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Preparative Carbohydrate Chemistry


Preparative Carbohydrate Chemistry
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Preparative Carbohydrate Chemistry


Preparative Carbohydrate Chemistry
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Author : Stephen Hanessian
language : en
Publisher: CRC Press
Release Date : 1997-01-02

Preparative Carbohydrate Chemistry written by Stephen Hanessian and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 1997-01-02 with Science categories.


Detailing commonly used methods and procedures, this reference discusses the reactions and derivative forms of carbohydrates. Preparative Carbohydrate Chemistry covers the formation, cleavage, and reactions of derivatives and illustrates bond-forming reactions of SN2 types, free radicals, chain extensions, and branching. The contents include: sugar derivatives; selected reactions in carbohydrate chemistry; chemical synthesis of oligosaccharides and O-and N -glycosyl compounds; enzymatic synthesis of sialic acid, KDO, and related deoxyulosonic acids, and of oligosaccharides; synthesis of -glycosyl compounds; carbocycles from carbohydrates; and total synthesis of sugars from non-sugars. This authoritative reference offers relevant chapters on reactions and derivative forms of carbohydrates, including commonly used methods as well as new experimental procedures. It also contains insightful chapter commentaries and succinct topic histories.



General Carbohydrate Method


General Carbohydrate Method
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Author : Roy Whistler
language : en
Publisher: Elsevier
Release Date : 2012-12-02

General Carbohydrate Method written by Roy Whistler and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-02 with Science categories.


Methods in Carbohydrate Chemistry, Volume VI: General Carbohydrate Methods contains a collection of selected methods from the entire field of carbohydrate chemistry. This volume is comprised of useful procedures in analytical and preparative carbohydrate chemistry. It is organized into 10 sections. The first section deals with methods for separation and analysis, which discusses chromatography and chemical, physical, and biochemical methods. Section II covers the preparation of mono- and polysaccharides and their derivatives. Section III describes a variety of oxidation methods. The fourth section is about procedures for the analysis of acyclic sugars. Sections V and VI present the etherification and esterification of carbohydrates. Nucleotides, nucleosides, and glycoside procedures are described in Sections VII and VIII. The ninth section focuses on radioactively labeled sugars. The final chapter provides a variety of physical methods such as mass spectrometry, nuclear magnetic resonance spectroscopy, and determination of molecular weights by osmometry. Chemists and biochemists will find this book very useful.



General Carbohydrate Methods


General Carbohydrate Methods
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Author : James N. BeMiller
language : en
Publisher:
Release Date : 1972

General Carbohydrate Methods written by James N. BeMiller and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1972 with Carbohydrates categories.




Methods In Carbohydrate Chemistry Analysis And Preparation Of Sugars


Methods In Carbohydrate Chemistry Analysis And Preparation Of Sugars
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Author : Roy Lester Whistler
language : en
Publisher:
Release Date : 1962

Methods In Carbohydrate Chemistry Analysis And Preparation Of Sugars written by Roy Lester Whistler and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1962 with Carbohydrates categories.




Carbohydrate Chemistry


Carbohydrate Chemistry
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Author : Pavol Kováč
language : en
Publisher: CRC Press
Release Date : 2016-04-19

Carbohydrate Chemistry written by Pavol Kováč and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2016-04-19 with Medical categories.


Long gone are the days when synthetic publications included parallel preparative experiments to document reproducibility of the experimental protocols and when journals required such documentation. The new Proven Synthetic Methods Series addresses concerns to chemists regarding irreproducibility of synthetic protocols, lack of characterization data



Analysis And Preparation Of Sugars


Analysis And Preparation Of Sugars
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Author :
language : en
Publisher:
Release Date : 1964

Analysis And Preparation Of Sugars written by and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1964 with categories.




Methods In Carbohydrate Chemistry


Methods In Carbohydrate Chemistry
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Author : Roy Lester Whistler
language : en
Publisher:
Release Date : 1962

Methods In Carbohydrate Chemistry written by Roy Lester Whistler and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1962 with Carbohydrates categories.




Carbohydrate Chemistry


Carbohydrate Chemistry
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Author : Christian Vogel
language : en
Publisher: CRC Press
Release Date : 2017-09-18

Carbohydrate Chemistry written by Christian Vogel and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2017-09-18 with Medical categories.


