Handbook Of Heterogeneous Catalytic Hydrogenation For Organic Synthesis
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Handbook Of Heterogeneous Catalytic Hydrogenation For Organic Synthesis
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Author : Shigeo Nishimura
language : en
Publisher: Wiley-Interscience
Release Date : 2001-04-17
Handbook Of Heterogeneous Catalytic Hydrogenation For Organic Synthesis written by Shigeo Nishimura and has been published by Wiley-Interscience this book supported file pdf, txt, epub, kindle and other format this book has been release on 2001-04-17 with Science categories.
A complete guide to the most important reduction method in organic synthesis The most comprehensive reference in the field, Handbook of Heterogeneous Catalytic Hydrogenation for Organic Synthesis provides synthetic chemists and chemical engineers in fine chemicals and pharmaceuticals with detailed experimental guidelines for heterogeneous catalytic hydrogenation. Organized by functional groups for ready reference and featuring detailed examples of hundreds of reactions, this handbook covers hydrogenations of alkenes, alkynes, aldehydes and ketones, nitriles, imines, nitro and nitroso compounds, carboxylic acids and esters, and aromatic and heterocyclic compounds. In addition, coverage includes the preparation of amines by reductive alkylation and the hydrogenolysis of a variety of compounds. Examples of hydrogenation of functional groups and reaction pathways are illustrated with numerous equations and schemes. Practitioners will appreciate the plenitude of experimental details given for most of the reactions selected, including amounts of reagents and catalysts, reaction temperatures, hydrogen pressures, and reaction times. They will also find helpful the more than one hundred tables included throughout the book detailing the effects of key factors governing rate and selectivity, such as compound structure, the nature of catalysts and supports, and the nature of solvents. Researchers will benefit from the introductory chapters covering an array of hydrogenation catalysts, including nickel, cobalt, copper, iron, platinum group metals, rhenium, and other oxide and sulfide catalysts, as well as reactors and reaction conditions.
Catalytic Hydrogenation In Organic Syntheses
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Author : Rylander
language : en
Publisher: Elsevier
Release Date : 2012-12-02
Catalytic Hydrogenation In Organic Syntheses written by Rylander and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-02 with Science categories.
Catalytic Hydrogenation in Organic Syntheses focuses on the process of catalytic hydrogenation in organic synthesis. This book gives the reader easy access to catalytic history, to show what can be done and how to do it. A variety of working generalities and common sense guides are given as aids in selecting catalytic metal, catalyst support, concentration of metal and catalyst, solvent, and reaction conditions. All manner of hydrogenation catalysts are considered and mechanisms of hydrogenation are presented at a level that is useful to the synthetic organic chemist. This volume is comprised of 15 chapters and begins with an overview of catalytic hydrogenation and heterogeneous hydrogenation catalysts, along with hydrogenation reactors and reaction conditions. The discussion then shifts to the hydrogenation of compounds such as acetylenes, olefins, aldehydes, ketones, nitriles, oximes, acids, esters, lactones, anhydrides, and nitro compounds as well as carbocyclic aromatics and heterocyclic compounds. The reader is also introduced to reductive alkylation, catalytic dehydrohalogenation, and hydrogenolysis of small rings. A chapter on miscellaneous hydrogenolyses concludes the book. This book will be of interest to organic chemists working in the field of catalytic hydrogenation.
Heterogeneous Catalysis In Organic Chemistry
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Author : Gerard V. Smith
language : en
Publisher: Academic Press
Release Date : 1999-06-30
Heterogeneous Catalysis In Organic Chemistry written by Gerard V. Smith and has been published by Academic Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 1999-06-30 with Science categories.
