Modulated Temperature Differential Scanning Calorimetry
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Modulated Temperature Differential Scanning Calorimetry
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Author : Mike Reading
language : en
Publisher: Springer Science & Business Media
Release Date : 2006-10-12
Modulated Temperature Differential Scanning Calorimetry written by Mike Reading and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2006-10-12 with Technology & Engineering categories.
MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of the sample’s heat capacity from the modulation. The new information this provided sparked a revolution in scanning calorimetry by enabling new insights to be gained into almost all aspects of polymer characteristics. This book provides both a basic and advanced treatment of the theory of the technique followed by a detailed exposition of its application to reacting systems, blends and semicrystalline polymers by the leaders in all of these fields. It is an essential text for anybody interested in calorimetry or polymer characterization, especially if they have found that conventional DSC cannot help them with their problems.
Differential Scanning Calorimetry
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Author : Günther Höhne
language : en
Publisher: Springer Science & Business Media
Release Date : 2013-03-09
Differential Scanning Calorimetry written by Günther Höhne and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-03-09 with Science categories.
In this fully updated and revised second edition the authors provide the newcomer and the experienced practitioner with a balanced and comprehensive insight into all important DSC methods, including a sound presentation of the theoretical basis of DSC and TMDSC measurements. Emphasis is layed on instrumentation, the underlying measurement principles, metrologically correct calibrations, factors influencing the measurement process, and on the exact interpretation of the results. The information given enables the research scientist, the analyst and experienced laboratory staff to apply DSC methods successfully and to measure respective properties correctly.
Modulated Temperature Differential Scanning Calorimetry
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Author : Mike Reading
language : en
Publisher: Springer Science & Business Media
Release Date : 2006-02-22
Modulated Temperature Differential Scanning Calorimetry written by Mike Reading and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2006-02-22 with Medical categories.
MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of the sample’s heat capacity from the modulation. The new information this provided sparked a revolution in scanning calorimetry by enabling new insights to be gained into almost all aspects of polymer characteristics. This book provides both a basic and advanced treatment of the theory of the technique followed by a detailed exposition of its application to reacting systems, blends and semicrystalline polymers by the leaders in all of these fields. It is an essential text for anybody interested in calorimetry or polymer characterization, especially if they have found that conventional DSC cannot help them with their problems.
Differential Scanning Calorimetry
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Author : G.W.H. Höhne
language : en
Publisher:
Release Date : 2003
Differential Scanning Calorimetry written by G.W.H. Höhne and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2003 with categories.
In this updated and fully revised second edition, the authors provide the newcomer and the experienced practitioner with a balanced and comprehensive insight into all important methods and aspects of Differential Scanning Calorimetry (DSC), including a sound presentation of the theoretical basis of DSC thermal analysis and temperature-modulated DSC (TMDCS). Emphasis is placed on modern evaluation techniques, instrumentation, the underlying measurement principles, metrologically correct calibrations, factors influencing the measurement process, and on the exact interpretation of the results. The information enables the research scientist, the analyst and experienced laboratory staff to choose the most suitable equipment, to apply DSC methods successfully, to interpret the measurement curve, and thus to measure key properties precisely. In addition, the new edition includes improved instrumental techniques such as Tzerotm and StepScantm, new evaluation techniques, more applications, and the latest references. Calorimetry - Dynamische Differenzkalorimetrie - Thermal Analysis - Thermische Analyse
Thermal Analysis Of Polymers
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Author : Joseph D. Menczel
language : en
Publisher: John Wiley & Sons
Release Date : 2014-07-09
Thermal Analysis Of Polymers written by Joseph D. Menczel and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2014-07-09 with Science categories.
Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background. Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation. Written by experts in the various areas of thermal analysis Relevant and detailed experiments and examples follow each chapter.
Principles And Applications Of Thermal Analysis
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Author : Paul Gabbott
language : en
Publisher: John Wiley & Sons
Release Date : 2008-04-30
Principles And Applications Of Thermal Analysis written by Paul Gabbott and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2008-04-30 with Science categories.
Thermal Analysis techniques are used in a wide range of disciplines, from pharmacy and foods to polymer science, materials and glasses; in fact any field where changes in sample behaviour are observed under controlled heating or controlled cooling conditions. The wide range of measurements possible provide fundamental information on the material properties of the system under test, so thermal analysis has found increasing use both in basic characterisation of materials and in a wide range of applications in research, development and quality control in industry and academia. Principles and Applications of Thermal Analysis is written by manufacturers and experienced users of thermal techniques. It provides the reader with sound practical instruction on how to use the techniques and gives an up to date account of the principle industrial applications. By covering basic thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) including the new approach of Fast Scanning DSC, together with dynamic mechanical analysis (DMA /TMA) methods, then developing the discussion to encompass industrial applications, the book serves as an ideal introduction to the technology for new users. With a strong focus on practical issues and relating the measurements to the physical behaviour of the materials under test, the book will also serve as an important reference for experienced analysts.
