In Situ Characterization Techniques For Nanomaterials
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In Situ Characterization Techniques For Nanomaterials
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Author : Challa S.S.R. Kumar
language : en
Publisher: Springer
Release Date : 2018-04-17
In Situ Characterization Techniques For Nanomaterials written by Challa S.S.R. Kumar and has been published by Springer this book supported file pdf, txt, epub, kindle and other format this book has been release on 2018-04-17 with Technology & Engineering categories.
Seventh volume of a 40 volume series on nanoscience and nanotechnology, edited by the renowned scientist Challa S.S.R. Kumar. This handbook gives a comprehensive overview about In-situ Characterization Techniques for Nanomaterials. Modern applications and state-of-the-art techniques are covered and make this volume an essential reading for research scientists in academia and industry.
In Situ Characterization Techniques For Nanomaterials
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Author : Challa S. S. R. Kumar
language : en
Publisher:
Release Date : 2018
In Situ Characterization Techniques For Nanomaterials written by Challa S. S. R. Kumar and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2018 with Nanostructured materials categories.
Seventh volume of a 40 volume series on nanoscience and nanotechnology, edited by the renowned scientist Challa S.S.R. Kumar. This handbook gives a comprehensive overview about In-situ Characterization Techniques for Nanomaterials. Modern applications and state-of-the-art techniques are covered and make this volume an essential reading for research scientists in academia and industry.
Characterization Techniques For Nanomaterials
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Author : Imalka Munaweera
language : en
Publisher: CRC Press
Release Date : 2023-03-01
Characterization Techniques For Nanomaterials written by Imalka Munaweera and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2023-03-01 with Science categories.
Manipulation of matter at the nanoscale level is the key factor in nanotechnology, and it is considered as a great driving force behind the current industrial revolution since it offers facile and feasible remedies for many problems. Because of the unique characteristic properties of nanomaterials, they can be employed in a wide variety of fields such as agriculture and food technology, catalysis, biomedical applications, tissue culture engineering, and fertilizers. In this regard, characterization of nanomaterials plays a significant role in determining their optical, thermal, and physicochemical properties. Many techniques have been used in nanomaterial characterization, and the most important techniques are discussed in detail in this book with their principles, basic operation procedures, and applications with suitable examples. In summary, this book offers broad content on the most important chemical and structural characterization techniques of nanomaterials. The book offers comprehensive coverage of the most essential topics, including the following: Provides a comprehensive understanding of physical and chemical characterization techniques of nanomaterials Includes details about basic principles of each characterization technique with appropriate examples Covers most of the important characterization techniques that should be known to undergraduate/early career scientists/beginners in materials chemistry Provides all the basic knowledge to understand and carry out the respective analysis of nanomaterials Fulfills the timely need of a book that covers the most important and useful characterization techniques in nanomaterial characterization Up to date, there are no other books/book chapters which discuss most of these nanocharacterization techniques in one segment with all the basic instrumentation details and narrated examples of nanomaterial characterization. In a nutshell, this book will be a great asset to undergraduates/early career scientists/beginners of material science as it provides a comprehensive and complete understanding of most of the techniques used in nanocharacterization tools in a short time. Intended audience is based on science education while specifically focusing on undergraduates/graduate students/early scientists and beginners of chemistry, materials chemistry, and nanotechnology and nanoscience.
In Situ Transmission Electron Microscopy Characterization Of Nanomaterials
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Author : Joon Hwan Lee
language : en
Publisher:
Release Date : 2013
In Situ Transmission Electron Microscopy Characterization Of Nanomaterials written by Joon Hwan Lee and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013 with categories.