The features of this book which will be of special interest to academic organic chemists are the introduction (Chapter 1), which presents a short course on the concepts and language of heterogeneous catalysis, covers organic reaction mechanisms of hydrogenation (Chapter 2), hydrogenolysis (Chapter 4), and oxidation (Chapter 6), a presents problems and solutions specific for running heterogeneous catalytic organic reactions in solution. These materials can supplement advanced chemistry courses. Most synthetic organic chemists use a variety of "protecting groups" which they attach to functional groups (reactive groups of atoms) while some reaction is being conducted on another part of the molecule. These protecting groups prevent reactions of the functional groups during other reactions and are removed later by a heterogeneous catalytic method called hydrogenolysis. One unique feature of this book, not found in other books on catalysis, is an exhaustive chapter (Chapter 4) on hydrogenolysis, which is dredged from the recent synthetic literature published by modern organic chemists. Academic organic chemists should find this chapter extremely useful and may wish to adopt the book as a supplement for advanced organic chemistry courses designed for seniors and for graduate students. It will also be useful for professors and their research groups engaged in synthetic organic chemistry. Many academic organic chemists are not aware of recent advances in heterogeneous enantioselective catalysis (Chapter 3) or in selective low temperature, liquid phase heterogeneous catalytic oxidations by hydrogen peroxide (Chapter 6). These specialty topics are timely and may be new to academic organic chemists and can be used to supplement their advanced courses. Several features of this book will also be of special interest to industrial chemists who are unfamiliar with heterogeneous catalysis. Many good organic chemists are hire by industry. They synthesize a new compound using standard organic synthetic techniques but are informed by their supervisor that they must convert some of their synthetic steps into heterogeneous catalytic steps. They may not have been exposed to heterogeneous catalysis and have few places to turn. This book offers them a crash course in heterogeneous catalysis as well as many examples of reactions and conditions with which they can start their search. Those industrial organic chemists already familiar with heterogeneous catalysis will find this book useful as a reference to many examples in the recent literature. They will find recent surface science discoveries correlated with heterogeneous catalysis or organic reactions and mechanistic suggestions designed to stimulate innovative nontraditional thinking about organic reactions on surfaces. Written by organic chemists for organic chemists Introduces heterogeneous catalysis concepts and language Presents a comprehensive compilation of protecting group removal procedures Covers liquid-phase hydrogenations, hydrogenolysis, and oxidations Addresses heterogeneous methods for producing pure enantiomers of chiral products Examines the emerging field of heterogenized homogeneous catalysts Mixes practical applications with mechanistic interpretations
Heterogeneous Catalysis For The Synthetic Chemist
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Author : Robert L. Augustine
language : en
Publisher: CRC Press
Release Date : 2020-08-11
Heterogeneous Catalysis For The Synthetic Chemist written by Robert L. Augustine and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2020-08-11 with Science categories.
This work delineates the effect of different reaction variables on the outcome of heterogeneously catalyzed reactions, and explains how to optimize the product yield of specific compounds. Metal catalysis, simple and complex oxides, zeolites and clays are discussed, both as catalysts and as potential supports for catalytically active metals.
Heterogeneous Catalysis In Sustainable Synthesis
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Author : Bela Torok
language : en
Publisher: Elsevier
Release Date : 2021-09-17
Heterogeneous Catalysis In Sustainable Synthesis written by Bela Torok and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2021-09-17 with Science categories.
Heterogeneous Catalysis in Sustainable Synthesis is a practical guide to the use of solid catalysts in synthetic chemistry that focuses on environmentally benign applications. Collating essential information on solid catalysts into a single volume, it reveals how the efficient use of heterogeneous catalysts in synthetic chemistry can support sustainable applications. Beginning with a review of the fundamentals of heterogeneous catalytic synthesis, the book then explores the basic concepts of heterogeneous catalytic reactions from adsorption to catalyst poisons, the use of non-traditional activation methods, recommended solvents, the major types of both metal and non-metal solid catalysts, and applications of these catalysts in sustainable synthesis. Based on the extensive experience of its expert author, this book aims to encourage and support synthetic chemists in using solid catalysts in their own work, while also highlighting the important link between heterogeneous catalysis and sustainability to all those interested. Combines foundational knowledge with a focus on practical applications Organizes information by reaction type, allowing readers to easily find examples of how to carry out specific reaction types with solid catalysts Highlights emerging areas such as nanoparticle catalysis and metal-organic framework (MOF) based catalysts
Catalytic Hydrogenation In Organic Synthesis
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Author : Morris Freifelder
language : en
Publisher: John Wiley & Sons
Release Date : 1978-11
Catalytic Hydrogenation In Organic Synthesis written by Morris Freifelder and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 1978-11 with Science categories.
