Early Days Of X Ray Crystallography


Early Days Of X Ray Crystallography
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Early Days Of X Ray Crystallography


Early Days Of X Ray Crystallography
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Author : André Authier
language : en
Publisher: OUP Oxford
Release Date : 2013-08-02

Early Days Of X Ray Crystallography written by André Authier and has been published by OUP Oxford this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-08-02 with Science categories.


The year 2012 marked the centenary of one of the most significant discoveries of the early twentieth century, the discovery of X-ray diffraction (March 1912, by Laue, Friedrich and Knipping) and of Bragg's law (November 1912). The discovery of X-ray diffraction confirmed the wave nature of X-rays and the space-lattice hypothesis. It had two major consequences: the analysis of the structure of atoms, and the determination of the atomic structure of materials. This had a momentous impact in chemistry, physics, mineralogy, material science, biology and X-ray spectroscopy. The book relates the discovery itself, the early days of X-ray crystallography, and the way the news of the discovery spread round the world. It explains how the first crystal structures were determined by William Bragg and his son Lawrence, and recounts which were the early applications of X-ray crystallography in chemistry, mineralogy, materials science, physics, biological sciences and X-ray spectroscopy. It also tells how the concept of space lattice developed since ancient times up to the nineteenth century, and how our conception of the nature of light has changed over time. The contributions of the main actors of the story, prior to the discovery, at the time of the discovery and immediately afterwards, are described through their writings and are put into the context of the time, accompanied by brief biographical details. This thoroughly researched account on the multiple faces of a scientific specialty, X-ray crystallography, is aimed both at the scientists, who rarely subject the historical material of past discoveries in their field to particular scrutiny with regard to the historical details and at the historians of science who often lack the required expert knowledge to scrutinize the involved technical content in sufficient depth (M. Eckert - Metascience).



Fifty Years Of X Ray Diffraction


Fifty Years Of X Ray Diffraction
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Author : P.P. Ewald
language : en
Publisher: Springer Science & Business Media
Release Date : 2012-12-06

Fifty Years Of X Ray Diffraction written by P.P. Ewald and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-06 with Science categories.


Origin, Scope, and Plan of this Book In July 1962 the fiftieth anniversary of Max von Laue's discovery of the Diffraction of X-rays by crystals is going to be celebrated in Munich by a large international group of crystallographers, physi cists, chemists, spectroscopists, biologists, industrialists, and many others who are employing the methods based on Laue's discovery for their own research. The invitation for this celebration will be issued jointly by the Ludwig Maximilian University of Munich, where the discovery was made, by the Bavarian Academy of Sciences, where it was first made public, and by the International Union of Crystallo graphy, which is the international organization of the National Committees of Crystallography formed in some 30 countries to repre sent and advance the interests of the 3500 research workers in this field. The year 1912 also is the birth year of two branches of the physical sciences which developed promptly from Laue's discovery, namely X-ray Crystal Structure Analysis which is most closely linked to the names ofW. H. (Sir William) Bragg and W. L. (Sir Lawrence) Bragg, and X-ray Spectroscopy which is associated with the names of W. H. Bragg, H. G. J. Moseley, M. de Broglie and Manne Siegbahn. Crystal Structure Analysis began in November 1912 with the first papers ofW. L. Bragg, then still a student in Cambridge, in which, by analysis of the Laue diagrams _of zinc blende, he determined the correct lattice upon which the structure of this crystal is built.



Structure Determination By X Ray Crystallography


Structure Determination By X Ray Crystallography
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Author : Mark Ladd
language : en
Publisher: Springer Science & Business Media
Release Date : 2014-07-08

Structure Determination By X Ray Crystallography written by Mark Ladd and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2014-07-08 with Science categories.


