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Electrochemical Detection In Hplc


Electrochemical Detection In Hplc
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Electrochemical Detection In Hplc


Electrochemical Detection In Hplc
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Author : Robert J Flanagan
language : en
Publisher: Royal Society of Chemistry
Release Date : 2007-10-31

Electrochemical Detection In Hplc written by Robert J Flanagan and has been published by Royal Society of Chemistry this book supported file pdf, txt, epub, kindle and other format this book has been release on 2007-10-31 with Science categories.


Electrochemical Detection in HPLC: Analysis of Drugs and Poisons is the first monograph devoted to the application of this mode of analysis to the assay of exogenous compounds such as drugs in biological fluids and associated areas. The introductory chapters provide information on basic electrochemistry and HPLC-ED, and on trouble-shooting. The specialized area of thiol analysis is also discussed in detail. Salient practical details of published applications of the technique in analytical toxicology and related areas are provided in a standard format. Alternative techniques are suggested throughout. The emphasis is on the analysis of exogenous compounds, although catecholamines and other endogenous species are discussed in so far as they may be used as drugs. The practical nature of this book will make it useful to professionals working in the field. It will also be of benefit to analysts wishing to use HPLC-ED in the analysis of biological samples for analytes not specifically covered in the volume.



Coulometric Electrode Array Detectors For Hplc


Coulometric Electrode Array Detectors For Hplc
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Author : Ian N. Acworth
language : en
Publisher: VSP
Release Date : 1997

Coulometric Electrode Array Detectors For Hplc written by Ian N. Acworth and has been published by VSP this book supported file pdf, txt, epub, kindle and other format this book has been release on 1997 with Science categories.


This sixth volume in the book series Progress in HPLC-HPCE examines the enhancement of high- performance liquid chromatography through the development of an advanced mode of electrochemical detection (ECD) --- the coulometric array detection --- from its initial, yet problematic, amperometric (thin-layer) design to the highly sensitive, selective and stable coulometric (flow-through) design. Unlike amperometric electrodes, the coulometric electrode is 100% efficient and measures signals from all of the analyte passing through it, which leads to improved sensitivity as well as unique selectivity. The coulometric electrode array offers the resolution of the photodiode array with the extreme sensitivity of an electrochemical detector.



Electrochemical Detection In Medicine And Chemistry


Electrochemical Detection In Medicine And Chemistry
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Author : H. Parvez
language : en
Publisher: VSP
Release Date : 1987-12

Electrochemical Detection In Medicine And Chemistry written by H. Parvez and has been published by VSP this book supported file pdf, txt, epub, kindle and other format this book has been release on 1987-12 with Science categories.




Coulometric Electrode Array Detectors For Hplc


Coulometric Electrode Array Detectors For Hplc
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Author : I.H. Acworth
language : en
Publisher: CRC Press
Release Date : 2024-01-26

Coulometric Electrode Array Detectors For Hplc written by I.H. Acworth and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2024-01-26 with Science categories.


This sixth volume in the book series Progress in HPLC-HPCE examines the enhancement of high- performance liquid chromatography through the development of an advanced mode of electrochemical detection (ECD) --- the coulometric array detection --- from its initial, yet problematic, amperometric (thin-layer) design to the highly sensitive, selective and stable coulometric (flow-through) design. Unlike amperometric electrodes, the coulometric electrode is 100% efficient and measures signals from all of the analyte passing through it, which leads to improved sensitivity as well as unique selectivity. The coulometric electrode array offers the resolution of the photodiode array with the extreme sensitivity of an electrochemical detector.



A Practical Guide To Hplc Detection


A Practical Guide To Hplc Detection
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Author : Donald Parriott
language : en
Publisher: Academic Press
Release Date : 2012-12-02

A Practical Guide To Hplc Detection written by Donald Parriott and has been published by Academic Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-02 with Science categories.


This guide for the practicing chromatographer who wants a ready source of information on HPLC detection explores and compares existing detection systems and detectors, outlines the common problems associated with a given detector, and offers proven approaches to avoiding such problems. - Addresses the practical aspects of HPLC detection, including: basic theory, when a particular type of detector can be used, how detectors from various manufacturers differ, common problems of detectors and ways to avoid them - Presents an overview of today's most common techniques - Discusses the advantages and disadvantages of HPLC, dispelling common misconceptions



Pulsed Electrochemical Detection In High Performance Liquid Chromatography


Pulsed Electrochemical Detection In High Performance Liquid Chromatography
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Author : William R. LaCourse
language : en
Publisher: Wiley-Interscience
Release Date : 1997-08-18

Pulsed Electrochemical Detection In High Performance Liquid Chromatography written by William R. LaCourse and has been published by Wiley-Interscience this book supported file pdf, txt, epub, kindle and other format this book has been release on 1997-08-18 with Science categories.