Based on over 22 years of experience, this book presents a substantial accumulation of knowledge. Clearly and understandably written, it gives detailed descriptions of many experiments, providing step-by-step procedures along with personal notes and observations, directions, suggestions, and safety precautions. The yields obtained in these experiments are good to excellent, and most of the hydrogenations discussed are carried out under very mild conditions.
Handbook Of Asymmetric Heterogeneous Catalysis
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Author : Kuiling Ding
language : en
Publisher: John Wiley & Sons
Release Date : 2008-10-20
Handbook Of Asymmetric Heterogeneous Catalysis written by Kuiling Ding and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2008-10-20 with Science categories.
In this most up-to-date handbook each chapter contains a general introduction, followed by the principles of the immobilization and, finally, applications. In this way, it covers the most important approaches currently employed for the heterogenization of chiral catalysts, including data tables, applications, reaction types and literature citations. For chemists in both academia and industry as well as those working in the fine chemical and pharmaceutical industry.
Hydrogenation
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Author : Iyad Karamé
language : en
Publisher: BoD – Books on Demand
Release Date : 2012-10-10
Hydrogenation written by Iyad Karamé and has been published by BoD – Books on Demand this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-10-10 with Science categories.
The domain of catalytic hydrogenation continues to grow fast, reflecting the wide range of chemical applications that can be enhanced by the easy use of molecular hydrogen. The advances in characterization techniques and their application have improved our understanding of the catalytic processes and mechanisms occurring in both homogeneous and heterogeneous catalysis. The aim of this volume, although not exhaustive, is to provide a general overview of new progress of the hydrogenation reactions. This volume comprises a series of various contributions, as reviews or original articles, treating heterogeneously and homogeneously catalyzed hydrogenation reactions. It is composed of three parts: hydrogenation reactions in fine organic chemistry, hydrogenation reactions in environmental chemistry and renewable energy, and special topics in hydrogenation.
Hydrogenation
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Author : S. David Jackson
language : en
Publisher: Walter de Gruyter GmbH & Co KG
Release Date : 2018-09-24
Hydrogenation written by S. David Jackson and has been published by Walter de Gruyter GmbH & Co KG this book supported file pdf, txt, epub, kindle and other format this book has been release on 2018-09-24 with Science categories.
This book gives a comprehensive overview of modern hydrogenation methods used in organic synthesis.In clearly structured chapters, the authors cover the catalysts, scope and limitations of their application, and the techniques for hydrogenation of carbon-carbon, carbon-heteroatom and heteroatom-heteroatom multiple bonds.
Catalytic Hydrogenation
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Author : L. Cervený
language : en
Publisher: Elsevier
Release Date : 1986-08-01
Catalytic Hydrogenation written by L. Cervený and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 1986-08-01 with Technology & Engineering categories.
The collection of contributions in this volume presents the most up-to-date findings in catalytic hydrogenation. The individual chapters have been written by 36 top specialists each of whom has achieved a remarkable depth of coverage when dealing with his particular topic. In addition to detailed treatment of the most recent problems connected with catalytic hydrogenations, the book also contains a number of previously unpublished results obtained either by the authors themselves or within the organizations to which they are affiliated.Because of its topical and original character, the book provides a wealth of information which will be invaluable not only to researchers and technicians dealing with hydrogenation, but also to all those concerned with homogeneous and heterogeneous catalysis, organic technology, petrochemistry and chemical engineering.