Chromatography Mass Spectroscopy In Polymer Analysis
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Chromatography Mass Spectroscopy In Polymer Analysis
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Author : T. R Crompton
language : en
Publisher: Smithers Rapra
Release Date : 2010-12-02
Chromatography Mass Spectroscopy In Polymer Analysis written by T. R Crompton and has been published by Smithers Rapra this book supported file pdf, txt, epub, kindle and other format this book has been release on 2010-12-02 with Science categories.
The combination of chromatography with mass spectroscopy is a very useful technique which is being increasingly used by polymer chemists to improve existing polymers and to discover new ones with specific physical properties such as thermal stability and retention of properties over a long service life.This technique is extremely powerful for the analysis and characterisation of polymers and is often based on the use of controlled chromatography - mass spectroscopy to measure a polymer's decomposition with techniques such as pyrolysis, followed by chromatography to separate any breakdown product, and, finally, mass spectroscopy, to achieve an unequivocal identification of the pyrolysis products obtained. The detail that can be obtained by such methods includes structure of the polymer backbone, branching, end groups, isomeric detail and fine detail in the structure of copolymers.The first three chapters of the book discuss the various chromatographic and mass spectroscopic techniques now available.Chapters 3-8 cover the complementary methods, based on the combination of mass spectroscopy with various chromatographic techniques such as high-performance liquid chromatography, gas chromatography and supercritical fluid chromatography.Pyrolysis chromatography-mass spectroscopy is a method of studying the structure of polymers which involves subjecting the polymer pyrolysis products to a chromatographic technique to simplify subsequent analysis and, finally mass spectroscopy to identify the pyrolysis products with the possibility of deducing finer details of polymer structure than were previously attainable by classical methods (Chapters 9-11).By providing a thorough up-to-date review of work in this field it is hoped that the book will be of interest to all those engaged in polymer research and development, and polymer users in general.
Pyrolysis Gas Chromatography Mass Spectrometry Of Polymeric Materials
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Author : Peter Kusch
language : en
Publisher: World Scientific
Release Date : 2018-10-08
Pyrolysis Gas Chromatography Mass Spectrometry Of Polymeric Materials written by Peter Kusch and has been published by World Scientific this book supported file pdf, txt, epub, kindle and other format this book has been release on 2018-10-08 with Science categories.
The methodology of analytical pyrolysis-GC/MS has been known for several years, but is seldom used in research laboratories and process control in the chemical industry. This is due to the relative difficulty of interpreting the identified pyrolysis products as well as the variety of them. This book contains full identification of several classes of polymers/copolymers and biopolymers that can be very helpful to the user. In addition, the practical applications can encourage analytical chemists and engineers to use the techniques explored in this volume.The structure and the functions of various types of pyrolyzers and the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C are described. Practical applications of these techniques are also included, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems.
Mass Spectrometry Of Polymers
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Author : Giorgio Montaudo
language : en
Publisher: CRC Press
Release Date : 2001-10-29
Mass Spectrometry Of Polymers written by Giorgio Montaudo and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2001-10-29 with Science categories.
Mass Spectrometry (MS) has rapidly become an indispensable tool in polymer analysis, and modern MS today complements in many ways the structural data provided by Nuclear Magnetic Resonance (NMR) and Infrared (IR) methods. Recent advances have sparked a growing interest in this field and established a need for a summary of progress made and results
Pyrolysis Gc Ms Data Book Of Synthetic Polymers
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Author : Shin Tsuge
language : en
Publisher: Elsevier
Release Date : 2011-08-02
Pyrolysis Gc Ms Data Book Of Synthetic Polymers written by Shin Tsuge and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2011-08-02 with Science categories.
In this data book, both conventional Py-GC/MS where thermal energy alone is used to cause fragmentation of given polymeric materials and reactive Py-GC/MS in the presence of organic alkaline for condensation polymers are compiled. Before going into detailed presentation of the data, however, acquiring a firm grip on the proper understanding about the situation of Py-GC/MS would promote better utilization of the following pyrolysis data for various polymers samples. This book incorporates recent technological advances in analytical pyrolysis methods especially useful for the characterization of 163 typical synthetic polymers. The book briefly reviews the instrumentation available in advanced analytical pyrolysis, and offers guidance to perform effectually this technique combining with gas chromatography and mass spectrometry. Main contents are comprehensive sample pyrograms, thermograms, identification tables, and representative mass spectra (MS) of pyrolyzates for synthetic polymers. This edition also highlights thermally-assisted hydrolysis and methylation technique effectively applied to 33 basic condensation polymers. - Coverage of Py-GC/MS data of conventional pyrograms and thermograms of basic 163 kinds of synthetic polymers together with MS and retention index data for pyrolyzates, enabling a quick identification - Additional coverage of the pyrograms and their related data for 33 basic condensation polymers obtained by the thermally-assisted hydrolysis and methylation technique - All compiled data measured under the same experimental conditions for pyrolysis, gas chromatography and mass spectrometry to facilitate peak identification - Surveyable instant information on two facing pages dedicated to the whole data of a given polymer sample
Mass Spectrometry In Polymer Chemistry
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Author : Christopher Barner-Kowollik
language : en
Publisher: John Wiley & Sons
Release Date : 2012-01-10
Mass Spectrometry In Polymer Chemistry written by Christopher Barner-Kowollik and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-01-10 with Science categories.