With the recent development of in situ transmission electron microscopy (TEM) characterization techniques, the real time study of property-structure correlations in nanomaterials becomes possible. This dissertation reports the direct observations of deformation behavior of Al2O3-ZrO2-MgAl2O4 (AZM) bulk ceramic nanocomposites, strengthening mechanism of twins in YBa2Cu3O7−x (YBCO) thin film, work hardening event in nanocrystalline nickel and deformation of 2wt% Al doped ZnO (AZO) thin film with nanorod structures using the in situ TEM nanoindentation tool. The combined in situ movies with quantitative loading-unloading curves reveal the deformation mechanism of the above nanomaterial systems. At room temperature, in situ dynamic deformation studies show that the AZM nanocomposites undergo the deformation mainly through the grain-boundary sliding and rotation of small grains, i.e., ZrO2 grains, and some of the large grains, i.e., MgAl2O4 grains. We observed both plastic and elastic deformations in different sample regions in these multi-phase ceramic nanocomposites at room temperature. Both ex situ (conventional) and in situ nanoindentation were conducted to reveal the deformation of YBCO films from the directions perpendicular and parallel to the twin interfaces. Hardness measured perpendicular to twin interfaces is ~50% and 40% higher than that measured parallel to twin interfaces, by ex situ and in situ, respectively. By using an in situ nanoindentation tool inside TEM, dynamic work hardening event in nanocrystalline nickel was directly observed. During stain hardening stage, abundant Lomer-Cottrell (L-C) locks formed both within nanograins and against twin boundaries. Two major mechanisms were identified during interactions between L-C locks and twin boundaries. Quantitative nanoindentation experiments recorded during in situ experiments show an increase of yield strength from 1.64 to 2.29 GPa during multiple loading-unloading cycles. In situ TEM nanoindentation has been conducted to explore the size dependent deformation behavior of two different types (type I: ~ 0.51 of width/length ratio and type II: ~ 088 ratio) of AZO nanorods. During the indentation on type I nanord structure, annihilation of defects has been observed which is caused by limitation of the defect activities by relatively small size of the width. On the other hand, type II nanorod shows dislocation activities which enhanced the grain rotation under the external force applied on more isotropic direction through type II nanorod. The electronic version of this dissertation is accessible from http://hdl.handle.net/1969.1/148150
Characterization Of Nanostructures
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Author : Sverre Myhra
language : en
Publisher: CRC Press
Release Date : 2012-06-12
Characterization Of Nanostructures written by Sverre Myhra and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-06-12 with Science categories.
The techniques and methods that can be applied to materials characterization on the microscale are numerous and well-established. Divided into two parts, Characterization of Nanostructures provides thumbnail sketches of the most widely used techniques and methods that apply to nanostructures, and discusses typical applications to single nanoscale objects, as well as to ensembles of such objects. Section I: Techniques and Methods overviews the physical principles of the main techniques and describes those operational modes that are most relevant to nanoscale characterization. It provides sufficient technical detail so that readers and prospective users can gain an appreciation of the strengths and limitations of particular techniques. The section covers both mainstream and less commonly used techniques. Section II: Applications of Techniques to Structures of Different Dimensionalities and Functionalities deals with the methods for materials characterization of generic types of systems, using carefully chosen illustrations from the literature. Each chapter begins with a brief description of the materials and supplies a context for the methods for characterization. The volume concludes with a series of flow charts and brief descriptions of tactical issues. The authors focus on the needs of the research laboratory but also address those of quality control, industrial troubleshooting, and online analysis. Characterization of Nanostructures describes those techniques and their operational modes that are most relevant to nanoscale characterization. It is especially relevant to systems of different dimensionalities and functionalities. The book builds a bridge between generalists, who play vital roles in the post-disciplinary area of nanotechnology, and specialists, who view themselves as more in the context of the discipline.
Nanocharacterization Techniques
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Author : Osvaldo de Oliveira Jr
language : en
Publisher: William Andrew
Release Date : 2017-03-18
Nanocharacterization Techniques written by Osvaldo de Oliveira Jr and has been published by William Andrew this book supported file pdf, txt, epub, kindle and other format this book has been release on 2017-03-18 with Technology & Engineering categories.
Nanocharacterization Techniques covers the main characterization techniques used in nanomaterials and nanostructures. The chapters focus on the fundamental aspects of characterization techniques and their distinctive approaches. Significant advances that have taken place over recent years in refining techniques are covered, and the mathematical foundations needed to use the techniques are also explained in detail. This book is an important reference for materials scientists and engineers looking for a through analysis of nanocharacterization techniques in order to establish which is best for their needs. Includes a detailed analysis of different nanocharacterization techniques, allowing readers to explore which one is best for their particular needs Provides examples of how each characterization technique has been used, giving readers a greater understanding of how each technique can be profitably used Covers the mathematical background needed to utilize each of these techniques to their best effect, meaning that readers can gain a full understanding of the theoretical principles behind each technique covered Serves as an important, go-to reference for materials scientists and engineers
Bimetallic Nanostructures
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Author : Ya-Wen Zhang
language : en
Publisher: John Wiley & Sons
Release Date : 2018-05-14
Bimetallic Nanostructures written by Ya-Wen Zhang and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2018-05-14 with Science categories.
