Pyrolysis Gas Chromatography Mass Spectrometry Of Polymeric Materials Second Edition

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Pyrolysis Gas Chromatography Mass Spectrometry Of Polymeric Materials
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Author : Peter Kusch
language : en
Publisher: World Scientific
Release Date : 2018-10-08
Pyrolysis Gas Chromatography Mass Spectrometry Of Polymeric Materials written by Peter Kusch and has been published by World Scientific this book supported file pdf, txt, epub, kindle and other format this book has been release on 2018-10-08 with Science categories.
The methodology of analytical pyrolysis-GC/MS has been known for several years, but is seldom used in research laboratories and process control in the chemical industry. This is due to the relative difficulty of interpreting the identified pyrolysis products as well as the variety of them. This book contains full identification of several classes of polymers/copolymers and biopolymers that can be very helpful to the user. In addition, the practical applications can encourage analytical chemists and engineers to use the techniques explored in this volume.The structure and the functions of various types of pyrolyzers and the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C are described. Practical applications of these techniques are also included, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems.
Pyrolysis Gas Chromatography Mass Spectrometry Of Polymeric Materials Second Edition
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Author : Peter Kusch
language : en
Publisher: World Scientific
Release Date : 2023-08-28
Pyrolysis Gas Chromatography Mass Spectrometry Of Polymeric Materials Second Edition written by Peter Kusch and has been published by World Scientific this book supported file pdf, txt, epub, kindle and other format this book has been release on 2023-08-28 with Science categories.
Readers will find many practical applications of pyrolysis-GC/MS as well as R&D usage in this newly revised and expanded edition. Detailed experimental descriptions for the identification of synthetic polymers and copolymers are included. This volume presents the current state of analytical pyrolysis, and contains full identification of several classes of polymers/copolymers and biopolymers that readers will find helpful. Structures and functions of various types of pyrolyzers are explored, as well as the results of the pyrolysis-gas chromatographic-mass spectrometric identification of synthetic polymers/copolymers and biopolymers at 700°C.Practical applications of this hyphenated technique, detailing the analysis of microplastics, failure analysis in the automotive industry and solutions for technological problems are provided. Numerous practical applications of pyrolysis-GC/MS, for industrial and R&D usage, will be of benefit to Chemists and Engineers, as well as for students of Chemistry and Polymer Sciences.
Pyrolysis Gc Ms Data Book Of Synthetic Polymers
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Author : Shin Tsuge
language : en
Publisher: Elsevier
Release Date : 2011-08-02
Pyrolysis Gc Ms Data Book Of Synthetic Polymers written by Shin Tsuge and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2011-08-02 with Science categories.
In this data book, both conventional Py-GC/MS where thermal energy alone is used to cause fragmentation of given polymeric materials and reactive Py-GC/MS in the presence of organic alkaline for condensation polymers are compiled. Before going into detailed presentation of the data, however, acquiring a firm grip on the proper understanding about the situation of Py-GC/MS would promote better utilization of the following pyrolysis data for various polymers samples. This book incorporates recent technological advances in analytical pyrolysis methods especially useful for the characterization of 163 typical synthetic polymers. The book briefly reviews the instrumentation available in advanced analytical pyrolysis, and offers guidance to perform effectually this technique combining with gas chromatography and mass spectrometry. Main contents are comprehensive sample pyrograms, thermograms, identification tables, and representative mass spectra (MS) of pyrolyzates for synthetic polymers. This edition also highlights thermally-assisted hydrolysis and methylation technique effectively applied to 33 basic condensation polymers. - Coverage of Py-GC/MS data of conventional pyrograms and thermograms of basic 163 kinds of synthetic polymers together with MS and retention index data for pyrolyzates, enabling a quick identification - Additional coverage of the pyrograms and their related data for 33 basic condensation polymers obtained by the thermally-assisted hydrolysis and methylation technique - All compiled data measured under the same experimental conditions for pyrolysis, gas chromatography and mass spectrometry to facilitate peak identification - Surveyable instant information on two facing pages dedicated to the whole data of a given polymer sample
Forensic Examination Of Fibres Second Edition
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Author : James Robertson
language : en
Publisher: CRC Press
Release Date : 2002-09-11
Forensic Examination Of Fibres Second Edition written by James Robertson and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2002-09-11 with Law categories.
This book is the definitive text for forensic scientists, police and lawyers who may be involved with the use of textile fibres to provide evidence in criminal cases. While covering the subject in detail from recovery of the evidence, through the different stages of laboratory examination, to evaulating the meaning of findings, it is written in such a way that it should be interesting and understandable to the beginner and to the layman, as well as to the expert.
Scientist And The Forger The Second Edition Probing A Turbulent Art World
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Author : Jehane Ragai
language : en
Publisher: World Scientific
Release Date : 2018-01-31
Scientist And The Forger The Second Edition Probing A Turbulent Art World written by Jehane Ragai and has been published by World Scientific this book supported file pdf, txt, epub, kindle and other format this book has been release on 2018-01-31 with Art categories.
In The Scientist and the Forger: Probing a Turbulent Art World the author draws upon an enthralling range of case studies, from Botticelli to Leonardo, Campendonk to Pollock and Chagall to Freud, equipping the reader with a holistic understanding of an art world shaped by fast-moving trends, and increasingly permeated by science. We are taken on a gripping journey, becoming witness to the attempts currently being made to safeguard a partly complicit art market virtually under siege.How can we determine whether it was Leonardo's hand that created Salvator Mundi? How can we prove that a suspected Pollock is a forgery? And how can Man in a Black Cravat be seemingly incontrovertibly attributed to Lucian Freud, despite this artist's adamant refusal to recognize it as one of his own? This book reveals how art historians and scientists collaborate conclusively to authenticate paintings or demonstrate that they are forgeries, and as the enigma of La Bella Principessa continues to baffle, the question remains: do we have enough reason to hope that we shall one day know her true story? Building on the first edition, a more in depth look is taken at some of the greatest scandals to date — with an interpretation of the psychological behavior of Ann Freedman the former president and director of the Knoedler Gallery.
