Advances In Solid Phase Microextraction
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Advances In Solid Phase Microextraction
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Author : Attilio Naccarato
language : en
Publisher:
Release Date : 2020
Advances In Solid Phase Microextraction written by Attilio Naccarato and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2020 with categories.
Analysis imposes substantial challenges, especially when dealing with analytes present at trace levels in complex matrices. Although modern instrumentation has simplified analyses and makes them more reliable, its use is only the last step of the whole analytical process. On the other hand, sample preparation still represents the bottleneck in many analytical methods and often requires the use of extensive protocols before instrumental analysis. Solid-phase microextraction (SPME) is a well-established sample-prep technique for simultaneous extraction and pre-concentration of compounds from a variety of matrices. Given its compliance with the principles of green analytical chemistry, as well as the simplicity, versatility, and availability of different formats, SPME addresses several challenges associated with the traditional sample preparation approaches and allows for a substantial streamlining of the analytical workflow. This book is the reprint of a Special Issue that includes six contributions provided by some of the world's leading research groups in the field and focuses on recent advances in solid-phase microextraction.
Solid Phase Microextraction
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Author : Gangfeng Ouyang
language : en
Publisher: Springer
Release Date : 2016-11-24
Solid Phase Microextraction written by Gangfeng Ouyang and has been published by Springer this book supported file pdf, txt, epub, kindle and other format this book has been release on 2016-11-24 with Science categories.
This book offers comprehensive information on the developments and applications of the solid phase microextraction (SPME) technique. The first part of the book briefly introduces readers to the fundamentals of SPME, while subsequent sections describe the applications of SPME technique in detail, including environmental analysis (air, water, soil/sediments), food analysis (volatile/nonvolatile compounds), and bioanalysis (plants, animal tissues, body fluids). The advantages and future challenges of the SPME technique are also discussed. Including recent research advances and further developments of SPME, the book offers a practical reference guide and a valuable resource for researchers and users of SPME techniques. The target audience includes analytical chemists, environmental scientists, biological scientists, material scientists, and analysts, as well as students at universities/institutes in related fields. Dr. Gangfeng Ouyang is a Professor at the School of Chemistry and Chemical Engineering, Sun Yat-sen University, China. Dr. Ruifen Jiang is an Associate Professor at the School of Environment, Jinan University, China.
Solid Phase Microextraction
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Author : Warrane Verreau
language : en
Publisher:
Release Date : 2017
Solid Phase Microextraction written by Warrane Verreau and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2017 with Extraction (Chemistry) categories.
In Chapter One, the specific patterns and applications of micro extraction techniques in bionalysis are reviewed. The various micro-extraction techniques can be classified into two rudimentary categories: solid-phase micro-extraction and liquid-phase micro-extraction, which are derived from conventional solid-phase extraction and liquid-liquid extraction, correspondingly. Next, an overview of the application of solid-phase micro-extraction in assessing target chemical families in different alcoholic beverages is provided. The results re-count the last 10 years of scientific publications, concentrating on the extraction conditions used for investigating different compounds in wines, beer and spirits according to the chemical families. Additionally, the authors discuss optimisation strategies for achieving accurate quantification. Chapter Three presents research on solid phase micro-extraction its advantages. Since solid phase micro-extraction was presented in the early 1990s, there has been an increase in research on new methodical solutions in many research facilities around the world that could potentially increase use of this technique. In Chapter Four, modern uses of new sorbent coatings in solid-phase micro-extraction are analysed. The combination of molecularly imprinted polymers with solid phase micro-extraction results in a possible technique for sample preparation, predominantly considering their described success in recent literature.
Handbook Of Solid Phase Microextraction
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Author : Janusz Pawliszyn
language : en
Publisher: Elsevier
Release Date : 2011-11-29
Handbook Of Solid Phase Microextraction written by Janusz Pawliszyn and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2011-11-29 with Science categories.
The relatively new technique of solid phase microextraction (SPME) is an important tool to prepare samples both in the lab and on-site. SPME is a "green" technology because it eliminates organic solvents from analytical laboratory and can be used in environmental, food and fragrance, and forensic and drug analysis. This handbook offers a thorough background of the theory and practical implementation of SPME. SPME protocols are presented outlining each stage of the method and providing useful tips and potential pitfalls. In addition, devices and fiber coatings, automated SPME systems, SPME method development, and In Vivo applications are discussed. This handbook is essential for its discussion of the latest SPME developments as well as its in depth information on the history, theory, and practical application of the method. Practical application of Solid Phase Microextraction methods including detailed steps Provides history of extraction methods to better understand the process Suitable for all levels, from beginning student to experienced practitioner
Solid Phase Microextraction
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Author : Sue Ann Wercinski
language : en
Publisher: CRC Press
Release Date : 1999-07-09
Solid Phase Microextraction written by Sue Ann Wercinski and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 1999-07-09 with Science categories.
An explanation of proven methods of chemical analysis, focusing on the myriad applications of solid phase microextraction (SPME) to laboratories performing high-sample throughput, quick sample turnaround time, low detection levels, and dirty sample matrices. It supplies commentary on developments in SPME technology from its inventor, Janusz Pawliszyn.
Solid Phase Microextraction
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Author : Janusz Pawliszyn
language : en
Publisher: John Wiley & Sons
Release Date : 1997-04-21
Solid Phase Microextraction written by Janusz Pawliszyn and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 1997-04-21 with Science categories.
