Solid State Nmr Of Polymers


Solid State Nmr Of Polymers
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Solid State Nmr Of Polymers


Solid State Nmr Of Polymers
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Author : L.J. Mathias
language : en
Publisher: Springer Science & Business Media
Release Date : 2013-06-29

Solid State Nmr Of Polymers written by L.J. Mathias and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-06-29 with Technology & Engineering categories.


The chapters in this collection are from papers which were presented at a symposium on solid-state NMR of polymers. A two-part program on available NMR techniques applicable to solid polymer analysis was presented at the 3rd Chemical Congress of North American held in Toronto, Ontario, June 5-10,1988. The program was sponsored by the Division of Polymer Chemistry with support provided by the Division, its Industrial Sponsors, and the Donors of the Petroleum Research Fund administered by the American Chemical Society. Co-organizers included Professor Colin Fyfe of the University of British Columbia (Vancouver, Canada), Professor Hans Spiess of the Max Planck Institut fur Polymerforschung (Mainz, West Germany), and myself. The full-day tutorial, which was free to registered attendees, covered the range of topics. The purpose of the tutorial was to provide a basic introduction to the field so that newcomers to its present and future applications could develop sufficient understanding to learn effectively from the subsequent symposium. The first talk attempted to give listeners a feel for the way a novice spectroscopist can learn to use the various NMR techniques to explore his own areas of interest. Simple experiments can provide unique information about solid polymers that can be useful in interpreting synthetic results and in relating solid-state conformation, morphology and molecular motion to physical properties.



Solid State Nmr Of Polymers


Solid State Nmr Of Polymers
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Author : P. Mirau
language : en
Publisher: iSmithers Rapra Publishing
Release Date : 2001

Solid State Nmr Of Polymers written by P. Mirau and has been published by iSmithers Rapra Publishing this book supported file pdf, txt, epub, kindle and other format this book has been release on 2001 with Nuclear magnetic resonance spectroscopy categories.


NMR spectroscopy has emerged as one of the most important methods for the solid-state characterisation of polymers. This report gives an overview of the methods and applications of NMR to relevant polymer problems with an emphasis on how NMR can be used for materials characterisation and to understand structure-property relationships in polymers. An additional indexed section containing several hundred abstracts from the Rapra Polymer Library database gives useful references for further reading.



Multidimensional Solid State Nmr And Polymers


Multidimensional Solid State Nmr And Polymers
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Author : Klaus Schmidt-Rohr
language : en
Publisher: Elsevier
Release Date : 2012-12-02

Multidimensional Solid State Nmr And Polymers written by Klaus Schmidt-Rohr and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-02 with Science categories.


NMR spectroscopy is the most valuable and versatile analytical tool in chemistry. While excellent monographs exist on high-resolution NMR in liquids and solids, this is the first book to address multidimensional solid-state NMR. Multidimensional techniques enable researchers to obtain detailed information about the structure, dynamics, orientation, and phase separation of solids, which provides the basis of a better understanding of materials properties on the molecular level.Dramatic progress-much of it pioneered by the authors-has been achieved in this area, especially in synthetic polymers. Solid-state NMR now favorably competes with well-established techniques, such as light, x-ray, or neutron scattering, electron microscopy, and dielectric and mechanical relaxation. The application of multidimensional solid-state NMR inevitably involves use of concepts from different fields of science. This book also provides the first comprehensive treatment of both the new experimental techniques and the theoretical concepts needed in more complex data analysis. The text addresses spectroscopists and polymer scientists by treating the subject on different levels; descriptive, technical, and mathematical approaches are used when appropriate. It presents an overview of new developments with numerous experimental examples and illustrations, which will appeal to readers interested in both the information content as well as the potential of solid-state NMR. The book also contains many previously unpublished details that will be appreciated by those who want to perform the experiments. The techniques described are applicable not only to the study of synthetic polymers but to numerous problems in solid-state physics, chemistry, materials science, and biophysics. Key Features * Presents original theories and new perspectives on scattering techniques * Provides a systematic treatment of the whole subject * Gives readers access to previously unpublished material * Includes extensive illustrations



Solid State Nmr Of Polymers


Solid State Nmr Of Polymers
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Author : L. J. Mathias
language : en
Publisher:
Release Date : 2014-01-15

Solid State Nmr Of Polymers written by L. J. Mathias and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2014-01-15 with categories.




Nmr Of Polymers


Nmr Of Polymers
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Author : Frank A. Bovey
language : en
Publisher: Academic Press
Release Date : 1996-11-19

Nmr Of Polymers written by Frank A. Bovey and has been published by Academic Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 1996-11-19 with Technology & Engineering categories.


NMR has made important contributions to our understanding of structure–property relationships in polymers. This book provides an up-to-date and comprehensive overview of the fundamentals of NMR, with applications of multidimensional NMR and the new solution and solid-state methods in polymer science. NMR of Polymers is written by leading authorities for graduate students and professionals in academia and industry. Provides comprehensive overview of NMR in Polymer Science Covers multidimensional NMR Includes new solution and solid state methods Addresses chain conformation and dynamics



Nmr Spectroscopy Of Polymers In Solution And In The Solid State


Nmr Spectroscopy Of Polymers In Solution And In The Solid State
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Author : H. N. Cheng
language : en
Publisher:
Release Date : 2003

Nmr Spectroscopy Of Polymers In Solution And In The Solid State written by H. N. Cheng and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2003 with Science categories.


