Modulated Temperature Differential Scanning Calorimetry
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Modulated Temperature Differential Scanning Calorimetry
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Author : Mike Reading
language : en
Publisher: Springer Science & Business Media
Release Date : 2006-10-12
Modulated Temperature Differential Scanning Calorimetry written by Mike Reading and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2006-10-12 with Technology & Engineering categories.
MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of the sample’s heat capacity from the modulation. The new information this provided sparked a revolution in scanning calorimetry by enabling new insights to be gained into almost all aspects of polymer characteristics. This book provides both a basic and advanced treatment of the theory of the technique followed by a detailed exposition of its application to reacting systems, blends and semicrystalline polymers by the leaders in all of these fields. It is an essential text for anybody interested in calorimetry or polymer characterization, especially if they have found that conventional DSC cannot help them with their problems.
Differential Scanning Calorimetry
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Author : Günther Höhne
language : en
Publisher: Springer Science & Business Media
Release Date : 2013-03-09
Differential Scanning Calorimetry written by Günther Höhne and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-03-09 with Science categories.
In this fully updated and revised second edition the authors provide the newcomer and the experienced practitioner with a balanced and comprehensive insight into all important DSC methods, including a sound presentation of the theoretical basis of DSC and TMDSC measurements. Emphasis is layed on instrumentation, the underlying measurement principles, metrologically correct calibrations, factors influencing the measurement process, and on the exact interpretation of the results. The information given enables the research scientist, the analyst and experienced laboratory staff to apply DSC methods successfully and to measure respective properties correctly.
Modulated Temperature Differential Scanning Calorimetry
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Author : Mike Reading
language : en
Publisher: Springer Science & Business Media
Release Date : 2006-02-22
Modulated Temperature Differential Scanning Calorimetry written by Mike Reading and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2006-02-22 with Medical categories.
MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of the sample’s heat capacity from the modulation. The new information this provided sparked a revolution in scanning calorimetry by enabling new insights to be gained into almost all aspects of polymer characteristics. This book provides both a basic and advanced treatment of the theory of the technique followed by a detailed exposition of its application to reacting systems, blends and semicrystalline polymers by the leaders in all of these fields. It is an essential text for anybody interested in calorimetry or polymer characterization, especially if they have found that conventional DSC cannot help them with their problems.
Differential Scanning Calorimetry
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Author : G.W.H. Höhne
language : en
Publisher:
Release Date : 2003
Differential Scanning Calorimetry written by G.W.H. Höhne and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2003 with categories.
In this updated and fully revised second edition, the authors provide the newcomer and the experienced practitioner with a balanced and comprehensive insight into all important methods and aspects of Differential Scanning Calorimetry (DSC), including a sound presentation of the theoretical basis of DSC thermal analysis and temperature-modulated DSC (TMDCS). Emphasis is placed on modern evaluation techniques, instrumentation, the underlying measurement principles, metrologically correct calibrations, factors influencing the measurement process, and on the exact interpretation of the results. The information enables the research scientist, the analyst and experienced laboratory staff to choose the most suitable equipment, to apply DSC methods successfully, to interpret the measurement curve, and thus to measure key properties precisely. In addition, the new edition includes improved instrumental techniques such as Tzerotm and StepScantm, new evaluation techniques, more applications, and the latest references. Calorimetry - Dynamische Differenzkalorimetrie - Thermal Analysis - Thermische Analyse
Materials Characterization By Dynamic And Modulated Thermal Analytical Techniques
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Author : Alan T. Riga
language : en
Publisher: ASTM International
Release Date : 2001
Materials Characterization By Dynamic And Modulated Thermal Analytical Techniques written by Alan T. Riga and has been published by ASTM International this book supported file pdf, txt, epub, kindle and other format this book has been release on 2001 with Calorimetry categories.
The special technical publication has been compiled from the 15 presentations at a May 2000 Association symposium in Toronto. They cover the fundamentals of the techniques, its use in curing and chemical reactions, measuring the glass transition and melting by modulated and comparative techniques, g
Thermal Analysis
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Author : El-Zeiny Ebeid
language : en
Publisher: Elsevier
Release Date : 2021-06-23
Thermal Analysis written by El-Zeiny Ebeid and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2021-06-23 with Science categories.