Gesetzliche Auflagen und ökonomische Erwägungen steigern den Bedarf an Propenpräparations- und -extraktionstechniken, die ohne toxische organische Lösungsmittel auskommen. Die hier erstmals in Buchform veröffentlichte Festphasen-Mikroextraktion (SPME) ist ein neuartiges Verfahren, das diesen Anforderungen entspricht und gegenwärtig apparativ umgesetzt wird. Der Erfinder selbst, ein international anerkannter Pionier auf dem Gebiet der lösungsmittelfreien Extraktion, erklärt theoretische Hintergründe und praktische Anwendungsmöglichkeiten. SPME ist einfach, kostengünstig, automatisierbar, zeit- und analytsparend. Interessant für Analytiker in Industrie und Forschung, für Spurenanalytik, Umwelt- und pharmazeutische Chemie.
Solid Phase Microextraction
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Author : Constantinos K. Zacharis
language : en
Publisher: MDPI
Release Date : 2020-02-07
Solid Phase Microextraction written by Constantinos K. Zacharis and has been published by MDPI this book supported file pdf, txt, epub, kindle and other format this book has been release on 2020-02-07 with Science categories.
This book covers the most recent research activities and achievements regarding to the solid phase microextraction (SPME) technique. It is a powerful sample preparation tool that addresses the new challenges of analytical laboratories. Among others, its fundamental applications involved the sampling of volatile compounds from various matrixes. The demonstrated topics ranged from aroma characterization of various fruits, essential oils to the utilization of SPME for in-tube extraction and isolation of selected compounds from complex samples followed by state-of-the-art analytical techniques.
Sample Preparation In Lc Ms Bioanalysis
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Author : Wenkui Li
language : en
Publisher: John Wiley & Sons
Release Date : 2019-03-12
Sample Preparation In Lc Ms Bioanalysis written by Wenkui Li and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019-03-12 with Science categories.
Revised and Expanded Handbook Provides Comprehensive Introduction and Complete Instruction for Sample Preparation in Vital Category of Bioanalysis Following in the footsteps of the previously published Handbook of LC-MS Bioanalysis, this book is a thorough and timely guide to all important sample preparation techniques used for quantitative Liquid Chromatography–Mass Spectrometry (LC-MS) bioanalysis of small and large molecules. LC-MS bioanalysis is a key element of pharmaceutical research and development, post-approval therapeutic drug monitoring, and many other studies used in human healthcare. While advances are continually being made in key aspects of LC-MS bioanalysis such as sensitivity and throughput, the value of research/study mentioned above is still heavily dependent on the availability of high-quality data, for which sample preparation plays the critical role. Thus, this text provides researchers in industry, academia, and regulatory agencies with detailed sample preparation techniques and step-by-step protocols on proper extraction of various analyte(s) of interest from biological samples for LC-MS quantification, in accordance with current health authority regulations and industry best practices. The three sections of the book with a total of 26 chapters cover topics that include: Current basic sample preparation techniques (e.g., protein precipitation, liquid-liquid extraction, solid-phase extraction, salting-out assisted liquid-liquid extraction, ultracentrifugation and ultrafiltration, microsampling, sample extraction via electromembranes) Sample preparation techniques for uncommon biological matrices (e.g., tissues, hair, skin, nails, bones, mononuclear cells, cerebrospinal fluid, aqueous humor) Crucial aspects of LC-MS bioanalytical method development (e.g., pre-analytical considerations, derivation strategies, stability, non-specific binding) in addition to sample preparation techniques for challenging molecules (e.g., lipids, peptides, proteins, oligonucleotides, antibody-drug conjugates) Sample Preparation in LC-MS Bioanalysis will prove a practical and highly valuable addition to the reference shelves of scientists and related professionals in a variety of fields, including pharmaceutical and biomedical research, mass spectrometry, and analytical chemistry, as well as practitioners in clinical pharmacology, toxicology, and therapeutic drug monitoring.
Solid Phase Microextraction
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Author : Constantinos K. Zacharis
language : en
Publisher:
Release Date : 2020
Solid Phase Microextraction written by Constantinos K. Zacharis and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2020 with Chemistry categories.
This book covers the most recent research activities and achievements regarding to the solid phase microextraction (SPME) technique. It is a powerful sample preparation tool that addresses the new challenges of analytical laboratories. Among others, its fundamental applications involved the sampling of volatile compounds from various matrixes. The demonstrated topics ranged from aroma characterization of various fruits, essential oils to the utilization of SPME for in-tube extraction and isolation of selected compounds from complex samples followed by state-of-the-art analytical techniques.
Bioanalytical Separations
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Author :
language : en
Publisher: Elsevier
Release Date : 2003-09-03
Bioanalytical Separations written by and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2003-09-03 with Science categories.
Bioanalytical Separations is volume 4 of the multi-volume series, Handbook of Analytical Separations, providing reviews of analytical separation methods and techniques used for the determination of analytes across a whole range of applications. The theme for this volume is bioanalysis, in this case specifically meaning the analysis of drugs and their metabolites in biological fluids. - Discusses new developments in instrumentation and methods of analyzing drugs and their metabolites in biological fluids - Provides guidance to the different methods, their relative value to the user, and the advantages and pitfalls of their use - Future trends are identified, in terms of the potential impact of new technologies