Analytical Pyrolysis Of Synthetic Organic Polymers
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Author : Serban C. Moldoveanu
language : en
Publisher: Elsevier
Release Date : 2005-01-20
Analytical Pyrolysis Of Synthetic Organic Polymers written by Serban C. Moldoveanu and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2005-01-20 with Science categories.
Analytical Pyrolysis of Synthetic Organic Polymers is a follow-up to Analytical Pyrolysis of Natural Organic Polymers, which is volume 20 of the series. The main focus of the book is on practical applications of analytical pyrolysis in synthetic organic polymer identification and characterization. The first part of the book has five chapters including an introduction, a discussion on physico-chemistry of thermal degradation of synthetic polymers and on instrumentation used in analytical pyrolysis, a chapter discussing what type of information can be obtained from analytical pyrolysis, and a chapter dedicated to the analysis and characterization of synthetic polymers.The second part systematically covers the analytical pyrolysis of various classes of synthetic polymers. Some theoretical background for the understanding of polymer structure using analytical pyrolysis is also discussed.* Includes broad coverage of organic synthetic macromolecules* Focuses on physico-chemistry of thermal degradation, and the analytical pyrolysis of various classes of synthetic polymers* Is well written and suitable for both researchers and chemists working in analytical chemistry or in synthetic polymers
Thermal Degradation Of Polymeric Materials
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Author : Krzysztof Pielichowski
language : en
Publisher: iSmithers Rapra Publishing
Release Date : 2005
Thermal Degradation Of Polymeric Materials written by Krzysztof Pielichowski and has been published by iSmithers Rapra Publishing this book supported file pdf, txt, epub, kindle and other format this book has been release on 2005 with Science categories.
Understanding the thermal degradation of polymers is of paramount importance for developing a rational technology of polymer processing and higher-temperature applications. Controlling degradation requires understanding of many different phenomena, including chemical mechanisms, the influence of polymer morphology, the complexities of oxidation chemistry, and the effects of stabilisers, fillers and other additives. This book offers a wealth of information for polymer researchers and processors requiring an understanding of the implications of thermal degradation on material and product performance.
Mass Spectrometry Of Polymers
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Author : Giorgio Montaudo
language : en
Publisher: CRC Press
Release Date : 2001-10-29
Mass Spectrometry Of Polymers written by Giorgio Montaudo and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2001-10-29 with Science categories.
Mass Spectrometry (MS) has rapidly become an indispensable tool in polymer analysis, and modern MS today complements in many ways the structural data provided by Nuclear Magnetic Resonance (NMR) and Infrared (IR) methods. Recent advances have sparked a growing interest in this field and established a need for a summary of progress made and results
Introduction To Polymer Chemistry Second Edition
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Author : Charles E. Carraher Jr.
language : en
Publisher: CRC Press
Release Date : 2011-07-08
Introduction To Polymer Chemistry Second Edition written by Charles E. Carraher Jr. and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2011-07-08 with Technology & Engineering categories.
As the first polymer book to receive the CHOICE Outstanding Academic Title distinction (2007), Introduction to Polymer Chemistry provided undergraduate students with a much-needed, well-rounded presentation of the principles and applications of natural, synthetic, inorganic, and organic polymers. With an emphasis on the environment and green chemistry and materials, this second edition continues that tradition, offering detailed coverage of natural and synthetic giant molecules, inorganic and organic polymers, elastomers, adhesives, coatings, fibers, plastics, blends, caulks, composites, and ceramics. Using simple fundamentals, the author shows how the basic principles of one polymer group can be applied to all of the other groups. He covers synthesis and polymerization reactions, reactivities, techniques for characterization and analysis, energy absorption and thermal conductivity, physical and optical properties, and practical applications. This edition also addresses environmental concerns and green polymeric materials, including biodegradable polymers and microorganisms for synthesizing materials. Brief case studies are woven within the text as historical accounts to illustrate various developments and the societal and scientific contexts in which these changes occurred. Introduction to Polymer Chemistry, Second Edition remains the premier text for understanding the behavior of polymers while offering new material on environmental science. Building on undergraduate work in foundational courses, the text fulfills the American Chemical Society Committee on Professional Training (ACS CPT) in-depth course requirement. It also provides a test bank with upon qualifying course adoption.
Practical Gas Chromatography
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Author : Katja Dettmer-Wilde
language : en
Publisher: Springer
Release Date : 2014-11-05
Practical Gas Chromatography written by Katja Dettmer-Wilde and has been published by Springer this book supported file pdf, txt, epub, kindle and other format this book has been release on 2014-11-05 with Science categories.
Gas chromatography continues to be one of the most widely used analytical techniques, since its applications today expand into fields such as biomarker research or metabolomics. This new practical textbook enables the reader to make full use of gas chromatography. Essential fundamentals and their implications for the practical work at the instrument are provided, as well as details on the instrumentation such as inlet systems, columns and detectors. Specialized techniques from all aspects of GC are introduced ranging from sample preparation, solvent-free injection techniques, and pyrolysis GC, to separation including fast GC and comprehensive GCxGC and finally detection, such as GC-MS and element-specific detection. Various fields of application such as enantiomer, food, flavor and fragrance analysis, physicochemical measurements, forensic toxicology, and clinical analysis are discussed as well as cutting-edge application in metabolomics is covered.