigarettes.Features of this book:• Presents analytical pyrolysis as a uniform subject and not as a conglomerate of scientific papers.• Puts together in an organized manner a large volume of available information in this specific field.• Provides original results which address subjects with relatively scarce information in literature.• Gives original views on subjects such as the parallel between the pyrolytic process and the ion fragmentation in mass spectrometry.• Includes the role of pyrolysis in the burning process.The three parts of the book are covered in 18 chapters, each divided into sections. Some sections are further divided by particular subjects. References are given for each chapter, and an effort has been made to include as much as possible from the available representative information. A few unpublished personal results are also included.
Practical Gas Chromatography
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Author : Katja Dettmer-Wilde
language : en
Publisher: Springer
Release Date : 2014-11-05
Practical Gas Chromatography written by Katja Dettmer-Wilde and has been published by Springer this book supported file pdf, txt, epub, kindle and other format this book has been release on 2014-11-05 with Science categories.
Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered.
Pyrolysis Gas Chromatography Mass Spectrometry Of Polymeric Materials
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Author : Peter Kusch
language : en
Publisher: World Scientific
Release Date : 2018-10-08
Pyrolysis Gas Chromatography Mass Spectrometry Of Polymeric Materials written by Peter Kusch and has been published by World Scientific this book supported file pdf, txt, epub, kindle and other format this book has been release on 2018-10-08 with Science categories.
The methodology of analytical pyrolysis-GC/MS has been known for several years, but is seldom used in research laboratories and process control in the chemical industry. This is due to the relative difficulty of interpreting the identified pyrolysis products as well as the variety of them. This book contains full identification of several classes of polymers/copolymers and biopolymers that can be very helpful to the user. In addition, the practical applications can encourage analytical chemists and engineers to use the techniques explored in this volume.The structure and the functions of various types of pyrolyzers and the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C are described. Practical applications of these techniques are also included, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems.
Biochar
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Author : Balwant Singh
language : en
Publisher: CSIRO PUBLISHING
Release Date : 2017-03
Biochar written by Balwant Singh and has been published by CSIRO PUBLISHING this book supported file pdf, txt, epub, kindle and other format this book has been release on 2017-03 with Nature categories.
Interest in biochar among soil and environment researchers has increased dramatically over the past decade. Biochar initially attracted attention for its potential to improve soil fertility and to uncouple the carbon cycle, by storing carbon from the atmosphere in a form that can remain stable for hundreds to thousands of years. Later it was found that biochar had applications in environmental and water science, mining, microbial ecology and other fields. Beneficial effects of biochar and its environmental applications cannot be fully realised unless the chemical, physical, structural and surface properties of biochar are known. Currently many of the analytical procedures used for biochar analysis are not well defined, which makes it difficult to choose the right biochar for an intended use and to compare the existing data for biochars. Also, in some instances the use of inappropriate procedures has led to erroneous or inaccurate values for biochars in the scientific literature. Biochar: A Guide to Analytical Methods fills this gap and provides procedures and guidelines for routine and advanced characterisation of biochars. Written by experts, each chapter provides background to a technique or procedure, a stepwise guide to analyses, and includes data for biochars made from a range of feedstocks common to all presented methods. Discussion about the unique features, advantages and disadvantages of a particular technique is an explicit focus of this handbook for biochar analyses. Biochar is primarily intended for researchers, postgraduate students and practitioners who require knowledge of biochar properties. It will also serve as an important resource for researchers, industry and regulatory agencies dealing with biochar.