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Fast 2d Solution State Nmr


Fast 2d Solution State Nmr
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Fast 2d Solution State Nmr


Fast 2d Solution State Nmr
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Author : Jean-Nicolas Dumez
language : en
Publisher: Royal Society of Chemistry
Release Date : 2023-05-17

Fast 2d Solution State Nmr written by Jean-Nicolas Dumez and has been published by Royal Society of Chemistry this book supported file pdf, txt, epub, kindle and other format this book has been release on 2023-05-17 with Science categories.


Written by active investigators in the field, this book describes state-of-the-art methods that can accelerate the acquisition of 2D NMR spectra in solution-state NMR. The acquisition of fast multi-dimensional NMR data has motivated numerous ground-breaking developments in NMR pulse sequences and associated data processing methods. These in turn have revolutionized the way 2D NMR acquisitions are performed, at the same time broadening the scope of applications of 2D NMR. The first part of the book provides an in-depth description of the concepts and implementation of major fast 2D NMR methods. The second part follows with illustrations of how such methods can be used in applications that require the acquisition of fast 2D NMR spectra, from reaction monitoring to hyperpolarization, including applications to a broad variety of samples and experimental conditions. Appealing to readers from both the methodology and applications communities, this title will fill a gap in the market for a book focused on small molecule NMR, and researchers from both academia and industry will find a rich plethora of knowledge.



Fast 2d Solution State Nmr


Fast 2d Solution State Nmr
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Author : Dr Jean-Nicolas Dumez
language : en
Publisher: Royal Society of Chemistry
Release Date : 2023-05-17

Fast 2d Solution State Nmr written by Dr Jean-Nicolas Dumez and has been published by Royal Society of Chemistry this book supported file pdf, txt, epub, kindle and other format this book has been release on 2023-05-17 with Science categories.


Written by active investigators in the field, this book describes state-of-the-art methods that can accelerate the acquisition of 2D NMR spectra in solution-state NMR. The acquisition of fast multi-dimensional NMR data has motivated numerous ground-breaking developments in NMR pulse sequences and associated data processing methods. These in turn have revolutionized the way 2D NMR acquisitions are performed, at the same time broadening the scope of applications of 2D NMR. The first part of the book provides an in-depth description of the concepts and implementation of major fast 2D NMR methods. The second part follows with illustrations of how such methods can be used in applications that require the acquisition of fast 2D NMR spectra, from reaction monitoring to hyperpolarization, including applications to a broad variety of samples and experimental conditions. Appealing to readers from both the methodology and applications communities, this title will fill a gap in the market for a book focused on small molecule NMR, and researchers from both academia and industry will find a rich plethora of knowledge.



Optimising Nmr Spectroscopy Through Method And Software Development


Optimising Nmr Spectroscopy Through Method And Software Development
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Author : Jonathan Yong
language : en
Publisher: Springer Nature
Release Date : 2024-01-09

Optimising Nmr Spectroscopy Through Method And Software Development written by Jonathan Yong and has been published by Springer Nature this book supported file pdf, txt, epub, kindle and other format this book has been release on 2024-01-09 with Science categories.


This book provides a comprehensive overview of Nuclear Magnetic Resonance (NMR) theory, its applications, and advanced techniques to improve the quality and speed of NMR data acquisition. In this book, the author expands his outstanding Ph.D. thesis and provides a valuable resource for researchers, professionals, and students in the field of NMR spectroscopy. The book covers quantum mechanics basics, and topics like density operators, pulse sequences, 1D pulse acquisition, INEPT (Insensitive nuclei enhancement by polarization transfer), product operators, and 2D NMR principles. It also explores innovative experiments like States HSQC (Heteronuclear Single Quantum Coherence) and echo-antiecho HSQC with gradients. In the subsequent chapters, the author discusses Pure Shift NMR, including PSYCHE (Pure Shift Yielded by Chirp Excitation) and its optimizations, such as waveform parameterization and time-reversal methods. The 'Discrete PSYCHE' approach and Ultrafast PSYCHE-iDOSY (Diffusion-ordered spectroscopy) are also highlighted. This book presents the POISE (Parameter Optimisation by Iterative Spectral Evaluation) software for real-time NMR experiment optimization, including pulse width calibration and Ernst angle optimization, and demonstrates applications across various NMR experiments. Lastly, the book examines accelerated 2D NMR data collection and the NOAH (NMR by Ordered Acquisition using 1H detection) supersequences, emphasizing automated pulse program creation using GENESIS (GENEration of Supersequences In Silico). Covered NMR experiments include 13C sensitivity-enhanced HSQC, 15N HMQC (Heteronuclear Multiple Quantum Coherence), dual HSQC, HSQC-TOCSY (Total Correlation Spectroscopy), HMBC (Heteronuclear Multiple Bond Correlation), and ADEQUATE (Adequate Sensitivity Double-Quantum Spectroscopy).