Combining an up-to-date insight into mass-spectrometric polymer analysis beyond MALDI with application details of the instrumentation, this is a balanced and thorough presentation of the most important and widely used mass-spectrometric methods. Written by the world's most proficient experts in the field, the book focuses on the latest developments, covering such technologies and applications as ionization protocols, tandem and liquid chromatography mass spectrometry, gas-phase ion-separation techniques and automated data processing. Chapters on sample preparation, polymer degradation and the usage of mass-spectrometric tools on an industrial scale round off the book. As a result, both entrants to the field and experienced researchers are able to choose the appropriate methods and instrumentations -- and to assess their respective strengths and limitations -- for the characterization of polymer compounds.
Maldi Tof Mass Spectrometry Of Synthetic Polymers
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Author : Harald Pasch
language : en
Publisher: Springer Science & Business Media
Release Date : 2003-02-27
Maldi Tof Mass Spectrometry Of Synthetic Polymers written by Harald Pasch and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2003-02-27 with Science categories.
MALDI-TOF mass spectrometry is one of the latest and most fascinating new developments in the analysis of organic compounds. Originally developed for the analysis of biomolecules, it has developed into one of the most powerful techniques for the characterization of synthetic polymers. This book describes the fundamentals of the MALDI process and the technical features of MALDI-TOF instrumentation. It reviews the application of MALDI-TOF for identification, chemical and molar mass analysis of synthetic polymers. With many examples, the monograph examines experimental protocols for the determination of endgroups, the analysis of copolymers and additives, and the coupling of liquid chromatography and MALDI-TOF in detail.
Mass Spectrometry In Polymer Chemistry
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Author : Christopher Barner-Kowollik
language : en
Publisher: John Wiley & Sons
Release Date : 2012-01-27
Mass Spectrometry In Polymer Chemistry written by Christopher Barner-Kowollik and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-01-27 with Science categories.
Combining an up-to-date insight into mass-spectrometric polymer analysis beyond MALDI with application details of the instrumentation, this is a balanced and thorough presentation of the most important and widely used mass-spectrometric methods. Written by the world's most proficient experts in the field, the book focuses on the latest developments, covering such technologies and applications as ionization protocols, tandem and liquid chromatography mass spectrometry, gas-phase ion-separation techniques and automated data processing. Chapters on sample preparation, polymer degradation and the usage of mass-spectrometric tools on an industrial scale round off the book. As a result, both entrants to the field and experienced researchers are able to choose the appropriate methods and instrumentations -- and to assess their respective strengths and limitations -- for the characterization of polymer compounds.
Mass Spectrometry Of Polymers
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Author : Giorgio Montaudo
language : en
Publisher: CRC Press
Release Date : 2001-10-29
Mass Spectrometry Of Polymers written by Giorgio Montaudo and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2001-10-29 with Science categories.
Mass Spectrometry (MS) has rapidly become an indispensable tool in polymer analysis, and modern MS today complements in many ways the structural data provided by Nuclear Magnetic Resonance (NMR) and Infrared (IR) methods. Recent advances have sparked a growing interest in this field and established a need for a summary of progress made and results
Molecular Characterization Of Polymers
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Author : Muhammad Imran Malik
language : en
Publisher: Elsevier
Release Date : 2021-03-09
Molecular Characterization Of Polymers written by Muhammad Imran Malik and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2021-03-09 with Technology & Engineering categories.
Molecular Characterization of Polymers presents a range of advanced and cutting-edge methods for the characterization of polymers at the molecular level, guiding the reader through theory, fundamentals, instrumentation, and applications, and supporting the end goal of efficient material selection and improved material performance. Each chapter focuses on a specific technique or family of techniques, including the different areas of chromatography, field flow fractionation, long chain branching, static and dynamic light scattering, mass spectrometry, NMR, X-Ray and neutron scattering, polymer dilute solution viscometry, microscopy, and vibrational spectroscopy. In each case, in-depth coverage explains how to successfully implement and utilize the technique. This practical resource is highly valuable to researchers and advanced students in polymer science, materials science, and engineering, and to those from other disciplines and industries who are unfamiliar with polymer characterization techniques. - Introduces a range of advanced characterization methods, covering aspects such as molecular weight, polydispersity, branching, composition, and tacticity - Enables the reader to understand and to compare the available technique, and implement the selected technique(s), with a view to improving properties of the polymeric material - Establishes a strong link between basic principles, characterization techniques, and real-life applications
Maldi Mass Spectrometry For Synthetic Polymer Analysis
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Author : Liang Li
language : en
Publisher: John Wiley & Sons
Release Date : 2009-10-22
Maldi Mass Spectrometry For Synthetic Polymer Analysis written by Liang Li and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2009-10-22 with Science categories.
Principles and Practices of Polymer Mass Spectrometry helps readers acquire the skills necessary for selecting the optimal methods, handling samples, analyzing the data, and interpreting the results of the mass spectrometry of polymers. This guide describes the principles of polymer MS and best practices in polymer characterization. It discusses different approaches, including MALDI, ESI, TOF MS, and FT-MS. It provides a guide to developing appropriate sample preparation protocols for different polymers. Complete with examples of applications and experiments, this is an excellent reference for scientists, researchers, graduate students, and others.