Volumes in the Proven Synthetic Methods Series address the concerns many chemists have regarding irreproducibility of synthetic protocols, lack of identification and characterization data for new compounds, and inflated yields reported in chemical communications—trends that have recently become a serious problem. Featuring contributions from world-renowned experts and overseen by a highly respected series editor, Carbohydrate Chemistry: Proven Synthetic Methods, Volume 4 compiles reliable synthetic methods and protocols for the preparation of intermediates for carbohydrate synthesis or other uses in the glycosciences. Exploring carbohydrate chemistry from both the academic and industrial points of view, this unique resource brings together useful information into one convenient reference. The series is unique among other synthetic literature in the carbohydrate field in that, to ensure reproducibility, an independent checker has verified the experimental parts involved by repeating the protocols or using the methods. The book includes new or more detailed versions of previously published protocols as well as those published in not readily available journals. The essential characteristics of the protocols presented are reliability, updated characterization data for newly synthesized substances and the expectation of wide utility in the carbohydrate field. The protocols presented will be of wide use to a broad range of readers in the carbohydrate field and the life sciences, including undergraduates taking carbohydrate workshops.



Carbohydrate Chemistry


Carbohydrate Chemistry
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Author : Paul Kosma
language : en
Publisher: CRC Press
Release Date : 2021-01-14

Carbohydrate Chemistry written by Paul Kosma and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2021-01-14 with Medical categories.


Volumes in the Proven Synthetic Methods Series address the concerns many chemists have regarding irreproducibility of synthetic protocols, lack of identification and characterization data for new compounds, and inflated yields reported in chemical communications—trends that have recently become a serious problem. Exploring carbohydrate chemistry from both the academic and industrial points of view, this unique resource brings together useful information into one convenient reference. The series is unique among other synthetic literature in the carbohydrate field in that, to ensure reproducibility, an independent checker has verified the experimental parts involved by repeating the protocols or using the methods. Featuring contributions from world-renowned experts and overseen by a highly respected series editor, this latest volume compiles reliable protocols for the preparation of intermediates for carbohydrate synthesis or other uses in the glycosciences. Key Features: Explains reliable and tested protocols for the preparation of intermediates for carbohydrate synthesis Offers a unique resource in glycosciences, compiling useful information in one reference Presents protocols that are of wide use to a broad range of readers in the carbohydrate field and the life sciences, including undergraduates taking carbohydrate workshops Explores synthetic carbohydrate chemistry from both the academic and industrial points of view Guarantees the reader a good, clean, reproducible experiment



Carbohydrate Chemistry


Carbohydrate Chemistry
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Author : Gijsbert van der Marel
language : en
Publisher: CRC Press
Release Date : 2014-03-04

Carbohydrate Chemistry written by Gijsbert van der Marel and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2014-03-04 with Medical categories.


The second volume in the series Carbohydrate Chemistry: Proven Synthetic Methods, Volume 2 offers a collection of synthetic procedures valuable to the practice of synthetic carbohydrate chemistry. The series takes an important and unique approach in that all described procedures have been independently verified as reliable and reproducible. With editors and contributors who are highly respected scientists in the field, this book provides a widely useful reference for both researchers and students, exploring carbohydrate chemistry from both academic and industrial points of view. The book begins with an introductory section that offers tricks and tips collected by the series editor from many years of experience working in carbohydrate laboratories. The subsequent chapters present detailed protocols on both specific synthetic transformations and the preparation of common synthetic intermediates, with figures to aid in comprehension. Procedures are described for regioselective benzylidene ring opening reactions, oxidation reactions to provide uronic acids, stereoselective alpha-glucosylation reactions, and more. Protocols for synthetic intermediates of general utility include 3,4,6-tri-O-acetyl-d-galactal, phenyl 4,6-O-benzylidene-1-thio-α-d-mannopyranoside, 1,2-anhydro-3,4,6-tri-O-benzyl-β-d-mannopyranoside, and methyl N-acetylneuraminic acid, among many others. Each chapter presents in-depth experimental descriptions for the reported procedures, including reaction setup, reaction conditions, work-up procedures, and purification protocols. The chapters also provide detailed characterization of all products and intermediates as well as copies of the 1H NMR and 13C NMR of the described products and intermediates to indicate the purity of the obtained materials and to serve as a valuable reference for future practitioners. This book provides an important starting point to reliably access synthetic carbohydrate materials and as such offers a valuable resource for the synthetic organic chemistry community. Through the streamlined access of well-defined products it provides a thrust to the rapidly growing field of chemical glycobiology.