High Resolution Nmr Spectroscopy
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High Resolution Nmr Techniques In Organic Chemistry
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Author : T. Claridge
language : en
Publisher: Elsevier
Release Date : 1999-12-24
High Resolution Nmr Techniques In Organic Chemistry written by T. Claridge and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 1999-12-24 with Science categories.
From the initial observation of proton magnetic resonance in water and in paraffin, the discipline of nuclear magnetic resonance has seen unparalleled growth as an analytical method. Modern NMR spectroscopy is a highly developed, yet still evolving, subject which finds application in chemistry, biology, medicine, materials science and geology. In this book, emphasis is on the more recently developed methods of solution-state NMR applicable to chemical research, which are chosen for their wide applicability and robustness. These have, in many cases, already become established techniques in NMR laboratories, in both academic and industrial establishments. A considerable amount of information and guidance is given on the implementation and execution of the techniques described in this book.
High Resolution Nmr
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Author : Edwin D. Becker
language : en
Publisher: Elsevier
Release Date : 2012-12-02
High Resolution Nmr written by Edwin D. Becker and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-02 with Science categories.
High Resolution NMR: Theory and Chemical Applications discusses the principles and theory of nuclear magnetic resonance and how this concept is used in the chemical sciences. This book is written at an intermediate level, with mathematics used to augment verbal descriptions of the phenomena. This text pays attention to developing and interrelating four approaches – the steady state energy levels, the rotating vector picture, the density matrix, and the product operator formalism. The style of this book is based on the assumption that the reader has an acquaintance with the general principles of quantum mechanics, but no extensive background in quantum theory or proficiency in mathematics is required. This book begins with a description of the basic physics, together with a brief account of the historical development of the field. It looks at the study of NMR in liquids, including high resolution NMR in the solid state and the principles of NMR imaging and localized spectroscopy. This book is intended to assist chemistry graduate students, advanced undergraduate students, or researchers to understand NMR at a fundamental level. This text also provides illustrations of the applications of NMR to the determination of the structure of small organic molecules and macromolecules, including proteins.
Modern Techniques In High Resolution Ft Nmr
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Author : Narayanan Chandrakumar
language : en
Publisher: Springer Science & Business Media
Release Date : 2012-12-06
Modern Techniques In High Resolution Ft Nmr written by Narayanan Chandrakumar and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-06 with Science categories.
The magnetism of nuclear spin systems has proved an amazingly fertile ground for the creativity of researchers. This happy circumstance results from the triple benediction that nature appears to have bestowed on nuclear spins: they are sporting spies-being infinitely manipulable (one is even tempted to say malleable), not unduly coy in revealing their secrets, and having a whole treasure house of secrets to reveal in the first place. researcher with Since spin dynamics are now orchestrated by the NMR ever more subtle scores, it is important to be able to tune into the pro ceedings with precision, if one is to make sense of it at all. Fortunately, it is not terribly difficult to do so, since in many ways spin dynamics are the theoretician's dream come true: they are often finite dimensional and quite tractable with basic quantum mechanics, frequently allowing near exact treatments and readily testable predictions. This book was conceived two years ago, with the objective of providing a simple, consistent introduction to the description of the spin dynamics that one encounters in modern NMR experiments. We believed it was a good time to attempt this, since it was possible by then to give sufficiently general descriptions of powelful classes of new NMR experiments. The choice of experiments we discuss in detail is necessarily subjective, al though we hope to have given a flavor of most of the important classes of pulse sequences, including some surface coil imaging applications.
High Resolution Nmr Techniques In Organic Chemistry
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Author : NMR Facility Manager the Dyson Perrins Laboratory Timothy D W Claridge
language : en
Publisher:
Release Date : 2016-05-27
High Resolution Nmr Techniques In Organic Chemistry written by NMR Facility Manager the Dyson Perrins Laboratory Timothy D W Claridge and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2016-05-27 with Chemistry, Organic categories.
"High-Resolution NMR Techniques in Organic Chemistry, Third Edition" describes the most important NMR spectroscopy techniques for the structure elucidation of organic molecules and the investigation of their behaviour in solution. Appropriate for advanced undergraduate and graduate students, research chemists and NMR facility managers, this thorough revision covers practical aspects of NMR techniques and instrumentation, data collection, and spectrum interpretation. It describes all major classes of one- and two-dimensional NMR experiments including homonuclear and heteronuclear correlations, the nuclear Overhauser effect, diffusion measurements, and techniques for studying protein ligand interactions. A trusted authority on this critical expertise, "High-Resolution NMR Techniques in Organic Chemistry," "Third Edition "is an essential resource for every chemist and NMR spectroscopist."
