Experimental Approaches Of Nmr Spectroscopy Ii
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Experimental Approaches Of Nmr Spectroscopy Ii
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Author : The NMR Society of Japan
language : en
Publisher: Springer
Release Date : 2024-12-23
Experimental Approaches Of Nmr Spectroscopy Ii written by The NMR Society of Japan and has been published by Springer this book supported file pdf, txt, epub, kindle and other format this book has been release on 2024-12-23 with Science categories.
This book describes advanced developments in the methodology and applications of NMR spectroscopy in the life science and materials science fields. In this book, experts in the NMR field have contributed an exciting range of topics that cover recent advances in structural and dynamic aspects of material molecules such as silk fibrils, polymer materials and organic light-emitting diodes, and biological molecules such as natural products, glycoproteins, and ribonucleic acid (RNA). This book emphasizes the experimental details for new researchers to use NMR spectroscopy and pick up the potential of this technique. It is also designed for those who are involved in either developing the technique or expanding the NMR application field by applying them to specific samples. The Nuclear Magnetic Resonance Society of Japan has organized this book not only for NMR members of Japan but also for readers worldwide who are interested in using NMR spectroscopy extensively.
Experimental Approaches Of Nmr Spectroscopy
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Author : The Nuclear Magnetic Resonance Society of Japan
language : en
Publisher: Springer
Release Date : 2017-11-23
Experimental Approaches Of Nmr Spectroscopy written by The Nuclear Magnetic Resonance Society of Japan and has been published by Springer this book supported file pdf, txt, epub, kindle and other format this book has been release on 2017-11-23 with Science categories.
This book describes the advanced developments in methodology and applications of NMR spectroscopy to life science and materials science. Experts who are leaders in the development of new methods and applications of life and material sciences have contributed an exciting range of topics that cover recent advances in structural determination of biological and material molecules, dynamic aspects of biological and material molecules, and development of novel NMR techniques, including resolution and sensitivity enhancement. First, this book particularly emphasizes the experimental details for new researchers to use NMR spectroscopy and pick up the potentials of NMR spectroscopy. Second, the book is designed for those who are involved in either developing the technique or expanding the NMR application fields by applying them to specific samples. Third, the Nuclear Magnetic Resonance Society of Japan has organized this book not only for NMR members of Japan but also for readers worldwide who are interested in using NMR spectroscopy extensively.
Nmr From Spectra To Structures
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Author : Terence N. Mitchell
language : en
Publisher: Springer Science & Business Media
Release Date : 2013-04-17
Nmr From Spectra To Structures written by Terence N. Mitchell and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-04-17 with Science categories.
NMR spectroscopy is one of the most important analytical methods available today. This practice-oriented textbook shows how NMR spectra is used in the education of organic structures. The emphasis is on practical rather than on theoretical aspects, which are treated only briefly. NMR- From Spectra to Strucures is a textbook providing an ideal practical guide to today ́s standard NMR experiments for students and laboratory personnel. The set of 35 graded problems includes not only the 1D NMR spectra (proton, carbon, DEPT/APT) but, for the first time in a textbook, also the most important 2D spectra (H,H and C,H correlation).
Nuclear Magnetic Resonance Spectroscopy
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Author : Joseph B. Lambert
language : en
Publisher: John Wiley & Sons
Release Date : 2019-01-04
Nuclear Magnetic Resonance Spectroscopy written by Joseph B. Lambert and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019-01-04 with Science categories.