NMR Spectroscopy of Polymers in Solution and in the Solid State includes 31 chapters, which are divided into the following sections: overview, solid state NMR of polymers, solution NMR of synthetic polymers, solution NMR of biopolymers, combined NMR-separation techniques, and dynamics of polymers in solution. NMR Spectroscopy of Polymers in Solution and in the Solid State brings together a variety of papers on both solution and solid state NMR in one convenient volume. Practicing NMR spectroscopists, students, and other newcomers to the field will benefit from the book's dual coverage.



Solid State Nmr Of Polymers


Solid State Nmr Of Polymers
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Author : T. Asakura
language : en
Publisher: Elsevier
Release Date : 1998-08-03

Solid State Nmr Of Polymers written by T. Asakura and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 1998-08-03 with Science categories.


In polymer science and technology, the advanced development of various new polymer materials with excellent properties and functions is desirable. For this purpose it is necesary to determine the exact relationship between physical properties and molecular structure-dynamics with powerful techniques. One such technique is solid state NMR. Recently, high resolution NMR studies of solids have been realized by using advanced pulse and mechanical techniques, which has resulted in a variety of structural and dynamical information on polymer systems. Solid state NMR has provided characteristic information which cannot be obtained by other spectroscopic methods. This book is divided into two parts. The first part covers the principles of NMR, important NMR parameters such as chemical shifts, relaxation times, dipolar interactions, quadrupolar interactions, pulse techniques and new NMR methods. In the second part, applications of NMR to a variety of polymer systems in the solid state are described. Features of this book: • Contains an up-to-date and comprehensive account of solid state NMR of polymers by leading researchers in the field • Provides a compilation of solid state NMR of polymers, which makes it an ideal reference book for both NMR researchers and general polymer scientists. This book will be of interest to the NMR community, and will be invaluable for both the beginner and the expert.



Current Developments In Solid State Nmr Spectroscopy


Current Developments In Solid State Nmr Spectroscopy
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Author : Norbert Müller
language : en
Publisher: Springer Science & Business Media
Release Date : 2013-04-17

Current Developments In Solid State Nmr Spectroscopy written by Norbert Müller and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-04-17 with Science categories.


Why to apply solid-state NMR? - By now, we should have learned that NMR is mainly used for the study of molecules in solution, while x-ray diffraction is the method of choice for solids. Based on this fact, the two recent 'NMR-Nobelprizes' went indeed into the liquid phase: my own one eleven years ago, and particularly the most recent one to Kurt Wuthrich. His prize is beyond any doubts very well justified. His contribution towards the study of biomolecules in solution, in their native (or almost native) environment is truly monumental. We all will profit from it indirectly when one of our future diseases will be cured with better drugs, based on the insightful knowledge gained through liquid-state NMR. Two fields of NMR are still left out of the Nobel Prize game: magnetic reso nance imaging (MRI) and solid-state NMR. The disrespect for MRI in Stockholm is particularly difficult to understand; but this is not a subject to be discussed at the present place. Solid-state NMR is the third of the three great fields of NMR, powerful already today and very promising for the near future.



Characterization Of Polymers In The Solid State I Part A Nmr And Other Spectroscopic Methods Part B Mechanical Methods


Characterization Of Polymers In The Solid State I Part A Nmr And Other Spectroscopic Methods Part B Mechanical Methods
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Author : H.H. Kausch
language : en
Publisher: Springer
Release Date : 2014-03-12

Characterization Of Polymers In The Solid State I Part A Nmr And Other Spectroscopic Methods Part B Mechanical Methods written by H.H. Kausch and has been published by Springer this book supported file pdf, txt, epub, kindle and other format this book has been release on 2014-03-12 with Technology & Engineering categories.


Pt. A: NMR and other Spectroscopic Methods. Pt. B: Mechanical Methods



Solid State Nmr Spectroscopy For Biopolymers


Solid State Nmr Spectroscopy For Biopolymers
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Author : Hazime Saitô
language : en
Publisher: Springer Science & Business Media
Release Date : 2006-08-05

Solid State Nmr Spectroscopy For Biopolymers written by Hazime Saitô and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2006-08-05 with Science categories.


‘‘Biopolymers’’ are polymeric materials of biological origin, including globular, membrane, and fibrous proteins, polypeptides, nucleic acids, po- saccharides, lipids, etc. and their assembly, although preference to respe- ive subjects may be different among readers who are more interested in their biological significance or industrial and/or medical applications. Nevert- less, characterizing or revealing their secondary structure and dynamics may be an equally very important and useful issue for both kinds of readers. Special interest in revealing the 3D structure of globular proteins, nucleic acids, and peptides was aroused in relation to the currently active Structural Biology. X-ray crystallography and multidimensional solution NMR sp- troscopy have proved to be the standard and indispensable means for this purpose. There remain, however, several limitations to this end, if one intends to expand its scope further. This is because these approaches are not always straightforward to characterize fibrous or membrane proteins owing to extreme difficulty in crystallization in the former, and insufficient spectral resolution due to sparing solubility or increased effective molecular mass in the presence of surrounding lipid bilayers in the latter.