Thermal Analysis: From Introductory Fundamentals to Advanced Applications presents an easy-to-understand introduction to Thermal Analysis (TA) principles alongside in-depth coverage of the wide variety of techniques currently in use across several industries. It covers differential scanning calorimetry (DSC), temperature modulated DSC (TMDSC), differential thermal analysis (DTA), thermogravimetry (TG) or thermogravimetric analysis (TGA), thermomechanical analysis (TMA), differential photo-calorimetry (DPC), dynamic mechanical analysis (DMA), thermodilatometry (TD), dielectric thermal analysis (DEA), thermally-stimulated current (TSC), emanation thermal analysis (ETA), thermoluminescence (TL), fast scanning calorimetry (FSC), and microcalorimetry. Chapters define the various TA techniques, report the Temperature-Modulated DSC (TMDSC) method and its applications, especially its use for studying the thermodynamic properties of polymers and pharmaceuticals, focus on the potential of TA in materials science with applications in chemistry and engineering, demonstrate, in detail, the various applications of TA in food, electronic industries, solid-state reactions, chemistry of polymers and large directing agents, kinetic studies, demonstrate the crystal structure and phase changes occurring upon heating by TA, and the potential of TA in recycling and waste management. Gives a solid introduction to the scientific principles of TA for those who are new to these techniques or need a deeper understanding Illustrates concepts with more than 100 schematic and analysis curves, several flow charts, process diagrams and photographs Contains chapters that cover the user of TA in materials science and crystal structures
Thermal Analysis Of Polymers
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Author : Joseph D. Menczel
language : en
Publisher: John Wiley & Sons
Release Date : 2014-07-09
Thermal Analysis Of Polymers written by Joseph D. Menczel and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2014-07-09 with Science categories.
Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background. Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation. Written by experts in the various areas of thermal analysis Relevant and detailed experiments and examples follow each chapter.
Principles Of Thermal Analysis And Calorimetry
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Author : Simon Gaisford
language : en
Publisher: Royal Society of Chemistry
Release Date : 2019-03-15
Principles Of Thermal Analysis And Calorimetry written by Simon Gaisford and has been published by Royal Society of Chemistry this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019-03-15 with Science categories.
The use of thermal and calorimetric methods has shown rapid growth over the past few decades, in an increasingly wide range of applications. The original text was published in 2001; since then there have been significant advances in various analytical techniques and their applications. This second edition supplies an up to date, concise and readable account of the principles, experimental apparatus and practical procedures used in thermal analysis and calorimetric methods of analysis. Written by experts in their field, brief accounts of the basic theory are reinforced with detailed technical advances and contemporary developments. Where appropriate, applications are used to highlight particular operating principles or methods of interpretation. As an important source of information for many levels of readership in a variety of areas, this book will be an aid for students and lecturers through to industrial and laboratory staff and consultants.
Thermal Analysis Of Polymeric Materials
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Author : Krzysztof Pielichowski
language : en
Publisher: John Wiley & Sons
Release Date : 2022-06-01
Thermal Analysis Of Polymeric Materials written by Krzysztof Pielichowski and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2022-06-01 with Technology & Engineering categories.
An all-in-one reference work covering the essential principles and techniques on thermal behavior and response of polymeric materials This book delivers a detailed understanding of the thermal behavior of polymeric materials evaluated by thermal analysis methods. It covers the most widely applied principles which are used in method development to substantiate what happens upon heating of polymers. It also reviews the key application areas of polymers in materials science. Edited by two experts in the field, the book covers a wide range of specific topics within the aforementioned categories of discussion, such as: Crucial thermal phenomena - glass transition, crystallization behavior and curing kinetics Polymeric materials that have gained considerable interest over the last decade The latest advancements in techniques related to the field, such as modulated temperature DSC and fast scanning calorimetry The recent advances in hyphenated techniques and their applications Polymer chemists, chemical engineers, materials scientists, and process engineers can use this comprehensive reference work to gain clarity on the topics discussed within and learn how to harness them in practical applications across a wide range of disciplines.
Handbook Of Thermal Analysis And Calorimetry
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Author : Michael E. Brown
language : en
Publisher: Elsevier
Release Date : 1998-09-07
Handbook Of Thermal Analysis And Calorimetry written by Michael E. Brown and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 1998-09-07 with Science categories.
Handbook of Thermal Analysis and Calorimetry, Volume 1: Principles and Practice describes the basic background information common to thermal analysis and calorimetry in general. Thermodynamic and kinetic principles are discussed along with the instrumentation and methodology associated with thermoanalytical and calorimetric techniques. The purpose is to collect the discussion of these general principles and minimize redundancies in the subsequent volumes that are concerned with the applications of these principles and methods. More unique methods, which pertain to specific processes or materials, are covered in later volumes.