Modern Techniques In High Resolution Ft Nmr

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Modern Techniques In High Resolution Ft Nmr
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Author : Narayanan Chandrakumar
language : en
Publisher: Springer Science & Business Media
Release Date : 2012-12-06
Modern Techniques In High Resolution Ft Nmr written by Narayanan Chandrakumar and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-06 with Science categories.
The magnetism of nuclear spin systems has proved an amazingly fertile ground for the creativity of researchers. This happy circumstance results from the triple benediction that nature appears to have bestowed on nuclear spins: they are sporting spies-being infinitely manipulable (one is even tempted to say malleable), not unduly coy in revealing their secrets, and having a whole treasure house of secrets to reveal in the first place. researcher with Since spin dynamics are now orchestrated by the NMR ever more subtle scores, it is important to be able to tune into the pro ceedings with precision, if one is to make sense of it at all. Fortunately, it is not terribly difficult to do so, since in many ways spin dynamics are the theoretician's dream come true: they are often finite dimensional and quite tractable with basic quantum mechanics, frequently allowing near exact treatments and readily testable predictions. This book was conceived two years ago, with the objective of providing a simple, consistent introduction to the description of the spin dynamics that one encounters in modern NMR experiments. We believed it was a good time to attempt this, since it was possible by then to give sufficiently general descriptions of powelful classes of new NMR experiments. The choice of experiments we discuss in detail is necessarily subjective, al though we hope to have given a flavor of most of the important classes of pulse sequences, including some surface coil imaging applications.
Modern Techniques In High Resolution Ft Nmr
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Author : Narayanan Chandrakumar
language : en
Publisher:
Release Date : 1986-11-01
Modern Techniques In High Resolution Ft Nmr written by Narayanan Chandrakumar and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1986-11-01 with categories.
High Resolution Nmr
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Author : Edwin D. Becker
language : en
Publisher: Elsevier
Release Date : 1999-10-08
High Resolution Nmr written by Edwin D. Becker and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 1999-10-08 with Science categories.
High Resolution NMR provides a broad treatment of the principles and theory of nuclear magnetic resonance (NMR) as it is used in the chemical sciences. It is written at an "intermediate" level, with mathematics used to augment, rather than replace, clear verbal descriptions of the phenomena. The book is intended to allow a graduate student, advanced undergraduate, or researcher to understand NMR at a fundamental level, and to see illustrations of the applications of NMR to the determination of the structure of small organic molecules and macromolecules, including proteins. Emphasis is on the study of NMR in liquids, but the treatment also includes high resolution NMR in the solid state and the principles of NMR imaging and localized spectroscopy. Careful attention is given to developing and interrelating four approaches - steady state energy levels, the rotating vector picture, the density matrix, and the product operator formalism. The presentation is based on the assumption that the reader has an acquaintance with the general principles of quantum mechanics, but no extensive background in quantum theory or proficiency in mathematics is required. Likewise, no previous background in NMR is assumed, since the book begins with a description of the basic physics, together with a brief account of the historical development of the field. This third edition of High Resolution NMR preserves the "conversational" approach of the previous editions that has been well accepted as a teaching tool. However, more than half the material is new, and the remainder has been revised extensively. Problems are included to reinforce concepts in the book. - Uses mathematics to augment, not replace, verbal explanations - Written in a clear and conversational style - Follows the successful format and approach of two previous editions - Revised and updated extensively--about 70 percent of the text is new - Includes problems and references to additional reading at the end of each chapter
Structure Elucidation By Modern Nmr
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Author : Helmut Duddeck
language : en
Publisher: Springer Science & Business Media
Release Date : 2012-12-06
Structure Elucidation By Modern Nmr written by Helmut Duddeck and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-06 with Science categories.
For several years, we have been organizing seminars and workshops on the application of modem one and two-dimensional NMR methods at the faculty of chemistry in the Ruhr-University Bochum, FRG, and elsewhere, addressing researchers and graduate students who work in the field of organic and natural products chemistry. In 1987, we wrote a workbook (StrukturaufkUirung mit modemer NMR-Spektroskopie, Steinkopff, Darmstadt, FRG, 1988) in German language based on our experience in these courses. Many of the exercises described therein have been used in such courses and some of them have been shaped by the participants to a great extent. The response of readers and discussions with colleagues from many countries encouraged us two years later to produce an English translation in order to make the book accessible to a wider audience. Moreover, the content has been increased from 20 exercise examples in the German, to 23 in English version. Now, after the rapid development of basic multipulse NMR me thods in the early 1980s, the avantgarde in modem NMR is concentrating on the invention and optimi zation of advanced techniques, e. g. , three-dimensional experiments. For the beginners, however, the situation has not changed markedly since the appearence of the first edition of this book. Therefore, we decided not to add new techniques to this second edition, but rather to increase the number of exerci ses from 23 to 33, the new ones being basically single-spectrum-problems.
