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Cracks In Superalloys


Cracks In Superalloys
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Cracks In Superalloys


Cracks In Superalloys
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Author : Jonas Saarimäki
language : en
Publisher: Linköping University Electronic Press
Release Date : 2018-01-18

Cracks In Superalloys written by Jonas Saarimäki and has been published by Linköping University Electronic Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2018-01-18 with categories.


Gas turbines are widely used in industry for power generation and as a power source at hard to reach locations where other possibilities for electrical power supplies are insufficient. New ways of producing greener energy is needed to reduce emission levels. This can be achieved by increasing the combustion temperature of gas turbines. High combustion temperatures can be detrimental and degrade critical components. This raises the demands on the high temperature performance of the superalloys used in gas turbine components. These components are frequently subjected to different cyclic loads combined with for example dwell-times and overloads at elevated temperatures, which can influence the crack growth. Dwell-times have been shown to accelerate crack growth and change cracking behaviour in both Inconel 718, Haynes 282 and Hastelloy X. On the other hand, overloads at the beginning of a dwell-time cycle have been shown to retard the dwell-time effect on crack growth in Inconel 718. More experiments and microstructural investigations are needed to better understand these effects. The work presented in this thesis was conducted under the umbrella of the research program Turbo Power; "High temperature fatigue crack propagation in nickel-based superalloys", where I have mainly looked at fatigue crack growth mechanisms in superalloys subjected to dwell-fatigue, which can have a devastating effect on crack propagation behaviour. Mechanical testing was performed under operation-like cycles in order to achieve representative microstructures and material data for the subsequent microstructural work. Microstructures were investigated using light optical microscopy and scanning electron microscopy (SEM) techniques such as electron channeling contrast imaging (ECCI) and electron backscatter diffraction (EBSD). The outcome of this work has shown that there is a significant increase in crack growth rate when dwell-times are introduced at maximum load (0 % overload) in the fatigue cycle. With the introduction of a dwell-time there is also a shift from transgranular to intergranular crack growth for both Inconel 718 and Haynes 282. The crack growth rate decreases with increasing overload levels in Inconel 718 when an overload is applied prior to the dwell-time. At high temperature, intergranular crack growth was observed in Inconel 718 as a result of oxidation and the creation of nanometric voids. Another observed growth mechanism was crack advance along ?-phase boundaries with subsequent oxidation of the ?-phase. This thesis comprises two parts. Part I gives an introduction to the field of superalloys and the acting microstructural mechanisms related to fatigue and crack propagation. Part II consists of five appended papers, which report the work completed as part of the project.



Effect Of Dwell Times On Crack Propagation In Superalloys


Effect Of Dwell Times On Crack Propagation In Superalloys
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Author : Jonas Saarimäki
language : en
Publisher: Linköping University Electronic Press
Release Date : 2015-12-10

Effect Of Dwell Times On Crack Propagation In Superalloys written by Jonas Saarimäki and has been published by Linköping University Electronic Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2015-12-10 with categories.


Gas turbines are widely used in industry for power generation and as a power source at "hard to reach" locations where other possibilities for electrical supply are insufficient. There is a strong need for greener energy, considering the effect that pollution has had on global warming, and we need to come up with ways of producing cleaner electricity. A way to achieve this is by increasing the combustion temperature in gas turbines. This increases the demand on the high temperature performance of the materials used e.g. superalloys in the turbine. These high combustion temperatures can lead to detrimental degradation of critical components. These components are commonly subjected to cyclic loading of different types e.g. combined with dwell-times and overloads at elevated temperatures, which influence the crack growth. Dwell-times have shown to accelerate crack growth and change the cracking behaviour in both Inconel 718 and Haynes 282. Overloads at the beginning of the dwell-time cycle have shown to retard the dwell time effect on crack growth in Inconel 718. To understand these effects more microstructural investigations are needed. The work presented in this licentiate thesis was conducted under the umbrella of the research program Turbo Power; "High temperature fatigue crack propagation in nickel-based superalloys", concentrating on fatigue crack growth mechanisms in superalloys during dwell-times, which have shown to have a devastating effect on the crack propagation behaviour. Mechanical testing was performed under operation-like conditions in order to achieve representative microstructures and material data for the subsequent microstructural work. The microstructures were microscopically investigated in a scanning electron microscope (SEM) using electron channeling contrast imaging (ECCI) as well as using light optical microscopy. The outcome of this work has shown that there is a significant increase in crack growth rate when dwell-times are introduced at the maximum load (0% overload) in the fatigue cycle. With the introduction of a dwell-time there is also a shift from transgranular to intergranular crack growth for both Inconel 718 and Haynes 282. When an overload is applied prior to the dwell-time, the crack growth rate decreases with increasing overload levels in Inconel 718. At high temperature crack growth in Inconel 718 took place as intergranular crack growth along grain boundaries due to oxidation and the creation of nanometric voids. Another observed growth mechanism was crack advance along phase boundaries with subsequent severe oxidation of the phase. This thesis comprises two parts. The first giving an introduction to the field of superalloys and the acting microstructural mechanisms that influence fatigue during dwell times. The second part consists of two appended papers, which report the work completed so far in the project.



