Introduction To Nmr Spectroscopy
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Introduction To Nmr Spectroscopy
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Author : R. J. Abraham
language : en
Publisher: Wiley-Blackwell
Release Date : 1988
Introduction To Nmr Spectroscopy written by R. J. Abraham and has been published by Wiley-Blackwell this book supported file pdf, txt, epub, kindle and other format this book has been release on 1988 with Science categories.
Introduction to NMR Spectroscopy R. J. Abraham, School of Chemistry, University of Liverpool J. Fisher, Biological NMR Centre, University of Leicester P. Loftus, Stuart Pharmaceuticals, Delaware, USA This book is a new, extended edition of Proton and Carbon 13 NMR by R. J. Abraham and P. Loftus. The initial chapters cover the fundamentals of NMR spectroscopy commencing with an explanation of how the nuclear magnetic response occurs, followed by a detailed discussion of chemical shifts and coupling constants, parameters not discussed to any length in other textbooks aimed at a similar level of interest. Emphasis is given to the vectorial description of multipulse experiments, as this is probably the easiest way to grasp how different information may be gained simply by changing a pulse sequence. An understanding of multipulse NMR is a prerequisite for understanding 2D NMR. The section on 2D NMR begins with a discussion of the resolved experiment. This is a logical initial choice as the spectra produced by this experiment may be readily compared with 1D spectra. Following on from this both heteronuclear and homonuclear correlation spectroscopy are described and examples given. The final section of the book should be considered as an applications section. It is aimed at showing the reader that NMR is not just of use to the synthetic organic chemist but is also of use to biochemists for investigating the solution state structure and function of proteins, enzymes, etc. The application of high resolution NMR to the solid state is also discussed, thereby indicating the developments which have taken place as far as spectrometer hardware is concerned.
Introduction To Nmr Spectroscopy
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Author : Raymond John Abraham
language : en
Publisher:
Release Date : 1988-11-24
Introduction To Nmr Spectroscopy written by Raymond John Abraham and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1988-11-24 with Science categories.
Introduction to NMR Spectroscopy R. J. Abraham, School of Chemistry, University of Liverpool J. Fisher, Biological NMR Centre, University of Leicester P. Loftus, Stuart Pharmaceuticals, Delaware, USA This book is a new, extended edition of Proton and Carbon 13 NMR by R. J. Abraham and P. Loftus. The initial chapters cover the fundamentals of NMR spectroscopy commencing with an explanation of how the nuclear magnetic response occurs, followed by a detailed discussion of chemical shifts and coupling constants, parameters not discussed to any length in other textbooks aimed at a similar level of interest. Emphasis is given to the vectorial description of multipulse experiments, as this is probably the easiest way to grasp how different information may be gained simply by changing a pulse sequence. An understanding of multipulse NMR is a prerequisite for understanding 2D NMR. The section on 2D NMR begins with a discussion of the resolved experiment. This is a logical initial choice as the spectra produced by this experiment may be readily compared with 1D spectra. Following on from this both heteronuclear and homonuclear correlation spectroscopy are described and examples given. The final section of the book should be considered as an applications section. It is aimed at showing the reader that NMR is not just of use to the synthetic organic chemist but is also of use to biochemists for investigating the solution state structure and function of proteins, enzymes, etc. The application of high resolution NMR to the solid state is also discussed, thereby indicating the developments which have taken place as far as spectrometer hardware is concerned.
Nuclear Magnetic Resonance Spectroscopy
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Author : Joseph B. Lambert
language : en
Publisher: John Wiley & Sons
Release Date : 2019-01-04
Nuclear Magnetic Resonance Spectroscopy written by Joseph B. Lambert and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019-01-04 with Science categories.
Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.
Proton And Carbon 13 Nmr Spectroscopy
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Author : Raymond John Abraham
language : en
Publisher:
Release Date : 1978
Proton And Carbon 13 Nmr Spectroscopy written by Raymond John Abraham and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1978 with Science categories.
Phosphorus 31 Nmr Spectroscopy
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Author : Olaf Kühl
language : en
Publisher: Springer Science & Business Media
Release Date : 2008-08-22
Phosphorus 31 Nmr Spectroscopy written by Olaf Kühl and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2008-08-22 with Science categories.
Nuclear Magnetic Resonance is a powerful tool, especially for the identification of 1 13 hitherto unknown organic compounds. H- and C-NMR spectroscopy is known and applied by virtually every synthetically working Organic Chemist. Con- quently, the factors governing the differences in chemical shift values, based on chemical environment, bonding, temperature, solvent, pH, etc. , are well understood, and specialty methods developed for almost every conceivable structural challenge. Proton and carbon NMR spectroscopy is part of most bachelors degree courses, with advanced methods integrated into masters degree and other graduate courses. In view of this universal knowledge about proton and carbon NMR spectr- copy within the chemical community, it is remarkable that heteronuclear NMR is still looked upon as something of a curiosity. Admittedly, most organic compounds contain only nitrogen, oxygen, and sulfur atoms, as well as the obligatory hydrogen and carbon atoms, elements that have an unfavourable isotope distribution when it comes to NMR spectroscopy. Each of these three elements has a dominant isotope: 14 16 32 16 32 N (99. 63% natural abundance), O (99. 76%), and S (95. 02%), with O, S, and 34 14 S (4. 21%) NMR silent. N has a nuclear moment I = 1 and a sizeable quadrupolar moment that makes the NMR signals usually very broad and dif cult to analyse.
