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Experimental Pulse Nmr


Experimental Pulse Nmr
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Experimental Pulse Nmr


Experimental Pulse Nmr
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Author : Eiichi Fukushima
language : en
Publisher: CRC Press
Release Date : 2018-03-08

Experimental Pulse Nmr written by Eiichi Fukushima and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2018-03-08 with Science categories.


This book is about pulse nuclear magnetic resonance (NMR), with its techniques, the information to be obtained, and practical advice on performing experiments. The emphasis is on the motivation and physical ideas underlying NMR experiments and the actual techniques, including the hardware used. The level is generally suitable for those to whom pulse NMR is a new technique, be they students in chemistry or physics on the one hand and research workers in biology, geology, or agriculture, on the other. The book can be used for a senior or first year graduate course where it could supplement the standard NMR texts.



200 And More Nmr Experiments


200 And More Nmr Experiments
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Author : Stefan Berger
language : en
Publisher: John Wiley & Sons
Release Date : 2004-07-02

200 And More Nmr Experiments written by Stefan Berger and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2004-07-02 with Science categories.


This work-book will guide you safely, in step-by-step descriptions, through every detail of the NMR experiments within, beginning with 1D routine experiments and ending with a series of advanced 3D experiments on a protein: ? Which experiment can best yield the desired information? ? How must the chosen experiment be performed? ? How does one read the required information from the spectrum? ? How does this particular pulse sequence work? ? Which other experiments give similar information? This third edition of the book, following its two highly successful predecessors, has been revised and expanded to 206 experiments. They are organized in 15 chapters, covering test procedures and routine spectra, variable temperature measurements, the use of auxiliary reagents, 1D multipulse experiments, spectra of heteronuclides, and the application of selective pulses. The second and third dimensions are introduced using pulsed field gradients, and experiments on solid state materials are described. A key part describes 3D experiments on the protein ubiquitin with 76 amino acids. What is new in this third edition? 1. 24 new experiments have been inserted into the 14 chapters that were in the 2nd edition, e.g., alpha/beta-SELINCOR-TOCSY, WET, DOSY, ct-COSY, HMSC, HSQC with adiabatic pulses, HETLOC. J-resolved HMBC, (1,1)- and (1,n)-ADEQUATE, STD, REDOR, and HR-MAS. 2. 20 new protein NMR experiments have been specially devised and are collected in the newly added Chapter 15, ProteinNMR, for which one needs a special model sample: fully 13C- and 15N-labeled human ubiquitin. Techniques used include the constant time principle, the PEP method, filters, gradient selection, and the echo/anti-echo procedure. The guide has been written by experts in this field, following the principle of learning by doing: all the experiments have been specially performed for this book, exactly as described and shown in the spectra that are reproduced. Being a reference source and work-book for the NMR laboratory as well as a textbook, it is a must for every scientist working with NMR, as well as for students preparing for their laboratory courses



50 And More Essential Nmr Experiments


50 And More Essential Nmr Experiments
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Author : Matthias Findeisen
language : en
Publisher: John Wiley & Sons
Release Date : 2013-07-30

50 And More Essential Nmr Experiments written by Matthias Findeisen and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-07-30 with Science categories.


This book is the perfect link for learning how to perform the experiments after only having studied theory. In eight chapters more than 50 essential NMR experiments are described in detail. Special focus is put on the organic set of NMR spectra (1H, 13C-APT, COSY, NOESY, HSQC and HMBC). Different chapters deal with advanced organic NMR, selective methods, heteronuclear NMR, relaxation and diffusion measurements, organic applications and maintenance. Every experiment has a section providing the reader with the purpose and scope of the specific experiment. Every experiment is concluded with the spectrum as it is obtained under the conditions described. Questions and comments enable the reader to check their understanding. The authors are very experienced and the whole book is in full color, which enhances the reading experience and makes the spectra and other figures easier to understand. This book is strongly recommended for all students and researchers who are involved in the structural elucidation of chemical compounds both in practical education and in pursuing research, in particular if they handle an NMR spectrometer.



Pulse And Fourier Transform Nmr


Pulse And Fourier Transform Nmr
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Author : Thomas C. Farrar
language : en
Publisher: Elsevier
Release Date : 2012-12-02

Pulse And Fourier Transform Nmr written by Thomas C. Farrar and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-02 with Science categories.


Pulse and Fourier Transform NMR: Introduction to Theory and Methods presents the different types of pulse experiments that are commonly used and provides the theoretical background necessary for understanding these techniques. This book evaluates the practical application of pulse methods and the necessary instrumentation. Organized into seven chapters, this book begins with an overview of the NMR fundamentals and the basic pulse methods. This text then summarizes the important features of pulse spectrometers. Other chapters consider the rationale, the advantages, and the limitations of Fourier transform NMR methods. This book discusses as well how the idea of the rotating frame can be utilized to understand certain experiments that extend the range of application of pulse methods. The final chapter deals with a few significant special uses of pulse techniques. This book is a valuable resource for chemists and readers who are familiar with high resolution NMR but with no background in pulse methods.