Aspects Of Crack Growth In Single Crystal Nickel Base Superalloys


Aspects Of Crack Growth In Single Crystal Nickel Base Superalloys
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Author : Christian Busse
language : en
Publisher: Linköping University Electronic Press
Release Date : 2017-11-20

Aspects Of Crack Growth In Single Crystal Nickel Base Superalloys written by Christian Busse and has been published by Linköping University Electronic Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2017-11-20 with categories.


This Licentiate of Engineering thesis is a product of the results generated in the research project KME-702, which comprises modelling, microstructure investigations and material testing of cast nickel-base superalloys. The main objective of this work is to model the fatigue crack propagation behaviour in single-crystal nickel-base superalloys. To achieve this, the influence of the crystal orientations on the cracking behaviour is assessed. The results show that the crystal orientation is strongly affecting the material response and must be accounted for. Furthermore, a linear elastic crack driving force parameter suitable for describing crystallographic cracking has been developed. This parameter is based on resolved anisotropic stress intensity factors and is able to predict the correct crystallographic cracking plane after a transition from a Mode I crack. Finally, a method to account for inelastic deformations in a linear elastic fracture mechanics context was investigated. A residual stress field is extracted from an uncracked finite-element model with a perfectly plastic material model and superimposed on the stress field from the cracked model with a linear elastic material model to account for the inelastic deformations during the determination of the crack driving force. The modelling work is validated by material testing on two different specimen geometries at different temperatures. This Licentiate of Engineering thesis consists of two parts, where Part I gives an introduction and background to the research area, while Part II consists of three papers. Denna licentiatavhandling är en produkt av resultat som genererats i forskningsprojektet KME-702, och omfattar modellering, mikrostrukturundersökningar och materialprovning av gjutna nickelbaserade superlegeringar. Huvudsyftet med detta arbete är att modellera sprickförloppet under utmattning i enkristallina nickelbaserade superlegeringar. För att uppnå detta har kristallorienteringens inverkan på sprickbeteendet utvärderats. Resultaten visar att kristallorienteringen har en stark inverkan på materialbeteendet, således måste hänsyn till denna tas. Dessutom har en linjär-elastisk sprickdrivkraftsparameter lämplig att beskriva kristallografisk sprickbildning utvecklats. Denna parameter är baserad på anisotropa spänningsintensitetsfaktorer på kristallplan och kan prediktera det korrekta kristallografiska sprickplanet efter övergång från Modus I spricka. Slutligen har undersökts en metod för att ta hand om inelastiska deformationer i en linjär-elastisk brottmekanikskontext. Ett restspänningsfält extraherades från en osprucken finita element modell med en ideal plastisk materialmodell. Denna överlagrades på spänningsfältet från den spruckna modellen, som analyserades med en linjär-elastisk materialmodell, för att ta hänsyn till de inelastiska deformationerna vid bestämning av sprickdrivkraften. Modelleringsarbetet validerades genom materialprovning på två olika provgeometrier vid olika temperaturer. Licentiatavhandlingen består av två delar, där del I ger en introduktion och bakgrund till forskningsområdet medan del II består av tre papper. Dieses Lizentiat der Ingenieurwissenschaften ist im Rahmen des Forschungsprojekts KME-702 entstanden, welches Modellierung, Mikrostrukturuntersuchungen und Materialtests von gegossenen nickelbasierten Superlegierungen umfasst. Das Hauptziel dieser Arbeit ist die Modellierung der Ermüdungsrissausbreitung in einkristallinen nickelbasierten Superlegierungen. Um dieses zu erreichen, wurde der Einfluss der Kristallorientierungen auf das Rissverhalten untersucht. Die Ergebnisse zeigen, dass die Kristallorientierung das Materialverhalten stark beeinflusst und daher berücksichtigt werden muss. Darüber hinaus wurde ein linear elastischer Rissantriebskraftparameter entwickelt, der zum Beschreiben von kristallographischen Rissen geeignet ist. Dieser Parameter basiert auf aufgelösten anisotropen Spannungsintensitätsfaktoren und ist in der Lage, die korrekte kristallographische Rissebene nach einem Übergang von einem Modus I Riss vorherzusagen. Abschließend wird in einem linear-elastisch bruchmechanischen Kontext eine Methode untersucht, die nichtelastischen Deformationen bei der Bestimmung der Rissantriebskraft zu berücksichtigen. Dazu wird aus einem Finite-Elemente Modell, welches keinen Riss aufweist und mit einem perfekt plastischen Materialmodell beschrieben wird, das Restspannungsfeld extrahiert und dem Spannungsfeld überlagert, welches aus dem Modell mit Riss unter Verwendung eines linear elastischen Materialmodells erzeugt wurde. Die Modellierung wird durch Materialtests an zwei verschiedenen Probengeometrien bei unterschiedlichen Temperaturen validiert. Dieses Lizentiat der Ingenieurwissenschaften besteht aus zwei Teilen, wobei Teil I eine Einführung und einen Hintergrund in das Forschungsgebiet gibt, während Teil II aus drei Forschungsartikeln besteht.