Nmr Spectroscopy Of Polymers
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Author : Tatsuki Kitayama
language : en
Publisher: Springer Science & Business Media
Release Date : 2004-02-17
Nmr Spectroscopy Of Polymers written by Tatsuki Kitayama and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2004-02-17 with Technology & Engineering categories.
Based on the authors ́ extensive experimental experience, NMR Spectroscopy of Polymers explains the practical use of NMR spectroscopy in polymer chemistry.
Nmr Spectroscopy
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Author : Harald Günther
language : en
Publisher: John Wiley & Sons
Release Date : 2013-12-13
Nmr Spectroscopy written by Harald Günther and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-12-13 with Science categories.
Nuclear magnetic resonance (NMR) spectroscopy is one of the most powerful and widely used techniques in chemical research for investigating structures and dynamics of molecules. Advanced methods can even be utilized for structure determinations of biopolymers, for example proteins or nucleic acids. NMR is also used in medicine for magnetic resonance imaging (MRI). The method is based on spectral lines of different atomic nuclei that are excited when a strong magnetic field and a radiofrequency transmitter are applied. The method is very sensitive to the features of molecular structure because also the neighboring atoms influence the signals from individual nuclei and this is important for determining the 3D-structure of molecules. This new edition of the popular classic has a clear style and a highly practical, mostly non-mathematical approach. Many examples are taken from organic and organometallic chemistry, making this book an invaluable guide to undergraduate and graduate students of organic chemistry, biochemistry, spectroscopy or physical chemistry, and to researchers using this well-established and extremely important technique. Problems and solutions are included.
Understanding Nmr Spectroscopy
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Author : James Keeler
language : en
Publisher: John Wiley & Sons
Release Date : 2011-09-19
Understanding Nmr Spectroscopy written by James Keeler and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2011-09-19 with Science categories.
This text is aimed at people who have some familiarity with high-resolution NMR and who wish to deepen their understanding of how NMR experiments actually ‘work’. This revised and updated edition takes the same approach as the highly-acclaimed first edition. The text concentrates on the description of commonly-used experiments and explains in detail the theory behind how such experiments work. The quantum mechanical tools needed to analyse pulse sequences are introduced set by step, but the approach is relatively informal with the emphasis on obtaining a good understanding of how the experiments actually work. The use of two-colour printing and a new larger format improves the readability of the text. In addition, a number of new topics have been introduced: How product operators can be extended to describe experiments in AX2 and AX3 spin systems, thus making it possible to discuss the important APT, INEPT and DEPT experiments often used in carbon-13 NMR. Spin system analysis i.e. how shifts and couplings can be extracted from strongly-coupled (second-order) spectra. How the presence of chemically equivalent spins leads to spectral features which are somewhat unusual and possibly misleading, even at high magnetic fields. A discussion of chemical exchange effects has been introduced in order to help with the explanation of transverse relaxation. The double-quantum spectroscopy of a three-spin system is now considered in more detail. Reviews of the First Edition “For anyone wishing to know what really goes on in their NMR experiments, I would highly recommend this book” – Chemistry World “...I warmly recommend for budding NMR spectroscopists, or others who wish to deepen their understanding of elementary NMR theory or theoretical tools” – Magnetic Resonance in Chemistry
High Resolution Nmr Techniques In Organic Chemistry
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Author : T. Claridge
language : en
Publisher: Elsevier
Release Date : 1999-12-24
High Resolution Nmr Techniques In Organic Chemistry written by T. Claridge and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 1999-12-24 with Science categories.
From the initial observation of proton magnetic resonance in water and in paraffin, the discipline of nuclear magnetic resonance has seen unparalleled growth as an analytical method. Modern NMR spectroscopy is a highly developed, yet still evolving, subject which finds application in chemistry, biology, medicine, materials science and geology. In this book, emphasis is on the more recently developed methods of solution-state NMR applicable to chemical research, which are chosen for their wide applicability and robustness. These have, in many cases, already become established techniques in NMR laboratories, in both academic and industrial establishments. A considerable amount of information and guidance is given on the implementation and execution of the techniques described in this book.
Nmr Spectroscopy Explained
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Author : Neil E. Jacobsen
language : en
Publisher: John Wiley & Sons
Release Date : 2007-08-24
Nmr Spectroscopy Explained written by Neil E. Jacobsen and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2007-08-24 with Science categories.
NMR Spectroscopy Explained : Simplified Theory, Applications and Examples for Organic Chemistry and Structural Biology provides a fresh, practical guide to NMR for both students and practitioners, in a clearly written and non-mathematical format. It gives the reader an intermediate level theoretical basis for understanding laboratory applications, developing concepts gradually within the context of examples and useful experiments. Introduces students to modern NMR as applied to analysis of organic compounds. Presents material in a clear, conversational style that is appealing to students. Contains comprehensive coverage of how NMR experiments actually work. Combines basic ideas with practical implementation of the spectrometer. Provides an intermediate level theoretical basis for understanding laboratory experiments. Develops concepts gradually within the context of examples and useful experiments. Introduces the product operator formalism after introducing the simpler (but limited) vector model.