Nmr In Biological Systems
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Author : K.V.R. Chary
language : en
Publisher: Springer Science & Business Media
Release Date : 2008-04-08
Nmr In Biological Systems written by K.V.R. Chary and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2008-04-08 with Science categories.
During teaching NMR to students and researchers, we felt the need for a text-book which can cover modern trends in the application of NMR to biological systems. This book covers the entire area of NMR in Biological Sciences (Biomolecules, cells and tissues, animals, plants and drug design). As well as being useful to researchers, this is an excellent book for teaching a course on NMR in Biological Systems.
A Comprehensive Textbook Of Modern Pharmaceutical Analytical Techniques
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Author : Dr. Sanmati Kumar Jain
language : en
Publisher: Shashwat Publication
Release Date : 2025-06-07
A Comprehensive Textbook Of Modern Pharmaceutical Analytical Techniques written by Dr. Sanmati Kumar Jain and has been published by Shashwat Publication this book supported file pdf, txt, epub, kindle and other format this book has been release on 2025-06-07 with Medical categories.
A Comprehensive Textbook of Modern Pharmaceutical Analytical Techniques is a meticulously crafted academic resource designed to meet the growing demands of postgraduate students, researchers, and professionals in the field of pharmaceutical sciences. Aligned with the latest Pharmacy Council of India (PCI) curriculum for M. Pharm programs, this textbook presents a unified and in-depth understanding of modern instrumental and analytical methodologies used in drug discovery, quality control, formulation analysis, and regulatory compliance. What sets this textbook apart is its clarity, scientific depth, and pedagogical approach. It integrates insights from leading scientific literature, pharmacopeias (IP, BP, USP, EP), international guidelines, and recent trends in analytical instrumentation. Furthermore, the book includes over 100 cited references from authoritative sources such as B.K. Sharma, Skoog & Holler, P.D. Sethi, Willard, and others, providing a rich academic foundation for further exploration.
Pulse And Fourier Transform Nmr
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Author : Thomas Clark Farrar
language : en
Publisher: Academic Press
Release Date : 1971-08-28
Pulse And Fourier Transform Nmr written by Thomas Clark Farrar and has been published by Academic Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 1971-08-28 with Mathematics categories.
Pulse and Fourier Transform NMR: Introduction to Theory and Methods presents the different types of pulse experiments that are commonly used and provides the theoretical background necessary for understanding these techniques. This book evaluates the practical application of pulse methods and the necessary instrumentation. Organized into seven chapters, this book begins with an overview of the NMR fundamentals and the basic pulse methods. This text then summarizes the important features of pulse spectrometers. Other chapters consider the rationale, the advantages, and the limitations of Fourier transform NMR methods. This book discusses as well how the idea of the rotating frame can be utilized to understand certain experiments that extend the range of application of pulse methods. The final chapter deals with a few significant special uses of pulse techniques. This book is a valuable resource for chemists and readers who are familiar with high resolution NMR but with no background in pulse methods.
Multidimensional Nmr Methods For The Solution State
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Author : Gareth A. Morris
language : en
Publisher: John Wiley & Sons
Release Date : 2012-12-19
Multidimensional Nmr Methods For The Solution State written by Gareth A. Morris and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-19 with Science categories.
