Supercritical Fluid Chromatography
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Modern Supercritical Fluid Chromatography
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Author : Larry M. Miller
language : en
Publisher: John Wiley & Sons
Release Date : 2019-12-12
Modern Supercritical Fluid Chromatography written by Larry M. Miller and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019-12-12 with Science categories.
Explains why modern supercritical fluid chromatography (SFC) is the leading "green" analytical and purification separations technology. Modern supercritical fluid chromatography (SFC) is the leading method used to analyze and purify chiral and achiral chemical compounds, many of which are pharmaceuticals, pharmaceutical candidates, and natural products including cannabis-related compounds. This book covers current SFC instrumentation as it relates to greater robustness, better reproducibility, and increased analytical sensitivity. Modern Supercritical Fluid Chromatography: Carbon Dioxide Containing Mobile Phases covers the history, instrumentation, method development and applications of SFC. The authors provided readers with an overview of analytical and preparative SFC equipment, stationary phases, and mobile phase choices. Topics covered include: Milestones of Supercritical Fluid Chromatography; Physical Properties of Supercritical Fluids; Instrumentation for SFC; Detection in SFC; Achiral SFC Method Development; Chiral SFC Method Development; and Preparative Scale SFC. The book also includes highlights of modern applications of SFC in the final chapters—namely pharmaceuticals, consumer products, foods, polymers, petroleum-related mixtures, and cannabis—and discusses the future of SFC. Provides a clear explanation of the physical and chemical properties of supercritical fluids, which gives the reader a better understanding of the basis for improved performance in SFC compared to HPLC and GC Describes the advantages of SFC as a green alternative to HPLC and GC for the analysis of both polar, water-soluble, and non-polar analytes Details both achiral and chiral SFC method development, including modifiers, additives, the impact of temperature and pressure, and stationary phase choices Details why SFC is the premier modern preparative chromatographic technique used to purify components of mixtures for subsequent uses, both from performance and economic perspectives Covers numerous detectors, with an emphasis on SFC-MS, SFC-UV, and SFC-ELSD (evaporative light scattering detection) Describes the application of SFC to numerous high-value application areas Modern Supercritical Fluid Chromatography: Carbon Dioxide Containing Mobile Phases will be of great interest to professionals, students, and professors involved in analytical, bioanalytical, separations science, medicinal, petroleum, and environmental chemistries. It will also appeal to pharmaceutical scientists, natural-product scientists, food and consumer-products scientists, chemical engineers, and managers in these areas.
Practical Supercritical Fluid Chromatography And Extraction
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Author : Thomas Caudell
language : en
Publisher: Routledge
Release Date : 2018-05-08
Practical Supercritical Fluid Chromatography And Extraction written by Thomas Caudell and has been published by Routledge this book supported file pdf, txt, epub, kindle and other format this book has been release on 2018-05-08 with Science categories.
An exploration of fundamental as well as practical aspects of supercritical fluid chromatography and extraction. It addresses topics such as: packed columns in SFC; detection in SFC; supercritical fluid chromatography/mass spectroscopy; and evaporative light scattering detection in SFC.
Analysis With Supercritical Fluids Extraction And Chromatography
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Author : Bernd Wenclawiak
language : en
Publisher: Springer Science & Business Media
Release Date : 2012-12-06
Analysis With Supercritical Fluids Extraction And Chromatography written by Bernd Wenclawiak and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-06 with Science categories.
The use of supercritical fluids in analytical chemistry is still grow ing. More and more analysts are discovering the favorable advan tages for a number of applications. Especially supercritical fluid extraction (SFE) has attracted a lot of interest in recent years due to its simplicity. Supercritical fluid chromatography (SFC) has become better established and the development of this technique has been accelerated by the many applications with capillary col umns which have been published in the literature. At first SFC equipment was based on instruments commonly used for liquid chromatography, and the first commercial in struments were derived from this technology. However, capillary columns can be much more easily interfaced to gas chromatogra phy equipment especially to the detectors commonly used for Oc. Many stationary phases both for packed micro columns and capillary columns have been designed for SFC purposes extending this technology to LC and OC. The most common fluid applied in SFC and SFE is carbon dioxide. The advantages of supercritical CO , such as having dif 2 fusivity like a gas and solvating power depending on temperature and pressure, are also valid for other fluids and modified fluids. Both properties are valuable for sample extraction and extraction selectivity.
Supercritical Fluid Chromatography With Patked Columns
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Author : Klaus Anton
language : en
Publisher: CRC Press
Release Date : 1997-09-19
Supercritical Fluid Chromatography With Patked Columns written by Klaus Anton and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 1997-09-19 with Science categories.
From the analytical to industrial preparative scale, this work provides a praxis-oriented overview of packed column supercritical fluid chromatography. It discusses and evaluates established applications and techniques, up-to-date and promising developments, and commercial instrumentation devices for use in industry. The book also reveals possibilities for problem solving and future innovations.
