Sample Preparation For Trace Element Analysis

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Sample Preparation For Trace Element Analysis
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Author : Zoltan Mester
language : en
Publisher: Elsevier
Release Date : 2003-12-16
Sample Preparation For Trace Element Analysis written by Zoltan Mester and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2003-12-16 with Science categories.
Following the collection of a sample, every analytical chemist will agree that its subsequent preservation and processing are of paramount importance. The availability of high performance analytical instrumentation has not diminished this need for careful selection of appropriate pretreatment methodologies, intelligently designed to synergistically elicit optimum function from these powerful measurement tools. Sample Preparation for Trace Element Analysis is a modern, comprehensive treatise, providing an account of the state-of-the art on the subject matter. The book has been conceived and designed to satisfy the varied needs of the practicing analytical chemist. It is a multi-author work, reflecting the diverse expertise arising from its highly qualified contributors. The first five chapters deal with general issues related to the determination of trace metals in varied matrices, such as sampling, contamination control, reference materials, calibration and detection techniques. The second part of the book deals with extraction and sampling technologies (totaling 15 chapters), providing theoretical and practical hints for the users on how to perform specific extractions. Subsequent chapters overview seven major representative matrices and the sample preparation involved in their characterization. This portion of the book is heavily based on the preceding chapters dealing with extraction technologies. The last ten chapters are dedicated to sample preparation for trace element speciation.- First title to provide comprehensive sample preparation information, dealing specifically with the analysis of samples for trace elements. - The 39 chapters are authored by international leaders of their fields.
Microwave Assisted Sample Preparation For Trace Element Determination
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Author : Erico Marlon Moraes Flores
language : en
Publisher: Newnes
Release Date : 2014-05-03
Microwave Assisted Sample Preparation For Trace Element Determination written by Erico Marlon Moraes Flores and has been published by Newnes this book supported file pdf, txt, epub, kindle and other format this book has been release on 2014-05-03 with Science categories.
Microwave-Assisted Sample Preparation for Trace Element Analysis describes the principles, equipment, and applications involved in sample preparation with microwaves for trace element analysis. The book covers well-established applications as well as new trends in this field. Hot topics such as sample preparation for speciation, metabolomics, and halogen determination, as well as the alternatives of sample preparation for special samples (for example, carbon nanotubes, polymers, petroleum products), are also discussed. The use of microwaves in sample preparation has increased in recent decades. Several applications of microwaves for sample preparation can be found in the literature for practically all types of sample matrices, especially for the determination of trace elements by atomic spectrometric techniques, safely and cleanly reducing the time involved in this step. Microwave-assisted sample preparation is not only a tool for research but also for routine analysis laboratories; the state-of-the-art in sample preparation in trace element analysis. This book is the only resource for chemists specifically focused on this topic. - The first book to describe the principles, equipment, and applications in microwave-assisted sample preparation - Written by experts in the field who provide a comprehensive overview of the important concepts - Introduces new alternatives and trends in microwave-assisted techniques
Modern Methods For Trace Element Determination
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Author : C. Vandecasteele
language : en
Publisher: John Wiley & Sons
Release Date : 1997-03-06
Modern Methods For Trace Element Determination written by C. Vandecasteele and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 1997-03-06 with Science categories.
Describes the theory, apparatus, performance and usage of modern methods for trace element determination, atomic absorption, emission, fluorescence and mass spectroscopies, x-ray techniques and activation analysis. Attention is given to sample preparation, current calibration procedures and to methods for trace element speciation. Contains in-depth information on relatively new techniques such as ICP-MS and PIXE. All methods are illustrated with authentic examples from the ever-expanding fields of environmental and biological analysis of high purity materials.
Element Analysis Of Biological Samples
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Author : G. Venkatesh Iyengar
language : en
Publisher: CRC Press
Release Date : 2020-11-25
Element Analysis Of Biological Samples written by G. Venkatesh Iyengar and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2020-11-25 with Science categories.
Despite the development of innovative new analytical techniques for biological trace element research, today's trace element investigators face formidable obstacles to obtaining reliable data. This complete reference identifies and assesses the challenges the analyst encounters at each stage of an analysis, and discusses the effects of various techniques on the sample. Three internationally recognized scientists and authors consider the effects of the numerous collection, storage, and sample preparatory techniques used in sample analysis. Proper analytical quality control, including such critical factors as sampling and sample preparation, specimen preservation and storage, and ashing, is examined. The book also looks at sample preparation methods unique to various instruments and speciation chemistry issues, and examines the link between chemical analysis and specimen banking. A previously unrecognized source of error, presampling factors, is also discussed.
Trace Element Analysis In Biological Specimens
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Author : R.F.M. Herber
language : en
Publisher: Elsevier
Release Date : 1994-05-19
Trace Element Analysis In Biological Specimens written by R.F.M. Herber and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 1994-05-19 with Science categories.