The content of this volume has been added to eMagRes (formerly Encyclopedia of Magnetic Resonance) - the ultimate online resource for NMR and MRI. The literature of multidimensional NMR began with the publication of three papers in 1975, then nine in 1976 and fifteen in 1977, and now contains many tens of thousands of papers. Any attempt to survey the field must therefore necessarily be very selective, not to say partial. In assembling this handbook, the Editors have sought to provide both the new researcher and the established scientist with a solid foundation for the understanding of multidimensional NMR, a representative if inevitably limited survey of its applications, an authoritative account of classic techniques such as COSY, NOESY and TOSCY, and an account of the latest progress in the development of multidimensional techniques. This handbook is structured in four parts. The first opens with an historical introduction to, and a brief account of, the practicalities and applications of multidimensional NMR methods, followed by a definitive survey of their conceptual basis and a series of articles setting out the generic principles of methods for acquiring and processing multidimensional NMR data. In the second part, the main families of multidimensional techniques, arranged in approximate order of increasing complexity, are described in detail, from simple J-resolved spectroscopy through to the powerful heteronuclear 3D and 4D methods that now dominate the study of structural biology in solution. The third part offers and illustrative selection from the very wide range of applications of multidimensional NMR methods, including some of the most recent developments in protein NMR. Finally, the fourth part introduces the idea of multidimensional spectra containing non-frequency dimensions, in which properties such as diffusion and relaxation are correlated. About EMR Handbooks / eMagRes Handbooks The Encyclopedia of Magnetic Resonance (up to 2012) and eMagRes (from 2013 onward) publish a wide range of online articles on all aspects of magnetic resonance in physics, chemistry, biology and medicine. The existence of this large number of articles, written by experts in various fields, is enabling the publication of a series of EMR Handbooks / eMagRes Handbooks on specific areas of NMR and MRI. The chapters of each of these handbooks will comprise a carefully chosen selection of articles from eMagRes. In consultation with the eMagRes Editorial Board, the EMR Handbooks / eMagRes Handbooks are coherently planned in advance by specially-selected Editors, and new articles are written (together with updates of some already existing articles) to give appropriate complete coverage. The handbooks are intended to be of value and interest to research students, postdoctoral fellows and other researchers learning about the scientific area in question and undertaking relevant experiments, whether in academia or industry. Have the content of this Handbook and the complete content of eMagRes at your fingertips! Visit: www.wileyonlinelibrary.com/ref/eMagRes View other eMagRes publications here
Fourier Transforms In Nmr Optical And Mass Spectrometry
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Author : A.G. Marshall
language : en
Publisher: Elsevier
Release Date : 2016-02-25
Fourier Transforms In Nmr Optical And Mass Spectrometry written by A.G. Marshall and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2016-02-25 with Science categories.
Written by spectroscopists for spectroscopists, here is a book which is not only a valuable handbook and reference work, but also an ideal teaching text for Fourier transform methods as they are applied in spectroscopy. It offers the first unified treatment of the three most popular types of FT/spectroscopy, with uniform notation and complete indexing of specialized terms. All mathematics is self-contained, and requires only a knowledge of simple calculus. The main emphasis is on pictures and physical analogs rather than detailed algebra. Instructive problems, presented at the end of each chapter, offer extensions of the basic treatment. Solutions are given or outlined for all problems.The book offers a wealth of practical information to spectroscopists. Non-ideal effects are treated in detail: noise (source- and detector-limited); non-linear response; limits to spectrometer performance based on finite detection period, finite data size, mis-phasing, etc. Common puzzles and paradoxes are explained: e.g. use of mathematically complex variables to represent physically real quantities; interpretation of negative frequency signals; on-resonance vs. off-resonance response; interpolation (when it helps and when it doesn't); ultimate accuracy of the data; differences between linearly- and circularly-polarized radiation; multiplex advantage or disadvantage, etc.Chapter 1 introduces the fundamental line shapes encountered in spectroscopy, from a simple classical mass-on-a-spring model. The Fourier transform relationship between the time-domain response to a sudden impulse and the steady-state frequency-domain response (absorption and dispersion spectra) to a continuous oscillation is established and illustrated. Chapters 2 and 3 summarize the basic mathematics (definitions, formulas, theorems, and examples) for continuous (analog) and discrete (digital) Fourier transforms, and their practical implications. Experimental aspects which are common to the signal (Chapter 4) and noise (Chapter 5) in all forms of Fourier transform spectrometry are followed by separate chapters for treatment of those features which are unique to FT/MS, FT/optical, FT/NMR, and other types of FT/spectroscopy.The list of references includes both historical and comprehensive reviews and monographs, along with articles describing several key developments. The appendices provide instant access to FT integrals and fast algorithms as well as a pictorial library of common Fourier transform function pairs. The comprehensive index is designed to enable the reader to locate particular key words, including those with more than one name.
High Resolution Nmr Techniques In Organic Chemistry
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Author : T. Claridge
language : en
Publisher: Elsevier
Release Date : 1999-12-24
High Resolution Nmr Techniques In Organic Chemistry written by T. Claridge and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 1999-12-24 with Science categories.
From the initial observation of proton magnetic resonance in water and in paraffin, the discipline of nuclear magnetic resonance has seen unparalleled growth as an analytical method. Modern NMR spectroscopy is a highly developed, yet still evolving, subject which finds application in chemistry, biology, medicine, materials science and geology. In this book, emphasis is on the more recently developed methods of solution-state NMR applicable to chemical research, which are chosen for their wide applicability and robustness. These have, in many cases, already become established techniques in NMR laboratories, in both academic and industrial establishments. A considerable amount of information and guidance is given on the implementation and execution of the techniques described in this book.