Combines clear and concise discussions of key NMR concepts with succinct and illustrative examples Designed to cover a full course in Nuclear Magnetic Resonance (NMR) Spectroscopy, this text offers complete coverage of classic (one-dimensional) NMR as well as up-to-date coverage of two-dimensional NMR and other modern methods. It contains practical advice, theory, illustrated applications, and classroom-tested problems; looks at such important ideas as relaxation, NOEs, phase cycling, and processing parameters; and provides brief, yet fully comprehensible, examples. It also uniquely lists all of the general parameters for many experiments including mixing times, number of scans, relaxation times, and more. Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition begins by introducing readers to NMR spectroscopy - an analytical technique used in modern chemistry, biochemistry, and biology that allows identification and characterization of organic, and some inorganic, compounds. It offers chapters covering: Experimental Methods; The Chemical Shift; The Coupling Constant; Further Topics in One-Dimensional NMR Spectroscopy; Two-Dimensional NMR Spectroscopy; Advanced Experimental Methods; and Structural Elucidation. Features classical analysis of chemical shifts and coupling constants for both protons and other nuclei, as well as modern multi‐pulse and multi-dimensional methods Contains experimental procedures and practical advice relative to the execution of NMR experiments Includes a chapter-long, worked-out problem that illustrates the application of nearly all current methods Offers appendices containing the theoretical basis of NMR, including the most modern approach that uses product operators and coherence-level diagrams By offering a balance between volumes aimed at NMR specialists and the structure-determination-only books that focus on synthetic organic chemists, Nuclear Magnetic Resonance Spectroscopy: An Introduction to Principles, Applications, and Experimental Methods, 2nd Edition is an excellent text for students and post-graduate students working in analytical and bio-sciences, as well as scientists who use NMR spectroscopy as a primary tool in their work.
Modern Nmr Approaches To The Structure Elucidation Of Natural Products
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Author : Antony Williams
language : en
Publisher: Royal Society of Chemistry
Release Date : 2016-12-12
Modern Nmr Approaches To The Structure Elucidation Of Natural Products written by Antony Williams and has been published by Royal Society of Chemistry this book supported file pdf, txt, epub, kindle and other format this book has been release on 2016-12-12 with Science categories.
The Ghanian plant Cryptolepis sanguinolenta is the source of a series of fascinating indoloquinoline alkaloids. The most unusual member of this alkaloid series was initially proposed to be a spiro nonacyclic structure, named cryptospirolepine, and was elucidated in 1993 based on the technologies available at that time. There were, however, several annoying attributes to the structure that bothered analysts for the ensuing 22 years. During the two decades that followed the initial work there have been enormous developments in NMR technology. Using new experimental approaches, specifically homodecoupled 1,1- and 1,n-HD-ADEQUATE NMR experiments developed in 2014, the structure of only a 700 μg sample of cryptospirolepine has been revised and is shown on the cover of this volume. The confluence of the NMR technological and methodological advances that allowed the revision of the structure of cryptospirolepine using a submilligram sample seems a fitting example for this book, which is dedicated to the NMR characterization of various classes of natural products. Volume 2 considers data processing and algorithmic based analyses tailored to natural product structure elucidation and reviews the application of NMR to the analysis of a series of different natural product families including marine natural products, terpenes, steroids, alkaloids and carbohydrates. Volume 1 discusses contemporary NMR approaches including optimized and future hardware and experimental approaches to obtain both the highest quality and most appropriate spectral data for analysis. These books, bringing together acknowledged experts, uniquely focus on the combination of experimental approaches and modern hardware and software applied to the structure elucidation of natural products. The volumes will be an essential resource for NMR spectroscopists, natural product chemists and industrial researchers working on natural product analysis or the characterization of impurities and degradation products of pharmaceuticals that can be as scarce as natural product samples.
Experimental Approaches Of Nmr Spectroscopy I
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Author : The NMR Society of Japan
language : en
Publisher: Springer
Release Date : 2024-11-11
Experimental Approaches Of Nmr Spectroscopy I written by The NMR Society of Japan and has been published by Springer this book supported file pdf, txt, epub, kindle and other format this book has been release on 2024-11-11 with Science categories.
This book describes advanced developments in the methodology and applications of NMR spectroscopy in the life science and materials science fields. In this book, new experimental methods and new NMR research fields are presented with chapters on the structure of membrane proteins, in cell NMR, and Electro-Mechano-Optical NMR is added. Experts in the field have contributed an exciting range of topics that cover recent advances in high-pressure NMR, selectively isotope-aided NMR, ultrafast MAS NMR, dynamic nuclear polarization (DNP) NMR, optical and microwave irradiation NMR. This book emphasizes the experimental details for new researchers to use NMR spectroscopy and pick up the potentials of this technique. It is also designed for those who are involved in either developing the technique or expanding the NMR application field by applying them to specific samples. The Nuclear Magnetic Resonance Society of Japan has organized this book not only for NMR users of Japan but also for readers worldwide who are interested in using NMR spectroscopy extensively.