Practical Nmr For Oil And Gas Exploration


Practical Nmr For Oil And Gas Exploration
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Author : Lizhi Xiao
language : en
Publisher: Royal Society of Chemistry
Release Date : 2023-08-14

Practical Nmr For Oil And Gas Exploration written by Lizhi Xiao and has been published by Royal Society of Chemistry this book supported file pdf, txt, epub, kindle and other format this book has been release on 2023-08-14 with Science categories.


Describing comprehensively the development and applications of NMR to oil and gas exploration, this book will bring the literature up to date as it has developed very quickly in the last two decades. Outlining new methodologies, it will provide a thorough and comprehensive document enabling a better understanding of the basics of NMR physics, petrophysics, downhole tools and data interpretation. Written by an author with more than 30 years’ experience in this hot and important topic, this book is designed to meet the needs of the community and encourage applications in low field NMR.



Annual Reports On Nmr Spectroscopy


Annual Reports On Nmr Spectroscopy
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Author :
language : en
Publisher: Elsevier
Release Date : 2024-07-11

Annual Reports On Nmr Spectroscopy written by and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2024-07-11 with Science categories.


Annual Reports on NMR Spectroscopy, Volume 111 presents the latest release in a series that has established itself as a premier resource for both specialists and non-specialists interested in new techniques and applications pertaining to NMR spectroscopy. Chapters in this new release include Electrophoretic NMR, Traceability and uncertainty in NMR measurements, Quantitative NMR Spectroscopy, Advances in Non-Uniform Sampling NMR, NMR spectroscopy of natural and synthetic fibers, Characterization of transition alkane complexes, and Recent applications of low field NMR to membrane science. - Serves as the premier resource for learning new techniques and applications in NMR spectroscopy - Provides a key reference for chemists and physicists using NMR spectroscopy to study the structure and dynamics of molecules - Covers all aspects of molecular science, including MRI (Magnetic Resonance Imaging)



Physical Principles Of Chirality In Nmr


Physical Principles Of Chirality In Nmr
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Author : Piotr Garbacz
language : en
Publisher: Royal Society of Chemistry
Release Date : 2024-09-20

Physical Principles Of Chirality In Nmr written by Piotr Garbacz and has been published by Royal Society of Chemistry this book supported file pdf, txt, epub, kindle and other format this book has been release on 2024-09-20 with Science categories.


How can we study one of the most elusive molecular properties, chirality, using nuclear interactions with the magnetic field that are apparently insensitive to handedness? This book answers this question from the physicochemical point of view by providing a clear, coherent, and comprehensive review of methods used in NMR studies of chirality. Presented arguments based on fundamental physical and chemical laws and in-depth descriptions of new methods utilizing purely physical interactions are mainly addressed to spectroscopists in both academia and industry. The introductory chapters provide the reader with the basics of NMR spectroscopy as a tool for the study of chiral compounds, and those more interested in the methods of chiral discrimination will benefit from the brief description of their common points and reasons why some of them may or may not work. In the following chapters, the book shows rapid progress in a newly emerging field of chirality-sensitive NMR, in particular, a search for effects that give direct information about the absolute configuration of a molecule.



Nmr Of Metal Organic Frameworks And Covalent Organic Frameworks


Nmr Of Metal Organic Frameworks And Covalent Organic Frameworks
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Author : Wei Wang
language : en
Publisher: Royal Society of Chemistry
Release Date : 2024-12-18

Nmr Of Metal Organic Frameworks And Covalent Organic Frameworks written by Wei Wang and has been published by Royal Society of Chemistry this book supported file pdf, txt, epub, kindle and other format this book has been release on 2024-12-18 with Technology & Engineering categories.