Cracks In Superalloys


Cracks In Superalloys
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Author : Jonas Saarimäki
language : en
Publisher:
Release Date : 2018

Cracks In Superalloys written by Jonas Saarimäki and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2018 with categories.




Modelling Of Crack Growth In Single Crystal Nickel Base Superalloys


Modelling Of Crack Growth In Single Crystal Nickel Base Superalloys
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Author : Christian Busse
language : en
Publisher: Linköping University Electronic Press
Release Date : 2019-09-24

Modelling Of Crack Growth In Single Crystal Nickel Base Superalloys written by Christian Busse and has been published by Linköping University Electronic Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019-09-24 with categories.


This dissertation was produced at the Division of Solid Mechanics at Linköping University and is part of a research project, which comprises modelling, microstructure investigations and material testing of cast nickel-base superalloys. The main objective of this work was to deepen the understanding of the fracture behaviour of single-crystal nickel-base superalloys and to develop a model to predict the fatigue crack growth behaviour. Frequently, crack growth in these materials has been observed to follow one of two distinct cracking modes; Mode I like cracking perpendicular to the loading direction or crystallographic crack growth on the octahedral {111}-planes, where the latter is associated with an increased fatigue crack growth rate. Thus, it is of major importance to account for this behaviour in component life prediction. Consequently, a model for the prediction of the transition of cracking modes and the correct active crystallographic plane, i.e. the crack path, and the crystallographic crack growth rate has been developed. This model is based on the evaluation of appropriate crack driving forces using three-dimensional finite-element simulations. A special focus was given towards the influence of the crystallographic orientation on the fracture behaviour. Further, a model to incorporate residual stresses in the crack growth modelling is presented. All modelling work is calibrated and validated by experiments on different specimen geometries with different crystallographic orientations. This dissertation consists of two parts, where Part I gives an introduction and background to the field of research, while Part II consists of six appended papers. Die vorliegende Dissertation wurde in der Abteilung für Festigkeitslehre an der Universität von Linköping erstellt und ist Teil eines Forschungsprojektes, welches Modellierung, Mikrostrukturuntersuchungen und Materialtests von gegossenen nickelbasierten Superlegierungen umfasst. Das Hauptziel dieser Arbeit war es, das Verständnis des Bruchverhaltens von einkristallinen Superlegierungen auf Nickelbasis zu vertiefen und ein Modell zur Vorhersage des Wachstumsverhaltens von Ermüdungsrissen zu entwickeln. Es wurde beobachtet, dass das Risswachstum in diesen Materialien einem von zwei unterschiedlichen Rissmodi folgt; Modus I Rissfortschritt senkrecht zur Belastungsrichtung oder kristallographisches Risswachstum auf den oktaedrischen f111g-Ebenen, wobei letzteres mit einer erhöhten Ermüdungsrisswachstumsrate verbunden ist. Somit ist es von grosser Bedeutung dieses Verhalten in der Lebensdauervorhersage einer Komponente zu berücksichtigen. Demzufolge wurde ein Modell für die Vorhersage des Übergangs zwischen den Rissmodi und der korrekten aktiven kristallographischen Ebene, d.h. des Risspfades, sowie der kristallographischen Risswachstumsrate erarbeitet. Dieses Modell basiert auf geeigneten Rissantriebskräften, welche mit Hilfe dreidimensionaler Finite-Elemente-Simulationen berechnet werden. Im Fokus stand insbesondere der Einuss der kristallographischen Orientierung auf das Bruchverhalten. Ausserdem wird ein Modell zur Berücksichtigung von Restspannungen in der Risswachstumsmodellierung präsentiert. Alle Modellierungsarbeiten wurden durch Experimente an verschiedenen Probengeometrien mit unterschiedlichen kristallographischen Orientierungen kalibriert und validiert. Diese Dissertation besteht aus zwei Teilen, wobei Teil I aus einer Einführung und einem Hintergrund in das Forschungsgebiet und Teil II aus sechs beigefügten Forschungsartikeln besteht.



