Evolved Gas Analysis
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Evolved Gas Analysis
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Author : Nicolas Fedelich
language : en
Publisher: Carl Hanser Verlag GmbH Co KG
Release Date : 2019-10-07
Evolved Gas Analysis written by Nicolas Fedelich and has been published by Carl Hanser Verlag GmbH Co KG this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019-10-07 with Technology & Engineering categories.
volved gas analysis (EGA) describes analysis of gases or volatile components evolved from a sample undergoing thermal analysis. It is often used in direct combination with chemical analysis techniques such as gas chromatography, IR spectroscopy, or mass spectrometry, and/or with thermogravimetric analysis (TGA), i.e. measuring the change in weight of the sample under controlled conditions. This book focuses on these so-called "hyphenated techniques" (EGA-TGA, TGA-GC/MS, etc.), which allow a great deal of chemical information about a sample to be revealed quickly and conveniently. The methods are highly applicable to polymer/plastics samples, but also to other materials including pharmaceuticals, biomass, and various organic and inorganic compounds. Examples of applications related to all these material types are provided in this book. This book provides practical help to anyone interested in the practical aspects of EGA-TGA, including those working in testing laboratories and their clients.
Introduction To Thermal Analysis
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Author : M.E. Brown
language : en
Publisher: Springer Science & Business Media
Release Date : 2006-01-10
Introduction To Thermal Analysis written by M.E. Brown and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2006-01-10 with Technology & Engineering categories.
to Thermal Analysis Techniques and Applications Edited by Michael E. Brown Chemistry Department, Rhodes University, Grahamstown, South Africa KLUWER ACADEMIC PUBLISHERS NEW YORK, BOSTON, DORDRECHT, LONDON, MOSCOW eBook ISBN: 0-306-48404-8 Print ISBN: 1-4020-0472-9 ©2004 Kluwer Academic Publishers New York, Boston, Dordrecht, London, Moscow Print ©2001 Kluwer Academic Publishers Dordrecht All rights reserved No part of this eBook may be reproduced or transmitted in any form or by any means, electronic, mechanical, recording, or otherwise, without written consent from the Publisher Created in the United States of America Visit Kluwer Online at: http://kluweronline. com and Kluwer's eBookstore at: http://ebooks. kluweronline. com CONTENTS Preface to the First Edition, Chapman & Hall, London, 1988 ix About the First Edition of this Book x Preface to the Second Edition xi 1. INTRODUCTION 1. 1 Definition and History 1 1. 2 Thermal Analysis Instruments 4 References 11 2. THERMAL EVENTS 2. 1 Introduction 13 2. 2 The Solid State 13 2. 3 Reactions of Solids 14 2. 4 Decomposition of Solids 15 2. 5 Reaction with the Surrounding Atmosphere 16 2. 6 Solid-Solid Interactions 16 References 17 3. THERMOGRAVIMETRY (TG) Introduction 3. 1 19 3. 2 The Balance 19 3. 3 Heating the Sample 21 3. 4 The Atmosphere 24 3. 5 The Sample 26 3. 6 Temperature Measurement 26 3. 7 Temperature Control 28 Sample Controlled Thermal Analysis (SCTA) 29 3. 8 3. 9 Calibration 36 3. 10 Presentation of TG Data 37 3.
Bureau Of Mines Apparatus For Thermal Analysis
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Author : Donald R. Johnson
language : en
Publisher:
Release Date : 1970
Bureau Of Mines Apparatus For Thermal Analysis written by Donald R. Johnson and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1970 with Gases categories.
Principles And Applications Of Thermal Analysis
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Author : Paul Gabbott
language : en
Publisher: John Wiley & Sons
Release Date : 2008-04-30
Principles And Applications Of Thermal Analysis written by Paul Gabbott and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2008-04-30 with Science categories.
Thermal Analysis techniques are used in a wide range of disciplines, from pharmacy and foods to polymer science, materials and glasses; in fact any field where changes in sample behaviour are observed under controlled heating or controlled cooling conditions. The wide range of measurements possible provide fundamental information on the material properties of the system under test, so thermal analysis has found increasing use both in basic characterisation of materials and in a wide range of applications in research, development and quality control in industry and academia. Principles and Applications of Thermal Analysis is written by manufacturers and experienced users of thermal techniques. It provides the reader with sound practical instruction on how to use the techniques and gives an up to date account of the principle industrial applications. By covering basic thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) including the new approach of Fast Scanning DSC, together with dynamic mechanical analysis (DMA /TMA) methods, then developing the discussion to encompass industrial applications, the book serves as an ideal introduction to the technology for new users. With a strong focus on practical issues and relating the measurements to the physical behaviour of the materials under test, the book will also serve as an important reference for experienced analysts.