The advances in and applications of x-ray and neutron crystallography form the essence of this new edition of this classic textbook, while maintaining the overall plan of the book that has been well received in the academic community since the first edition in 1977. X-ray crystallography is a universal tool for studying molecular structure, and the complementary nature of neutron diffraction crystallography permits the location of atomic species in crystals which are not easily revealed by X-ray techniques alone, such as hydrogen atoms or other light atoms in the presence of heavier atoms. Thus, a chapter discussing the practice of neutron diffraction techniques, with examples, broadens the scope of the text in a highly desirable way. As with previous editions, the book contains problems to illustrate the work of each chapter, and detailed solutions are provided. Mathematical procedures related to the material of the main body of the book are not discussed in detail, but are quoted where needed with references to standard mathematical texts. To address the computational aspect of crystallography, the suite of computer programs from the fourth edition has been revised and expanded. The programs enable the reader to participate fully in many of the aspects of x-ray crystallography discussed in the book. In particular, the program system XRAY* is interactive, and enables the reader to follow through, at the monitor screen, the computational techniques involved in single-crystal structure determination, albeit in two dimensions, with the data sets provided. Exercises for students can be found in the book, and solutions are available to instructors.



Early Papers On Diffraction Of X Rays By Crystals


Early Papers On Diffraction Of X Rays By Crystals
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Author : J.M. Bijvoet
language : en
Publisher: Springer Science & Business Media
Release Date : 2012-12-06

Early Papers On Diffraction Of X Rays By Crystals written by J.M. Bijvoet and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-06 with Technology & Engineering categories.


In the Preface to Early Papers on Diffraction of X-rays by Crystals Volume I (containing Chapters I-V and published in 1969), the history and planning of the complete book were outlined. The publication in two separate and consecutive volumes was merely a matter of management; the compilation of both volumes was done at the same time. There is a distinct difference in subject-matter between both volumes: Volume I contains the fundamentals of the theory, while Volume II treats the practical development of the 'trial' -method and the genesis and first applications of the Fourier method. In the period covered by Early Papers (1912-1935), the trial method leads to the successful conquest of structures with up to a hundred parameters. We conclude the book with Patterson's discovery (1934) of the p2-series as described in his second, more detailed and extended paper of 1935. With this method the apparatus was completed which led to the present undreamt-of successes of the Fourier method in the field of organic chemistry. We have considered the inclusion of Robertson's famous synthesis of the structure of phtalocyanine (1936). However, we decided that its proper place would be at the beginning of a book which, no doubt, will appear one day, describing this later period. Considerations of space caused us to give up the chapter on Texture planned at first.



Structure Determination By X Ray Crystallography


Structure Determination By X Ray Crystallography
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Author : M. Ladd
language : en
Publisher: Springer Science & Business Media
Release Date : 2012-12-06

Structure Determination By X Ray Crystallography written by M. Ladd and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-06 with Science categories.


Crystallography may be described as the science of the structure of materi als, using this word in its widest sense, and its ramifications are apparent over a broad front of current scientific endeavor. It is not surprising, therefore, to find that most universities offer some aspects of crystallography in their undergraduate courses in the physical sciences. It is the principal aim of this book to present an introduction to structure determination by X-ray crystal lography that is appropriate mainly to both final-year undergraduate studies in crystallography, chemistry, and chemical physics, and introductory post graduate work in this area of crystallography. We believe that the book will be of interest in other disciplines, such as physics, metallurgy, biochemistry, and geology, where crystallography has an important part to play. In the space of one book, it is not possible either to cover all aspects of crystallography or to treat all the subject matter completely rigorously. In particular, certain mathematical results are assumed in order that their applications may be discussed. At the end of each chapter, a short bibliog raphy is given, which may be used to extend the scope of the treatment given here. In addition, reference is made in the text to specific sources of information. We have chosen not to discuss experimental methods extensively, as we consider that this aspect of crystallography is best learned through practical experience, but an attempt has been made to simulate the interpretive side of experimental crystallography in both examples and exercises.



An Introduction To X Ray Crystallography


An Introduction To X Ray Crystallography
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Author : Michael M. Woolfson
language : en
Publisher: Cambridge University Press
Release Date : 1997-01-13

An Introduction To X Ray Crystallography written by Michael M. Woolfson and has been published by Cambridge University Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 1997-01-13 with Medical categories.


A textbook for the student beginning a serious study of X-ray crystallography.