Multiple Pulse Nmr Experiments


Multiple Pulse Nmr Experiments
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Author : Lee Michael Huber
language : en
Publisher:
Release Date : 1968

Multiple Pulse Nmr Experiments written by Lee Michael Huber and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1968 with categories.




100 And More Basic Nmr Experiments


100 And More Basic Nmr Experiments
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Author : Siegmar Braun
language : en
Publisher: Wiley-VCH
Release Date : 1996-01-25

100 And More Basic Nmr Experiments written by Siegmar Braun and has been published by Wiley-VCH this book supported file pdf, txt, epub, kindle and other format this book has been release on 1996-01-25 with Medical categories.


How do the pulse sequences of modern NMR work? Which experiment conveys the desired information? How can the maximal amount of information be retrieved from measured spectra? Have you ever been confronted with questions like these? Get the answers and explore the full productivity of your NMR equipment! This book is a reliable guide through the maze of modern NMR tools. Written by leading experts, it describes more than a hundred NMR experiments including selective pulses, field gradients and the second and third dimension. Being textbook as well as reference book for the laboratory, this book is a must for every scientist working with NMR as well as for students preparing for their lab courses.



Fast Nmr Data Acquisition


Fast Nmr Data Acquisition
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Author : Mehdi Mobli
language : en
Publisher: Royal Society of Chemistry
Release Date : 2017-05-23

Fast Nmr Data Acquisition written by Mehdi Mobli and has been published by Royal Society of Chemistry this book supported file pdf, txt, epub, kindle and other format this book has been release on 2017-05-23 with Science categories.


Providing a definitive reference source on novel methods in NMR acquisition and processing, this book will highlight similarities and differences between emerging approaches and focus on identifying which methods are best suited for different applications. The highly qualified editors have conducted extensive research into the fundamentals of fast methods of data acquisition in NMR, including applications of non-Fourier methods of spectrum analysis. With contributions from additional distinguished experts in allied fields, clear explanations are provided on methods that speed up NMR experiments using different ways to manipulate the nuclei in the sample, modern methods for estimating the spectrum from the time domain response recorded during an NMR experiment, and finally how the data is sampled. Starting with a historical overview of Fourier Transformation and its role in modern NMR spectroscopy, this volume will clarify and demystify this important emerging field for spectroscopists and analytical chemists in industry and academia.



150 And More Basic Nmr Experiments


150 And More Basic Nmr Experiments
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Author : Siegmar Braun
language : en
Publisher: Wiley-VCH
Release Date : 1998-09-10

150 And More Basic Nmr Experiments written by Siegmar Braun and has been published by Wiley-VCH this book supported file pdf, txt, epub, kindle and other format this book has been release on 1998-09-10 with Mathematics categories.


NMR is one of the most widely used analytical techniques in chemistry. This book gives a problem-oriented introduction to modern applications in a "how-to" format.



Nmr Spectroscopy Data Acquisition


Nmr Spectroscopy Data Acquisition
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Author : Christian Schorn
language : en
Publisher: John Wiley & Sons
Release Date : 2001

Nmr Spectroscopy Data Acquisition written by Christian Schorn and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2001 with Science categories.


The key to correct structure analysis. This volume of the successful "Spectroscopic Techniques" series familiarizes newcomers with the basic data acquisition procedures, modular pulse sequence units and complete sequences in NMR spectroscopy. It applies the numerous possibilities of Bruker's simulation program NMR-SIM to provide a guided introduction to the world of pulse sequences. The effectiveness of particular NMR experiments is demonstrated by the section "Check Its" and that of data processing by the accompanying CD-ROM with the Bruker processing software 1D and 2D WIN-NMR. This interactive approach to simulate spectra based on a reduced spin system and the processing of the accomplished NMR raw data is closely related to everyday work at the spectrometer. In this way, the author encourages beginners to use high resolution NMR, and also experts on NMR spectroscopy to evaluate new experiments using the easy-manageable simulation program.



Nmr Primer


Nmr Primer
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Author : Steven M. Pascal
language : en
Publisher: IM Publications
Release Date : 2008

Nmr Primer written by Steven M. Pascal and has been published by IM Publications this book supported file pdf, txt, epub, kindle and other format this book has been release on 2008 with Magnetic resonance categories.


"This book has one aim: to explain the key two-dimensional protein NMR experiment, the 1H,15N-HSQC, along with variants and extensions, in a generally accessible manner. Vector diagrams of one-, two- and three-dimensional pulse sequences are provided, along with accompanying animated versions. The animations allow the evolution of net magnetisation during the course of the experiments to be visualised and directly compared with the corresponding spin operator terms. First, a brief introduction to spins, populations, the NMR experiment and relaxation is provided. Evolution due to J-coupling is next described and used to explain magnetisation transfer in the HSQC experiment and several variants. The extraction of structural, sequential and dynamic information is then illustrated via various extensions of the HSQC. Extensive footnotes and appendices introduce several more advanced concepts, such as sensitivity enhancement and the TROSY effect."--Publisher's description.