As new porous materials, metal organic frameworks (MOFs) and covalent organic frameworks (COFs) have been receiving an abundance of research interest in recent years. This book is the first comprehensive title to cover solid state NMR, 129Xe NMR and diffusion NMR methods that have been applied to solve the key scientific issues in the MOFs and COFs research like structural determination, examination of the local structures and host-guest interactions. Structural Information is crucial not only to understand the synthetic mechanisms but also to establish the structure-activity relationship of MOFs and COFs. In comparison to single-crystal X-ray diffraction and high-resolution electron microscopy, solid state NMR provides determinative or complementary information regarding MOFs and COFs. This book will benefit researchers who are interested in structural identification but have little expertise in NMR. It bridges a gap in knowledge and provides a unique reference work in this field of research.



Nmr Methods For Characterization Of Synthetic And Natural Polymers


Nmr Methods For Characterization Of Synthetic And Natural Polymers
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Author : Rongchun Zhang
language : en
Publisher: Royal Society of Chemistry
Release Date : 2019-08-02

Nmr Methods For Characterization Of Synthetic And Natural Polymers written by Rongchun Zhang and has been published by Royal Society of Chemistry this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019-08-02 with Science categories.


Since the introduction of FT-NMR spectroscopy around five decades ago, NMR has achieved significant advances in hardware and methodologies, accompanied with the enhancement of spectral resolution and signal sensitivity. Rapid developments in the polymers field mean that accurate and quantitative characterization of polymer structures and dynamics is the keystone for precisely regulating and controlling the physical and chemical properties of the polymer. This book specifically focuses on NMR investigation of complex polymers for the polymer community as well as NMR spectroscopists, and will push the development of both fields. It covers the latest advances, for example high field DNP and ultrafast MAS methodologies, and show how these novel NMR methods characterize various synthetic and natural polymers.



Nuclear Magnetic Resonance


Nuclear Magnetic Resonance
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Author : Navin Khaneja
language : en
Publisher: Intechopen
Release Date : 2020

Nuclear Magnetic Resonance written by Navin Khaneja and has been published by Intechopen this book supported file pdf, txt, epub, kindle and other format this book has been release on 2020 with Science categories.


Nuclear magnetic resonance (NMR) has evolved as a versatile tool in chemistry and biology. This scientific technique is based on the detection of magnetic moments of atomic nuclei arising due to an intrinsic property called spin because of their precession in static magnetic fields. Nuclei are excited by radio frequency (RF) magnetic fields and subsequently their precession is observed by the voltage they induce on an induction coil as they precess. In this book, we present some of the most exciting developments in the field of NMR: for example, new developments in NMR instrumentation, new magnet technology, RF coil design, the design of novel NMR sensors, and new developments of methods in solution and solid-state NMR These range from new methods for the fast acquisition of 2D spectrum to NMR studies of molecular interactions in ionic solutions. Solid-state methods for the analysis of polyvinyl chloride and NMR studies of torsion angles in polypeptides are also included. The book will be a useful reference for practitioners in the field and at the same time will appeal to a broad audience interested in the general area of NMR.



Integrated Structural Biology


Integrated Structural Biology
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Author : Tatyana Polenova
language : en
Publisher: Royal Society of Chemistry
Release Date : 2023-12-08

Integrated Structural Biology written by Tatyana Polenova and has been published by Royal Society of Chemistry this book supported file pdf, txt, epub, kindle and other format this book has been release on 2023-12-08 with Science categories.


Modern research in biology increasingly relies on multiple techniques for describing structures and mechanisms. This book provides an overview of the contemporary integrated biology approaches for solving structures and understanding mechanisms of complex biological systems. It includes several methodology chapters discussing the current developments in the areas of cryo-electron microscopy (EM) and cryo-electron tomography (ET), computational biophysics, solution NMR spectroscopy, solid-state NMR spectroscopy and dynamic nuclear polarization (DNP), electron paramagnetic resonance (EPR), (photo-)chemically induced dynamic nuclear polarization (CIDNP), X-ray crystallography and small-angle X-ray and neutron scattering (SAXS/SANS). Several subsequent chapters demonstrate how these methods are used in synergy to address problems at the forefront of structural biology, with particular emphasis on examples where individual techniques are insufficient. Examples of biological systems include membrane proteins, viral protein assemblies, cytoskeleton protein assemblies, photosynthetic reaction centers, large enzyme complexes and whole cells. The book is targeted to both the current practitioners of structural biology and scientists who are interested in entering the fields of structural biology or biophysical chemistry.