Thermal Analysis
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Author : El-Zeiny Ebeid
language : en
Publisher: Elsevier
Release Date : 2021-06-23
Thermal Analysis written by El-Zeiny Ebeid and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2021-06-23 with Science categories.
Thermal Analysis: From Introductory Fundamentals to Advanced Applications presents an easy-to-understand introduction to Thermal Analysis (TA) principles alongside in-depth coverage of the wide variety of techniques currently in use across several industries. It covers differential scanning calorimetry (DSC), temperature modulated DSC (TMDSC), differential thermal analysis (DTA), thermogravimetry (TG) or thermogravimetric analysis (TGA), thermomechanical analysis (TMA), differential photo-calorimetry (DPC), dynamic mechanical analysis (DMA), thermodilatometry (TD), dielectric thermal analysis (DEA), thermally-stimulated current (TSC), emanation thermal analysis (ETA), thermoluminescence (TL), fast scanning calorimetry (FSC), and microcalorimetry. Chapters define the various TA techniques, report the Temperature-Modulated DSC (TMDSC) method and its applications, especially its use for studying the thermodynamic properties of polymers and pharmaceuticals, focus on the potential of TA in materials science with applications in chemistry and engineering, demonstrate, in detail, the various applications of TA in food, electronic industries, solid-state reactions, chemistry of polymers and large directing agents, kinetic studies, demonstrate the crystal structure and phase changes occurring upon heating by TA, and the potential of TA in recycling and waste management. Gives a solid introduction to the scientific principles of TA for those who are new to these techniques or need a deeper understanding Illustrates concepts with more than 100 schematic and analysis curves, several flow charts, process diagrams and photographs Contains chapters that cover the user of TA in materials science and crystal structures
Materials Characterization By Dynamic And Modulated Thermal Analytical Techniques
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Author : Alan T. Riga
language : en
Publisher: ASTM International
Release Date : 2001
Materials Characterization By Dynamic And Modulated Thermal Analytical Techniques written by Alan T. Riga and has been published by ASTM International this book supported file pdf, txt, epub, kindle and other format this book has been release on 2001 with Calorimetry categories.
The special technical publication has been compiled from the 15 presentations at a May 2000 Association symposium in Toronto. They cover the fundamentals of the techniques, its use in curing and chemical reactions, measuring the glass transition and melting by modulated and comparative techniques, g
Handbook Of Thermal Analysis And Calorimetry
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Author :
language : en
Publisher: Elsevier
Release Date : 2018-03-12
Handbook Of Thermal Analysis And Calorimetry written by and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2018-03-12 with Science categories.
Handbook of Thermal Analysis and Calorimetry: Recent Advances, Techniques and Applications, Volume Six, Second Edition, presents the latest in a series that has been well received by the thermal analysis and calorimetry community. This volume covers recent advances in techniques and applications that complement the earlier volumes. There has been tremendous progress in the field in recent years, and this book puts together the most high-impact topics selected for their popularity by new editors Sergey Vyazovkin, Nobuyoshi Koga and Christoph Schick—all editors of Thermochimica Acta. Among the important new techniques covered are biomass conversion; sustainable polymers; polymer nanocompsoties; nonmetallic glasses; phase change materials; propellants and explosives; applications to pharmaceuticals; processes in ceramics, metals, and alloys; ionic liquids; fast-scanning calorimetry, and more. Features 19 all-new chapters to bring readers up to date on the current status of the field Provides a broad overview of recent progress in the most popular techniques and applications Includes chapters authored by a recognized leader in each field and compiled by a new team of editors, each with at least 20 years of experience in the field of thermal analysis and calorimetry Enables applications across a wide range of modern materials, including polymers, metals, alloys, ceramics, energetics and pharmaceutics Overviews the current status of the field and summarizes recent progress in the most popular techniques and applications
Principles Of Thermal Analysis And Calorimetry
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Author : Simon Gaisford
language : en
Publisher: Royal Society of Chemistry
Release Date : 2019-03-15
Principles Of Thermal Analysis And Calorimetry written by Simon Gaisford and has been published by Royal Society of Chemistry this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019-03-15 with Science categories.
The use of thermal and calorimetric methods has shown rapid growth over the past few decades, in an increasingly wide range of applications. The original text was published in 2001; since then there have been significant advances in various analytical techniques and their applications. This second edition supplies an up to date, concise and readable account of the principles, experimental apparatus and practical procedures used in thermal analysis and calorimetric methods of analysis. Written by experts in their field, brief accounts of the basic theory are reinforced with detailed technical advances and contemporary developments. Where appropriate, applications are used to highlight particular operating principles or methods of interpretation. As an important source of information for many levels of readership in a variety of areas, this book will be an aid for students and lecturers through to industrial and laboratory staff and consultants.