Fatigue Crack Initiation And The Growth Of Short Cracks In Nickel Based Superalloys


Fatigue Crack Initiation And The Growth Of Short Cracks In Nickel Based Superalloys
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Author : James Finis McCarver
language : en
Publisher:
Release Date : 1981

Fatigue Crack Initiation And The Growth Of Short Cracks In Nickel Based Superalloys written by James Finis McCarver and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1981 with Chromium-cobalt-nickel-molybdenum alloys categories.




Alloy Design And Characterization Of Strengthened Nickel Based Superalloys For Additive Manufacturing


Alloy Design And Characterization Of Strengthened Nickel Based Superalloys For Additive Manufacturing
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Author : Jinghao Xu
language : en
Publisher: Linköping University Electronic Press
Release Date : 2021-01-28

Alloy Design And Characterization Of Strengthened Nickel Based Superalloys For Additive Manufacturing written by Jinghao Xu and has been published by Linköping University Electronic Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2021-01-28 with categories.


Nickel-based superalloys, an alloy system bases on nickel as the matrix element with the addition of up to 10 more alloying elements including chromium, aluminum, cobalt, tungsten, molybdenum, titanium, and so on. Through the development and improvement of nickel-based superalloys in the past century, they are well proved to show excellent performance at the elevated service temperature. Owing to the combination of extraordinary high-temperature mechanical properties, such as monotonic and cyclic deformation resistance, fatigue crack propagation resistance; and high-temperature chemical properties, such as corrosion and oxidation resistance, phase stability, nickel-based superalloys are widely used in the critical hot-section components in aerospace and energy generation industries. The success of nickel-based superalloy systems attributes to both the well-tailored microstructures with the assistance of carefully doped alloying elements, and the intently developed manufacturing processes. The microstructure of the modern nickel-based superalloys consists of a two-phase configuration: the intermetallic precipitates (Ni,Co)3(Al,Ti,Ta) known as γ′ phase dispersed into the austenite γ matrix, which is firstly introduced in the 1940s. The recently developed additive manufacturing (AM) techniques, acting as the disruptive manufacturing process, offers a new avenue for producing the nickel-based superalloy components with complicated geometries. However, γ′ strengthened nickel-based superalloys always suffer from the micro-cracking during the AM process, which is barely eliminated by the process optimization. On this basis, the new compositions of γ′ strengthened nickel-based superalloy adapted to the AM process are of great interest and significance. This study sought to design novel γ′ strengthened nickel-based superalloys readily for AM process with limited cracking susceptibility, based on the understanding of the cracking mechanisms. A two-parameter model is developed to predict the additive manufacturability for any given composition of a nickel-based superalloy. One materials index is derived from the comparison of the deformation-resistant capacity between dendritic and interdendritic regions, while another index is derived from the difference of heat resistant capacity of these two spaces. By plotting the additive manufacturability diagram, the superalloys family can be categorized into the easy-to-weld, fairly-weldable, and non-weldable regime with the good agreement of the existed knowledge. To design a novel superalloy, a Cr-Co-Mo-W-Al-Ti-Ta-Nb-Fe-Ni alloy family is proposed containing 921,600 composition recipes in total. Through the examination of additive manufacturability, undesired phase formation propensity, and the precipitation fraction, one composition of superalloy, MAD542, out of the 921,600 candidates is selected. Validation of additive manufacturability of MAD542 is carried out by laser powder bed fusion (LPBF). By optimizing the LPBF process parameters, the crack-free MAD542 part is achieved. In addition, the MAD542 superalloy shows great resistance to the post-processing treatment-induced cracking. During the post-processing treatment, extensive annealing twins are promoted to achieve the recrystallization microstructure, ensuring the rapid reduction of stored energy. After ageing treatment, up to 60-65% volume fraction of γ′ precipitates are developed, indicating the huge potential of γ′ formation. Examined by the high-temperature slow strain rate tensile and constant loading creep testing, the MAD542 superalloy shows superior strength than the LPBF processed and hot isostatic pressed plus heat-treated IN738LC superalloy. While the low ductility of MAD542 is existed, which is expected to be improved by modifying the post-processing treatment scenarios and by the adjusting building direction in the following stages of the Ph.D. research. MAD542 superalloy so far shows both good additive manufacturability and mechanical potentials. Additionally, the results in this study will contribute to a novel paradigm for alloy design and encourage more γ′-strengthened nickel-based superalloys tailored for AM processes in the future.