Early Papers On Diffraction Of X Rays By Crystals


Early Papers On Diffraction Of X Rays By Crystals
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Author : J. M. Bijvoet
language : en
Publisher: Springer
Release Date : 1969

Early Papers On Diffraction Of X Rays By Crystals written by J. M. Bijvoet and has been published by Springer this book supported file pdf, txt, epub, kindle and other format this book has been release on 1969 with X-ray crystallography categories.




X Ray Crystallography


X Ray Crystallography
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Author : Gregory S. Girolami
language : en
Publisher: University Science Books
Release Date : 2015-07-31

X Ray Crystallography written by Gregory S. Girolami and has been published by University Science Books this book supported file pdf, txt, epub, kindle and other format this book has been release on 2015-07-31 with Science categories.


X-Ray Crystallography is a well-balanced, thorough, and clearly written introduction to the most important and widely practiced technique to determine the arrangement of atoms in molecules and solids. Featuring excellent illustrations and homework problems throughout, the book is intended both for advanced undergraduate and graduate students who are learning the subject for the first time, as well as for those who have practical experience but seek a text summarizing the theory of diffraction and X-ray crystallography. It is organized into three parts: Part 1 deals with symmetry and space groups, Part 2 explains the physics of X rays and diffraction, and Part 3 examines the methods for solving and refining crystal structures. The discussion proceeds in a logical and clear fashion from the fundamentals through to advanced topics such as disorder, twinning, microfocus sources, low energy electron diffraction, charge flipping, protein crystallography, the maximum likelihood method of refinement, and powder, neutron, and electron diffraction. The author's clear writing style and distinctive approach is well suited for chemists, biologists, materials scientists, physicists, and scientists from related disciplines.



X Ray Diffraction Crystallography


X Ray Diffraction Crystallography
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Author : Yoshio Waseda
language : en
Publisher: Springer Science & Business Media
Release Date : 2011-03-18

X Ray Diffraction Crystallography written by Yoshio Waseda and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2011-03-18 with Technology & Engineering categories.


X-ray diffraction crystallography for powder samples is a well-established and widely used method. It is applied to materials characterization to reveal the atomic scale structure of various substances in a variety of states. The book deals with fundamental properties of X-rays, geometry analysis of crystals, X-ray scattering and diffraction in polycrystalline samples and its application to the determination of the crystal structure. The reciprocal lattice and integrated diffraction intensity from crystals and symmetry analysis of crystals are explained. To learn the method of X-ray diffraction crystallography well and to be able to cope with the given subject, a certain number of exercises is presented in the book to calculate specific values for typical examples. This is particularly important for beginners in X-ray diffraction crystallography. One aim of this book is to offer guidance to solving the problems of 90 typical substances. For further convenience, 100 supplementary exercises are also provided with solutions. Some essential points with basic equations are summarized in each chapter, together with some relevant physical constants and the atomic scattering factors of the elements.



Principles Of Protein X Ray Crystallography


Principles Of Protein X Ray Crystallography
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Author : Jan Drenth
language : en
Publisher: Springer Science & Business Media
Release Date : 2013-03-09

Principles Of Protein X Ray Crystallography written by Jan Drenth and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-03-09 with Science categories.


New textbooks at all levels of chemistry appear with great regularity. Some fields such as basic biochemistry, organic reaction mechanisms, and chemical thermodynamics are well represented by many excellent texts, and new or revised editions are published sufficiently often to keep up with progress in research. However, some areas of chemistry, especially many of those taught at the graduate level, suffer from a real lack of up to-date textbooks. The most serious needs occur in fields that are rapidly changing. Textbooks in these subjects usually have to be written by scientists actually involved in the research that is advancing the field. It is not often easy to persuade such individuals to set time aside to help spread the knowledge they have accumulated. Our goal, in this series, is to pinpoint areas of chemistry where recent progress has outpaced what is covered in any available textbooks, and then seek out and persuade experts in these fields to produce relatively concise but instructive intro ductions to their fields. These should serve the needs of one-semester or one-quarter graduate courses in chemistry and biochemistry. In some cases, the availability of texts in active research areas should help stimulate the creation of new courses. Charles R. Cantor v Preface to the Second Edition Since the publication of the previous edition in 1994, X-ray crystallography of proteins has advanced by improvements in existing techniques and by addition of new techniques.