High Resolution Nmr Techniques In Organic Chemistry
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Author : Timothy D.W. Claridge
language : en
Publisher: Newnes
Release Date : 2008-11-19
High Resolution Nmr Techniques In Organic Chemistry written by Timothy D.W. Claridge and has been published by Newnes this book supported file pdf, txt, epub, kindle and other format this book has been release on 2008-11-19 with Mathematics categories.
High-Resolution NMR Techniques in Organic Chemistry describes the most important high-resolution NMR techniques that find use in the structure elucidation of organic molecules and the investigation of their behavior in solution. The techniques are presented and explained using pictorial formats wherever possible, limiting the number of mathematical descriptions. The emphasis is on the more recently developed methods of solution-state NMR spectroscopy with a considerable amount of information on implementation and on the setting of critical parameters for anyone wishing to exploit these methods. - Presents a large number of examples to demonstrate the utility of the methods covered - Serves the needs of students and professionals in every chemistry laboratory - Describes the most important methods available, with guidance on execution of experiments
Quantum Description Of High Resolution Nmr In Liquids
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Author : Maurice Goldman
language : en
Publisher:
Release Date : 2023
Quantum Description Of High Resolution Nmr In Liquids written by Maurice Goldman and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2023 with Liquids categories.
This text describes the main methods of one- and two-dimensional high-resolution NMR spectroscopy in liquids within the quantum-mechanical formalism of the density matrix. In view of the increasing importance of NMR in chemistry and biochemistry, it is particularly addressed to those scientists who do not have a working knowledge of quantum calculations.
Principles Of High Resolution Nmr In Solids
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Author : M. Mehring
language : en
Publisher: Springer Science & Business Media
Release Date : 2012-12-06
Principles Of High Resolution Nmr In Solids written by M. Mehring and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-06 with Science categories.
The field of Nuclear Magnetic Resonance (NMR) has developed at a fascinating pace during the last decade. It always has been an extremely valuable tool to the organic chemist by supplying molecular "finger print" spectra at the atomic level. Unfortunately the high resolution achievable in liquid solutions could not be obtained in solids and physicists and physical chemists had to live with unresolved lines open to a wealth of curve fitting procedures and a vast amount of speculations. High resolution NMR in solids seemed to be a paradoxon. Broad structure less lines are usually encountered when dealing with NMR in solids. Only with the recent advent of mUltiple pulse, magic angle, cross-polarization, two-dimen sional and multiple-quantum spectroscopy and other techniques during the last decade it became possible to resolve finer details of nuclear spin interactions in solids. I have felt that graduate students, researchers and others beginning to get involved with these techniques needed a book which treats the principles, theo retical foundations and applications of these rather sophisticated experimental techniques. Therefore I wrote a monograph on the subject in 1976. Very soon new ideas led to the developement of "two-dimensional spectroscopy" and "multiple-quantum spectroscopy", topics which were not covered in the first edition of my book. Moreover an exponential growth of literature appeared in this area of research leaving the beginner in an awkward situation of tracing back from a current article to the roots of the experiment.
High Resolution Nmr Of Macromolecules
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Author : Frank A. Bovey
language : en
Publisher:
Release Date : 1972
High Resolution Nmr Of Macromolecules written by Frank A. Bovey and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1972 with categories.
Nmr Spectroscopy In Organic Chemistry
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Author : B. I. Ionin
language : en
Publisher: Springer Science & Business Media
Release Date : 2012-12-06
Nmr Spectroscopy In Organic Chemistry written by B. I. Ionin and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-06 with Science categories.
In recent years high-resolution nuclear magnetic resonance spec troscopy has found very wide application in organie chemistry in structural and physicochemical investigations and. also in the study of the characteristics of organic compounds which are re lated to the distribution of the electron cloud in the molecules. The vigorous development of this method, which may really be re garded as an independent branch of science, is the result of ex tensive progress in NMR technology, the refinement of its theory, and the accumulation of large amounts of experimental material, which has been correlated by empiricallaws and principles. The literature directly concerned with the NMR method and its applica tion has now grown to such an extent that a complete review of it is practically impossible. Therefore the authors have limited themselves to an examination of only the most important, funda mental, and general investigations. The book consists of six chapters. In the first chapter we have attempted to present the fundamentals of the NMR method in such a way that the reader with little knowledge of the subject will be able to use the method in practical work for investigating simple compounds and solving simple problems. The three subsequent chapters give a deeper analysis of the method, while the last two chapters and the appendix illustrate the various applications of NMR spectroscopy in organic chemistry.