The major theme of this book is analytical approaches to trace metal and speciation analysis in biological specimens. The emphasis is on the reliable determination of a number of toxicologically and environmentally important metals. It is essentially a handbook based on the practical experience of each individual author. The scope ranges from sampling and sample preparation to the application of various modern and well-documented methods, including quality assessment and control and statistical treatment of data. Practical advice on avoiding sample contamination is included.In the first part, the reader is offered an introduction into the basic principles and methods, starting with sampling, sample storage and sample treatment, with the emphasis on sample decomposition. This is followed by a description of the potential of atomic absorption spectrometry, atomic emission spectrometry, voltammetry, neutron activation analysis, isotope dilution analysis, and the possibilities for metal speciation in biological specimens. Quality control and all approaches to achieve reliable data are treated in chapters about interlaboratory and intralaboratory surveys and reference methods, reference materials and statistics and data evaluation.The chapters of the second part provide detailed information on the analysis of thirteen trace metals in the most important biological specimens. The following metals are treated in great detail: Aluminium, arsenic, cadmium, chromium, copper, lead, selenium, manganese, nickel, mercury, thallium, vanadium and zinc.The book will serve as a valuable aid for practical analysis in biomedical laboratories and for researchers involved with trace metal and species analysis in clinical, biochemical and environmental research.
Trace Element Analysis Of Food And Diet
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Author : Namik K Aras
language : en
Publisher: Royal Society of Chemistry
Release Date : 2007-10-31
Trace Element Analysis Of Food And Diet written by Namik K Aras and has been published by Royal Society of Chemistry this book supported file pdf, txt, epub, kindle and other format this book has been release on 2007-10-31 with Technology & Engineering categories.
Trace element analysis has a key role to play in quality control of food and diet. This timely book introduces the subject in a practical way - from sampling and the techniques available for trace analysis, to procedures for specific elements and data analysis. Beginning with a brief introduction and discussion of statistical evaluation of data, the subsequent chapter looks at trace analysis in general, with its essentials and terminology. Another section introduces sampling and preparation of foodstuffs such as wheat, potato, vegetables and milk. This is followed by descriptions of the various spectrometric techniques (atomic absorption, atomic emission, atomic fluorescence) that are available. Plasma techniques for both optical emission and mass spectrometry are presented, as are nuclear activation analysis and X-ray methods. A comparison of the various analytical techniques is provided, and a separate chapter handles speciation analysis. Finally, procedures for determining essential and toxic elements such as arsenic, iron, selenium and zinc are suggested, using several recent references. Detailed explanations and a simple format will appeal to laboratory technicians and graduate students, as well as more experienced researchers. Comprehensive coverage, coupled with illustrations and a guide to relevant literature and manufacturers, will make Trace Element Analysis of Food and Diet a valuable source of information for anyone working on analysis of trace elements in food, diet or other biological or environmental samples - particularly food engineers, agricultural scientists and government testing agency employees.
Determination Of Trace Elements
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Author : Zeev B. Alfassi
language : en
Publisher: Wiley-VCH
Release Date : 1994-10-17
Determination Of Trace Elements written by Zeev B. Alfassi and has been published by Wiley-VCH this book supported file pdf, txt, epub, kindle and other format this book has been release on 1994-10-17 with Science categories.
Determination of Trace Elements Edited by Zeev B. Alfassi The best way to determine trace elements! This easy-to-use handbook guides the reader through the maze of all modern analytical operations. Each method is described by an expert in the field. The book highlights the advantages and disadvantages of individual techniques and enables pharmacologists, environmentalists, material scientists, and food industry to select a judicious procedure for their trace element analysis.
Comprehensive Sampling And Sample Preparation
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Author : Josep M. Bayona
language : en
Publisher: Academic Press
Release Date : 2012-12-31
Comprehensive Sampling And Sample Preparation written by Josep M. Bayona and has been published by Academic Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-31 with Science categories.
Comprehensive Sampling and Sample Preparation is a complete treatment of the theory and methodology of sampling in all physical phases and the theory of sample preparation for all major extraction techniques. It is the perfect starting point for researchers and students to design and implement their experiments and support those experiments with quality-reviewed background information. In its four volumes, fundamentals of sampling and sample preparation are reinforced through broad and detailed sections dealing with Biological and Medical, Environmental and Forensic, and Food and Beverage applications. The contributions are organized to reflect the way in which analytical chemists approach a problem. It is intended for a broad audience of analytical chemists, both educators and practitioners of the art and can assist in the preparation of courses as well in the selection of sampling and sample preparation techniques to address the challenges at hand. Above all, it is designed to be helpful in learning more about these topics, as well as to encourage an interest in sampling and sample preparation by outlining the present practice of the technology and by indicating research opportunities. Sampling and Sample preparation is a large and well-defined field in Analytical Chemistry, relevant for many application areas such as medicine, environmental science, biochemistry, pharmacology, geology, and food science. This work covers all these aspects and will be extremely useful to researchers and students, who can use it as a starting point to design and implement their experiments and for quality-reviewed background information There are limited resources that Educators can use to effectively teach the fundamental aspects of modern sample preparation technology. Comprehensive Sampling and Sample Preparation addresses this need, but focuses on the common principles of new developments in extraction technologies rather than the differences between techniques thus facilitating a more thorough understanding Provides a complete overview of the field. Not only will help to save time, it will also help to make correct assessments and avoid costly mistakes in sampling in the process Sample and sample preparation are integral parts of the analytical process but are often less considered and sometimes even completely disregarded in the available literature. To fill this gap, leading scientists have contributed 130 chapters, organized in 4 volumes, covering all modern aspects of sampling and liquid, solid phase and membrane extractions, as well as the challenges associated with different types of matrices in relevant application areas
Isotope Dilution Mass Spectrometry
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Author : J. Ignacio Garcia Alonso
language : en
Publisher: Royal Society of Chemistry
Release Date : 2013
Isotope Dilution Mass Spectrometry written by J. Ignacio Garcia Alonso and has been published by Royal Society of Chemistry this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013 with Science categories.
This is the first textbook to present a comprehensive and instructive view of the theory and applications of this growing technique.