Experimental Approaches Of Nmr Spectroscopy I

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Experimental Approaches Of Nmr Spectroscopy I

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Author : The NMR Society of Japan
language : en
Publisher: Springer Nature
Release Date : 2025-03-14

Experimental Approaches Of Nmr Spectroscopy I written by The NMR Society of Japan and has been published by Springer Nature this book supported file pdf, txt, epub, kindle and other format this book has been release on 2025-03-14 with Science categories.

This book describes advanced developments in the methodology and applications of NMR spectroscopy in the life science and materials science fields. In this book, new experimental methods and new NMR research fields are presented with chapters on the structure of membrane proteins, in cell NMR, and Electro-Mechano-Optical NMR is added. Experts in the field have contributed an exciting range of topics that cover recent advances in high-pressure NMR, selectively isotope-aided NMR, ultrafast MAS NMR, dynamic nuclear polarization (DNP) NMR, optical and microwave irradiation NMR. This book emphasizes the experimental details for new researchers to use NMR spectroscopy and pick up the potentials of this technique. It is also designed for those who are involved in either developing the technique or expanding the NMR application field by applying them to specific samples. The Nuclear Magnetic Resonance Society of Japan has organized this book not only for NMR users of Japan but also for readers worldwide who are interested in using NMR spectroscopy extensively.

Experimental Approaches Of Nmr Spectroscopy

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Author : The Nuclear Magnetic Resonance Society of Japan
language : en
Publisher: Springer
Release Date : 2017-11-23

Experimental Approaches Of Nmr Spectroscopy written by The Nuclear Magnetic Resonance Society of Japan and has been published by Springer this book supported file pdf, txt, epub, kindle and other format this book has been release on 2017-11-23 with Science categories.

This book describes the advanced developments in methodology and applications of NMR spectroscopy to life science and materials science. Experts who are leaders in the development of new methods and applications of life and material sciences have contributed an exciting range of topics that cover recent advances in structural determination of biological and material molecules, dynamic aspects of biological and material molecules, and development of novel NMR techniques, including resolution and sensitivity enhancement. First, this book particularly emphasizes the experimental details for new researchers to use NMR spectroscopy and pick up the potentials of NMR spectroscopy. Second, the book is designed for those who are involved in either developing the technique or expanding the NMR application fields by applying them to specific samples. Third, the Nuclear Magnetic Resonance Society of Japan has organized this book not only for NMR members of Japan but also for readers worldwide who are interested in using NMR spectroscopy extensively.

Nuclear Magnetic Resonance Spectroscopy

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Author : Joseph B. Lambert
language : en
Publisher: John Wiley & Sons
Release Date : 2019-01-04

Nuclear Magnetic Resonance Spectroscopy written by Joseph B. Lambert and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019-01-04 with Science categories.

Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.

Experimental Approaches Of Nmr Spectroscopy Ii

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Author : The NMR Society of Japan
language : en
Publisher: Springer Nature
Release Date : 2025-03-14

Experimental Approaches Of Nmr Spectroscopy Ii written by The NMR Society of Japan and has been published by Springer Nature this book supported file pdf, txt, epub, kindle and other format this book has been release on 2025-03-14 with Science categories.

This book describes advanced developments in the methodology and applications of NMR spectroscopy in the life science and materials science fields. In this book, experts in the NMR field have contributed an exciting range of topics that cover recent advances in structural and dynamic aspects of material molecules such as silk fibrils, polymer materials and organic light-emitting diodes, and biological molecules such as natural products, glycoproteins, and ribonucleic acid (RNA). This book emphasizes the experimental details for new researchers to use NMR spectroscopy and pick up the potential of this technique. It is also designed for those who are involved in either developing the technique or expanding the NMR application field by applying them to specific samples. The Nuclear Magnetic Resonance Society of Japan has organized this book not only for NMR members of Japan but also for readers worldwide who are interested in using NMR spectroscopy extensively.

High Resolution Nmr Techniques In Organic Chemistry

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Author : T. Claridge
language : en
Publisher: Elsevier
Release Date : 1999-12-24

High Resolution Nmr Techniques In Organic Chemistry written by T. Claridge and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 1999-12-24 with Science categories.

From the initial observation of proton magnetic resonance in water and in paraffin, the discipline of nuclear magnetic resonance has seen unparalleled growth as an analytical method. Modern NMR spectroscopy is a highly developed, yet still evolving, subject which finds application in chemistry, biology, medicine, materials science and geology. In this book, emphasis is on the more recently developed methods of solution-state NMR applicable to chemical research, which are chosen for their wide applicability and robustness. These have, in many cases, already become established techniques in NMR laboratories, in both academic and industrial establishments. A considerable amount of information and guidance is given on the implementation and execution of the techniques described in this book.

Experimental Approaches Of Nmr Spectroscopy Ii

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Author : The NMR Society of Japan
language : en
Publisher: Springer
Release Date : 2024-12-23

Experimental Approaches Of Nmr Spectroscopy Ii written by The NMR Society of Japan and has been published by Springer this book supported file pdf, txt, epub, kindle and other format this book has been release on 2024-12-23 with Science categories.