Modern Nmr Approaches To The Structure Elucidation Of Natural Products
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Author : Antony J. Williams
language : en
Publisher: Royal Society of Chemistry
Release Date : 2016
Modern Nmr Approaches To The Structure Elucidation Of Natural Products written by Antony J. Williams and has been published by Royal Society of Chemistry this book supported file pdf, txt, epub, kindle and other format this book has been release on 2016 with Science categories.
The first volume in a two-part set that discusses contemporary NMR approaches for the structure elucidation of natural products. It covers optimized hardware and experimental approaches.
Nmr Spectroscopy Techniques Second Edition
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Author : Martha Bruch
language : en
Publisher: CRC Press
Release Date : 1996-03-05
Nmr Spectroscopy Techniques Second Edition written by Martha Bruch and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 1996-03-05 with Science categories.
This work elucidates the power of modern nuclear magnetic resonance (NMR) techniques to solve a wide range of practical problems that arise in both academic and industrial settings. This edition provides current information regarding the implementation and interpretation of NMR experiments, and contains material on: three- and four-dimensional NMR; the NMR analysis of peptides, proteins, carbohydrates and oligonucleotides; and more.
Solid State Nmr Iv Methods And Applications Of Solid State Nmr
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Author : B. Blümich
language : en
Publisher: Springer Science & Business Media
Release Date : 2012-12-06
Solid State Nmr Iv Methods And Applications Of Solid State Nmr written by B. Blümich and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-06 with Science categories.
Solid-State NMR is a branch of Nuclear Magnetic Resonance which is presently experiencing a phase of strongly increasing popularity. The most striking evidence is the large number of contributions from Solid-State Resonance at NMR meetings, approaching that ofliquid state resonance. Important progress can be observed in the areas of methodological developments and applications to organic and inorganic matter. One volume devoted to more or less one of each of these areas has been published in the preceding three issues. This volume can be considered an addendum to this series. Selected methods and applications of Solid-State NMR are featured in three chapters. The first one treats the recoupling of dipolar interactions in solids, which are averaged by fast sample rotation. Following an introduction to effective Hamiltonians and Floquet theory, different types of experiment such as rotary resonance, dipolar chemical shift correlation spectroscopy, rotational resonance and multipulse recoupling are treated in the powerful Floquet formalism. In the second chapter, the different approaches to line narrowing of quadrupolar nuclei are reviewed in a. consistent formulation of double resonance (DaR) and dynamic angle spinning (DAS). Practical aspects of probe design are considered as well as advanced 2D experiments, sensitivity enhancement techniques, and spinning sideband manipulations. The use of such techniques dramatically increases the number of nuclei which can be probed in high resolution NMR spectroscopy. The final chapter describes new experimental approaches and results of structural studies of noncrystalline solids.
50 And More Essential Nmr Experiments
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Author : Matthias Findeisen
language : en
Publisher: John Wiley & Sons
Release Date : 2013-07-30
50 And More Essential Nmr Experiments written by Matthias Findeisen and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-07-30 with Science categories.
This book is the perfect link for learning how to perform the experiments after only having studied theory. In eight chapters more than 50 essential NMR experiments are described in detail. Special focus is put on the organic set of NMR spectra (1H, 13C-APT, COSY, NOESY, HSQC and HMBC). Different chapters deal with advanced organic NMR, selective methods, heteronuclear NMR, relaxation and diffusion measurements, organic applications and maintenance. Every experiment has a section providing the reader with the purpose and scope of the specific experiment. Every experiment is concluded with the spectrum as it is obtained under the conditions described. Questions and comments enable the reader to check their understanding. The authors are very experienced and the whole book is in full color, which enhances the reading experience and makes the spectra and other figures easier to understand. This book is strongly recommended for all students and researchers who are involved in the structural elucidation of chemical compounds both in practical education and in pursuing research, in particular if they handle an NMR spectrometer.