Thermal Analysis Of Pharmaceuticals
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Author : Duncan Q.M. Craig
language : en
Publisher: CRC Press
Release Date : 2006-12-21
Thermal Analysis Of Pharmaceuticals written by Duncan Q.M. Craig and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2006-12-21 with Medical categories.
As a result of the Process Analytical Technologies (PAT) initiative launched by the U.S. Food and Drug Administration (FDA), analytical development is receiving more attention within the pharmaceutical industry. Illustrating the importance of analytical methodologies, Thermal Analysis of Pharmaceuticals presents reliable and versatile charac
Pyrolysis Gc Ms Data Book Of Synthetic Polymers
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Author : Shin Tsuge
language : en
Publisher: Elsevier
Release Date : 2011-08-02
Pyrolysis Gc Ms Data Book Of Synthetic Polymers written by Shin Tsuge and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2011-08-02 with Science categories.
In this data book, both conventional Py-GC/MS where thermal energy alone is used to cause fragmentation of given polymeric materials and reactive Py-GC/MS in the presence of organic alkaline for condensation polymers are compiled. Before going into detailed presentation of the data, however, acquiring a firm grip on the proper understanding about the situation of Py-GC/MS would promote better utilization of the following pyrolysis data for various polymers samples. This book incorporates recent technological advances in analytical pyrolysis methods especially useful for the characterization of 163 typical synthetic polymers. The book briefly reviews the instrumentation available in advanced analytical pyrolysis, and offers guidance to perform effectually this technique combining with gas chromatography and mass spectrometry. Main contents are comprehensive sample pyrograms, thermograms, identification tables, and representative mass spectra (MS) of pyrolyzates for synthetic polymers. This edition also highlights thermally-assisted hydrolysis and methylation technique effectively applied to 33 basic condensation polymers. Coverage of Py-GC/MS data of conventional pyrograms and thermograms of basic 163 kinds of synthetic polymers together with MS and retention index data for pyrolyzates, enabling a quick identification Additional coverage of the pyrograms and their related data for 33 basic condensation polymers obtained by the thermally-assisted hydrolysis and methylation technique All compiled data measured under the same experimental conditions for pyrolysis, gas chromatography and mass spectrometry to facilitate peak identification Surveyable instant information on two facing pages dedicated to the whole data of a given polymer sample
Polymer Reference Book
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Author : Thomas Roy Crompton
language : en
Publisher: iSmithers Rapra Publishing
Release Date : 2006
Polymer Reference Book written by Thomas Roy Crompton and has been published by iSmithers Rapra Publishing this book supported file pdf, txt, epub, kindle and other format this book has been release on 2006 with Science categories.
The aim of this book is to familiarise the reader with all aspects of the techniques used in the examination of polymers, covering chemical, physiochemical and purely physical methods of examination. The types of techniques available to the polymer chemist and technician are described, and their capabilities, limitations and applications are discussed. The book is intended, for all staff who are concerned with instrumentation and methodology in the polymer laboratory including laboratory designers, engineers and chemists, and also those concerned with the implementation of analytical specifications and process control limits.
A Mass Spectrometer Evolved Gas Analysis Experiment For In Situ Analysis Of Cometary Dust Volatiles
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Author : Brian Jay Anderson
language : en
Publisher:
Release Date : 1987
A Mass Spectrometer Evolved Gas Analysis Experiment For In Situ Analysis Of Cometary Dust Volatiles written by Brian Jay Anderson and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1987 with categories.
Methods Of Gas Analysis
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Author : Walther Hempel
language : en
Publisher:
Release Date : 1902
Methods Of Gas Analysis written by Walther Hempel and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1902 with Gas research categories.
Gas Effluent Analysis
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Author : William Lodding
language : en
Publisher:
Release Date : 1967
Gas Effluent Analysis written by William Lodding and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1967 with Science categories.