This book describes advanced developments in the methodology and applications of NMR spectroscopy in the life science and materials science fields. In this book, experts in the NMR field have contributed an exciting range of topics that cover recent advances in structural and dynamic aspects of material molecules such as silk fibrils, polymer materials and organic light-emitting diodes, and biological molecules such as natural products, glycoproteins, and ribonucleic acid (RNA). This book emphasizes the experimental details for new researchers to use NMR spectroscopy and pick up the potential of this technique. It is also designed for those who are involved in either developing the technique or expanding the NMR application field by applying them to specific samples. The Nuclear Magnetic Resonance Society of Japan has organized this book not only for NMR members of Japan but also for readers worldwide who are interested in using NMR spectroscopy extensively.

Biological Nmr Spectroscopy

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Author : John L. Markley
language : en
Publisher: Oxford University Press
Release Date : 1997-01-30

Biological Nmr Spectroscopy written by John L. Markley and has been published by Oxford University Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 1997-01-30 with Medical categories.

This book presents a critical assessment of progress on the use of nuclear magnetic resonance spectroscopy to determine the structure of proteins, including brief reviews of the history of the field along with coverage of current clinical and in vivo applications. The book, in honor of Oleg Jardetsky, one of the pioneers of the field, is edited by two of the most highly respected investigators using NMR, and features contributions by most of the leading workers in the field. It will be valued as a landmark publication that presents the state-of-the-art perspectives regarding one of today's most important technologies.

Spectroscopic Methods In Mineralogy And Material Sciences

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Author : Grant Henderson
language : en
Publisher: Walter de Gruyter GmbH & Co KG
Release Date : 2014-11-21

Spectroscopic Methods In Mineralogy And Material Sciences written by Grant Henderson and has been published by Walter de Gruyter GmbH & Co KG this book supported file pdf, txt, epub, kindle and other format this book has been release on 2014-11-21 with Science categories.

Spectroscopic Methods in Mineralogy and Material Science covers significant advances in the technological aspects and applications of spectroscopic and microscopic techniques used in the Earth and Materials Sciences. The current volume compliments the now classic Volume 18, Spectroscopic Methods in Mineralogy and Geology, which became an essential resource to many scientists and educators for the past two decades. This volume updates techniques covered in Volume 18, and introduces new techniques available for probing the secrets of Earth materials, such as X-ray Raman and Brillouin spectroscopy. Other important topics including Transmission Electron Microscopy (TEM) and Atomic Force Microscopy (AFM) are also covered.

Optimising Nmr Spectroscopy Through Method And Software Development

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Author : Jonathan Yong
language : en
Publisher: Springer Nature
Release Date : 2024-01-09

Optimising Nmr Spectroscopy Through Method And Software Development written by Jonathan Yong and has been published by Springer Nature this book supported file pdf, txt, epub, kindle and other format this book has been release on 2024-01-09 with Science categories.

This book provides a comprehensive overview of Nuclear Magnetic Resonance (NMR) theory, its applications, and advanced techniques to improve the quality and speed of NMR data acquisition. In this book, the author expands his outstanding Ph.D. thesis and provides a valuable resource for researchers, professionals, and students in the field of NMR spectroscopy. The book covers quantum mechanics basics, and topics like density operators, pulse sequences, 1D pulse acquisition, INEPT (Insensitive nuclei enhancement by polarization transfer), product operators, and 2D NMR principles. It also explores innovative experiments like States HSQC (Heteronuclear Single Quantum Coherence) and echo-antiecho HSQC with gradients. In the subsequent chapters, the author discusses Pure Shift NMR, including PSYCHE (Pure Shift Yielded by Chirp Excitation) and its optimizations, such as waveform parameterization and time-reversal methods. The 'Discrete PSYCHE' approach and Ultrafast PSYCHE-iDOSY (Diffusion-ordered spectroscopy) are also highlighted. This book presents the POISE (Parameter Optimisation by Iterative Spectral Evaluation) software for real-time NMR experiment optimization, including pulse width calibration and Ernst angle optimization, and demonstrates applications across various NMR experiments. Lastly, the book examines accelerated 2D NMR data collection and the NOAH (NMR by Ordered Acquisition using 1H detection) supersequences, emphasizing automated pulse program creation using GENESIS (GENEration of Supersequences In Silico). Covered NMR experiments include 13C sensitivity-enhanced HSQC, 15N HMQC (Heteronuclear Multiple Quantum Coherence), dual HSQC, HSQC-TOCSY (Total Correlation Spectroscopy), HMBC (Heteronuclear Multiple Bond Correlation), and ADEQUATE (Adequate Sensitivity Double-Quantum Spectroscopy).

Nmr Methods For Characterization Of Synthetic And Natural Polymers

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Author : Rongchun Zhang
language : en
Publisher: Royal Society of Chemistry
Release Date : 2019-07-29

Nmr Methods For Characterization Of Synthetic And Natural Polymers written by Rongchun Zhang and has been published by Royal Society of Chemistry this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019-07-29 with Science categories.

Since the introduction of FT-NMR spectroscopy around five decades ago, NMR has achieved significant advances in hardware and methodologies, accompanied with the enhancement of spectral resolution and signal sensitivity. Rapid developments in the polymers field mean that accurate and quantitative characterization of polymer structures and dynamics is the keystone for precisely regulating and controlling the physical and chemical properties of the polymer. This book specifically focuses on NMR investigation of complex polymers for the polymer community as well as NMR spectroscopists, and will push the development of both fields. It covers the latest advances, for example high field DNP and ultrafast MAS methodologies, and show how these novel NMR methods characterize various synthetic and natural polymers.