Fatigue Crack Propagation Of Nickel Base Superalloys At 650 C


Fatigue Crack Propagation Of Nickel Base Superalloys At 650 C
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Author : TP. Gabb
language : en
Publisher:
Release Date : 1988

Fatigue Crack Propagation Of Nickel Base Superalloys At 650 C written by TP. Gabb and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1988 with Creep categories.


The 650°C fatigue crack propagation behavior of two nickel-base superalloys, René 95 and Waspaloy, were studied with particular emphasis placed on understanding the roles of creep, environment, and two key grain boundary alloying additions, boron and zirconium. Comparison of air and vacuum data showed the air environment to be detrimental over a wide range of frequencies for both alloys. In-depth analysis of René 95 showed that at lower frequencies, such as 0.02 Hz, failure in air occurred by intergranular, environmentally assisted creep crack growth, while at higher frequencies, up to 5.0 Hz, environmental interactions were still evident but creep effects were minimized. The effect of boron and zirconium in Waspaloy was found to be important where environmental and/or creep interactions were present. In those instances, removal of boron and zirconium dramatically increased crack growth. It is therefore plausible that effective dilution of these elements may explain, in part, a previously observed trend in which crack growth rates increased with decreasing grain size.



A Study Of The Fatigue Behavior Of Small Cracks In Nickel Base Superalloys


A Study Of The Fatigue Behavior Of Small Cracks In Nickel Base Superalloys
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Author :
language : en
Publisher:
Release Date : 1988

A Study Of The Fatigue Behavior Of Small Cracks In Nickel Base Superalloys written by and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1988 with categories.


The fatigue of behavior of short cracks was investigate in five wrought nickel-base superalloys currently used for aircraft turbine disks. Cracks were initiated at artificial defects and at persistent slip bands. Test frequencies ranged from 20Hz to 10cpm. Fatigue crack growth rates were measured over crack lengths ranging from 10 um to 1mm. Most of the testing was performed in load control with stress ranges approaching the cyclic yield strengths of alloys. Strain controlled tests were performed on IN100 under elastic-plastic cycling conditions. Keywords: Crack propagation; Physical metallurgy.



Near Threshold Crack Growth In Nickel Base Superalloys


Near Threshold Crack Growth In Nickel Base Superalloys
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Author : HR. Van Stone
language : en
Publisher:
Release Date : 1988

Near Threshold Crack Growth In Nickel Base Superalloys written by HR. Van Stone and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1988 with Crack closure categories.


The influence of stress ratio on the elevated-temperature crack growth behavior of the nickel-base superalloys René 95 and Alloy 718 is discussed. The near-threshold and Region II crack growth behavior of a wide variety of microstructures for each alloy are explained using phenomenological descriptions of closure, that is, K-dependent or K-independent closure. K-dependent closure is the type of closure observed for nickel-base superalloys where increasing the R-ratio causes a uniform lateral shift of the entire fatigue crack growth curve. K-independent closure is the type commonly reported for steels and titanium alloys where increasing the R-ratio has a larger influence on near-threshold crack growth than on Region II crack growth. The existence of K-dependent closure in nickel-base superalloys results in microstructurally sensitive crack growth rates, even at high R-ratios. This permits the use of K-based crack growth prediction techniques and simplifies alloy and process development for applications having complex loading spectra.