Supercritical Fluid Chromatography
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Author : Colin F. Poole
language : en
Publisher: Elsevier
Release Date : 2017-02-16
Supercritical Fluid Chromatography written by Colin F. Poole and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2017-02-16 with Science categories.
Supercritical fluid chromatography (SFC) is a rapidly developing laboratory technique for the separation and identification of compounds in mixtures. Significant improvements in instrumentation have rekindled interest in SFC in recent years and enhanced its standing in the scientific community. Many scientists are familiar with column liquid chromatography and its strengths and weaknesses, but the possibilities brought to the table by SFC are less well-known and are underappreciated. Supercritical Fluid Chromatography is a thorough and encompassing reference that defines the concept of contemporary practice in SFC and how it should be implemented in laboratory science. Given the changes that have taken place in SFC, this book presents contemporary aspects and applications of the technique and introduces SFC as a natural solution in the larger field of separation science. The focus on state-of-the-art instrumental SFC distinguishes this work as the go-to reference work for those interested in implementing the technique at an advanced level. Edited and authored by world-leading chromatography experts Provides comprehensive coverage of SFC in a single source Extensive referencing facilitates identification of key research developments More than 200 figures and tables aid in the retention of key concepts
Supercritical Fluid Chromatography
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Author : Gérard Rossé
language : en
Publisher: Walter de Gruyter GmbH & Co KG
Release Date : 2018-12-17
Supercritical Fluid Chromatography written by Gérard Rossé and has been published by Walter de Gruyter GmbH & Co KG this book supported file pdf, txt, epub, kindle and other format this book has been release on 2018-12-17 with Science categories.
Supercritical Fluid Chromatography (SFC) provides a timely overview of SFC application areas which were unimaginable just a decade ago. This two-volume series opens with an overview of the history and expectant future of SFC and continues with recent applications in the pharmaceutical industry and other fascinating areas of science. SFC has found its place in the pharmaceutical industry with an increasing body of applications for chiral and achiral molecules in both the research and development phases of the drug discovery process. As illustrated in this two-volume series, the current interest in SFC extends well beyond the pharmaceutical industry. Chapters encompassing applications for polar and non-polar mixtures of importance are covering widely disparate areas in substance abuse, natural products including cannabinoids, bioactive lipids, flavor and fragrance. With its broad balance and coverage, this two-volume book constitutes a unique educational platform to students and scientists for many years to come. The major objective of this book editions is to inspire and stimulate readers to continue exploring the possibilities of exploiting supercritical fluids as a particular media for analysis, purifications and synthesis
Supercritical Fluid Chromatography For The Analysis Of Nitroaromatics Nitramines And Nitrate Esters
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Author : Paul H. Miyares
language : en
Publisher:
Release Date : 1992
Supercritical Fluid Chromatography For The Analysis Of Nitroaromatics Nitramines And Nitrate Esters written by Paul H. Miyares and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1992 with Chromatographic analysis categories.
Supercritical Fluid Chromatography And Micro Hplc
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Author : M. Yoshioka
language : en
Publisher: VSP
Release Date : 1989
Supercritical Fluid Chromatography And Micro Hplc written by M. Yoshioka and has been published by VSP this book supported file pdf, txt, epub, kindle and other format this book has been release on 1989 with Science categories.
First published in 1988. Routledge is an imprint of Taylor & Francis, an informa company.
Supercritical Fluid Chromatography
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Author : Gregory K. Webster
language : en
Publisher: CRC Press
Release Date : 2014-02-04
Supercritical Fluid Chromatography written by Gregory K. Webster and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2014-02-04 with Medical categories.
Analytical chemists in the pharmaceutical industry are always looking for more-efficient techniques to meet the analytical challenges of today’s pharmaceutical industry. One technique that has made steady advances in pharmaceutical analysis is supercritical fluid chromatography (SFC). SFC is meeting the chromatography needs of the industry by providing efficient and selective testing capabilities on the analytical and preparative scale. The supercritical fluid mobile phase, consisting mainly of CO2, facilitates cost reduction costs and helps the industry in meeting green chemistry standards. This book provides a comprehensive overview of the use of SFC in pharmaceutical analysis. Supercritical Fluid Chromatography reviews the use of SFC in drug-discovery applications and describes its application in drug development. When a drug is developed and brought to market, it is tested many times for impurities and degradants, enantiomeric purity, and analytical and preparative isolations—it is tested during discovery and development and for under-regulated and unregulated methodologies. The book describes the use of SFC for each of these applications and discusses more in-depth topics, such as the use of SFC in mass spectrometric and polarographic detection. The book also sheds light on the role of SFC in drug development from natural products and the advancement of SFC with new technologies and its use in pilot-scale operations as a chromatographic technique.
Modern Supercritical Fluid Chromatography
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Author : Curt M. White
language : en
Publisher:
Release Date : 1988
Modern Supercritical Fluid Chromatography written by Curt M. White and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1988 with Science categories.