Systematically summarizes the current status and recent advances in bimetallic structures, their shape-controlled synthesis, properties, and applications Intensive researches are currently being carried out on bimetallic nanostructures, focusing on a number of fundamental, physical, and chemical questions regarding their synthesis and properties. This book presents a systematic and comprehensive summary of the current status and recent advances in this field, supporting readers in the synthesis of model bimetallic nanoparticles, and the exploration and interpretation of their properties. Bimetallic Nanostructures: Shape-Controlled Synthesis for Catalysis, Plasmonics and Sensing Applications is divided into three parts. Part 1 introduces basic chemical and physical knowledge of bimetallic structures, including fundamentals, computational models, and in situ characterization techniques. Part 2 summarizes recent developments in synthetic methods, characterization, and properties of bimetallic structures from the perspective of morphology effect, including zero-dimensional nanomaterials, one-dimensional nanomaterials, and two-dimensional nanomaterials. Part 3 discusses applications in electrocatalysis, heterogeneous catalysis, plasmonics and sensing. Comprehensive reference for an important multidisciplinary research field Thoroughly summarizes the present state and latest developments in bimetallic structures Helps researchers find optimal synthetic methods and explore new phenomena in surface science and synthetic chemistry of bimetallic nanostructures Bimetallic Nanostructures: Shape-Controlled Synthesis for Catalysis, Plasmonics and Sensing Applications is an excellent source or reference for researchers and advanced students. Academic researchers in nanoscience, nanocatalysis, and surface plasmonics, and those working in industry in areas involving nanotechnology, catalysis and optoelectronics, will find this book of interest.
Scanning Microscopy For Nanotechnology
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Author : Weilie Zhou
language : en
Publisher: Springer Science & Business Media
Release Date : 2007-03-09
Scanning Microscopy For Nanotechnology written by Weilie Zhou and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2007-03-09 with Technology & Engineering categories.
This book presents scanning electron microscopy (SEM) fundamentals and applications for nanotechnology. It includes integrated fabrication techniques using the SEM, such as e-beam and FIB, and it covers in-situ nanomanipulation of materials. The book is written by international experts from the top nano-research groups that specialize in nanomaterials characterization. The book will appeal to nanomaterials researchers, and to SEM development specialists.
In Situ Characterization Of The Surface State Of Nanoparticles
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Author : Alfred P. Weber
language : en
Publisher:
Release Date : 1998
In Situ Characterization Of The Surface State Of Nanoparticles written by Alfred P. Weber and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1998 with Chemical engineering categories.
Nanocomposites
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Author : Luigi Nicolais
language : en
Publisher: John Wiley & Sons
Release Date : 2013-12-03
Nanocomposites written by Luigi Nicolais and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-12-03 with Science categories.
A Step-by-step guide to the synthesis and characterization of metal-polymer nanocomposites Polymer nanocomposites, polymers that are reinforced with nano-sized particles, provide enhanced mechanical, thermal, electrical, and barrier properties. Continued research and development of new polymer nanocomposites promises to provide enhanced materials to a broad range of industries, such as plastics, aerospace, automotive, electronics, packaging, and biomedical devices. Structured as a practical laboratory manual, this book enables readers to expertly synthesize and characterize metal-polymer nanocomposites by clearly setting forth the principles and techniques. Nanocomposites: In Situ Synthesis of Polymer-Embedded Nanostructures features contributions from an international team of materials science and nanotechnology experts. Chapters reflect the authors' critical review of the literature as well as their own laboratory experience working with polymer nanocomposites. The book begins with a detailed introduction to the science, properties, and applications of metal-polymer nanocomposites. Next, it covers such topics as: Morphological and topological concepts Phase separation and nanoparticle aggregation Methods for the synthesis of nanocomposites Morphological control Characterization techniques and data analysis methods Toxicity considerations High-resolution images of metal nanoparticles, created by transmission electron microscopy, are provided throughout the book. There are also plenty of process schemes and detailed drawings, helping readers better understand how to synthesize, characterize, and use these composite materials. A bibliography at the end of each chapter provides a gateway to original research papers and reviews in the field. With its focus on the practical steps of synthesis and characterization, Nanocomposites: In Situ Synthesis of Polymer-Embedded Nanostructures is recommended for both students and practitioners in nanotechnology, polymer science, and materials science and engineering.