A reliable, comprehensive, relevant view of HPLC and its applications The development of HPLC-PED represents the successful marriage of two powerful analytical technologies and has resulted in the best technique for sensitive and direct detection of biological compounds with poor optical detection properties. PED has been used extensively for the determination of carbohydrates and other polar aliphatic compounds, and as a result, numerous methods have been developed to enable the analysis of a wide variety of samples. Over the years, many articles, anecdotal information, and misinformation have permeated the scientific community, with the possible consequence of confusion or uncertainty with regard to PED on the part of the analyst. Pulsed Electrochemical Detection in High-Performance Liquid Chromatography presents a reliable, comprehensive, and relevant review of HPLC-PED and its applications. The book is divided into three major parts: background material necessary for a more thorough understanding of the principles and relevance of PED; an in-depth discussion of PED using voltammetry and other electroanalytical techniques and presenting the advantages, applicability, and optimization of all existing PED waveforms; and practical aspects of HPLC-PED, including a summary of the major applications and a look at future developments in the technique. Appendices include a pulsed voltammetry (PV) program specifically written to optimize pulsed amperometric detection (PAD) waveforms and all the known applications, categorized and listed in tabular form. For analytical chemists; biochemists; carbohydrate chemists; biotechnologists; undergraduate, graduate, and postdoctoral students; and lab technicians working in a range of areas including the pharmaceutical, medical, and food and beverage industries, this eminently readable guide is the first reliable book-length treatment of how to use PED coupled with HPLC.



Hplc Ec High Pressure Liquid Chromatography Electrochemical Detection Studies Of Selected Explosive Components Nitroanilines And Nitrophenols With Dual Electrode Electrochemical Detection


Hplc Ec High Pressure Liquid Chromatography Electrochemical Detection Studies Of Selected Explosive Components Nitroanilines And Nitrophenols With Dual Electrode Electrochemical Detection
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Author : D. L. Manning
language : en
Publisher:
Release Date : 1985

Hplc Ec High Pressure Liquid Chromatography Electrochemical Detection Studies Of Selected Explosive Components Nitroanilines And Nitrophenols With Dual Electrode Electrochemical Detection written by D. L. Manning and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1985 with categories.


The dual electrode electrochemical detector has greatly enhanced high pressure liquid chromatography/electrochemical detection (HPLC/EC) capability. The most fruitful mode of operation is in the dual parallel electrode configuration. The ability to assess peak purity in real samples is very beneficial. Simultaneous recording of cathodic and anodic chromatograms to look possible impurities and munition decomposition products is an added technique to ascertain sample purity. The extent of electrode crosstalk can be minimized by repeating the experiment with the Au/Hg electrode OFF. In view of the low collection efficiencies encountered, the dual series mode of operation, at present, is of limited practical value for these types of electroactive substances.



Amino Acid Analysis Protocols


Amino Acid Analysis Protocols
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Author : Catherine Cooper
language : en
Publisher: Springer Science & Business Media
Release Date : 2008-02-05

Amino Acid Analysis Protocols written by Catherine Cooper and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2008-02-05 with Science categories.


A collection of classic and cutting-edge techniques of high utility in answering specific biological questions about amino acids. Common methods include those based on HPLC or gas chromatography separation and analysis after precolumn derivatization. New techniques based on capillary electrophoresis separation, high-performance anion exchange chromatography, and mass spectrometry are also presented. Each method is described in step-by-step detail to ensure successful experimental results and emphasizes sample preparation, particularly the collection and storage of bodily fluids. Up-to-date and highly practical, Amino Acid Analysis Protocols offers analytical and clinical chemists, as well as a broad range of biological and biomedical investigators, a rich compendium of laboratory tools for the productive analysis of both common and uncommon amino acids.



Liquid Chromatography In Environmental Analysis


Liquid Chromatography In Environmental Analysis
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Author : James F. Lawrence
language : en
Publisher: Springer Science & Business Media
Release Date : 2013-11-11

Liquid Chromatography In Environmental Analysis written by James F. Lawrence and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-11-11 with Science categories.


Provides an engaging account of how genetic abnormalities, neurobiology and neuropsychology work in concert to manifest cognitive-behavioral dysfunction. The authors have woven the various molecular genetic, genomic, neurophysiological and neurobehavioral threads together into a cohesive fabric of human genes, brain, and behavior. The first section provides and introduction to neurobehavioral disorders and their phenotypes in order to investigate the pathway between genes and behavior. The second section covers autosomal disorders that produce neurobehavioral dysfunction including neurofibromatosis, Prader-Willi syndrome, and tuberous sclerosis among others. The final section considers X-linked disorders in which syndromal and nonsyndromal forms of XLMR are present. It includes the first comprehensive account of the genotype and phenotype in FRAXE, the other fragile X mutation.



Supercritical Fluid Chromatography And Micro Hplc


Supercritical Fluid Chromatography And Micro Hplc
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Author : M. Yoshioka
language : en
Publisher: VSP
Release Date : 1989

Supercritical Fluid Chromatography And Micro Hplc written by M. Yoshioka and has been published by VSP this book supported file pdf, txt, epub, kindle and other format this book has been release on 1989 with Science categories.


First published in 1988. Routledge is an imprint of Taylor & Francis, an informa company.