Quantitative Chromatographic Analysis

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Quantitative Chromatographic Analysis
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Author : Thomas Beesley
language : en
Publisher: CRC Press
Release Date : 2000-12-06
Quantitative Chromatographic Analysis written by Thomas Beesley and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2000-12-06 with Science categories.
Highlights critical factors involved in successful chromatographic analysis. Details analytical procedures; outlining sample preparation, collection, transportation, and storage. Provides step-by-step guidelines for producing analytical reports.
Quantitative Gas Chromatography For Laboratory Analyses And On Line Process Control
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Author : G. Guiochon
language : en
Publisher: Elsevier
Release Date : 1988-06-01
Quantitative Gas Chromatography For Laboratory Analyses And On Line Process Control written by G. Guiochon and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 1988-06-01 with Science categories.
Here is an invaluable new book on quantitative gas chromatography which explains how the method can - or should - be used for accurate and precise analysis. Gas chromatography is firmly established as one of the few major methods for the quantitative analysis of complex mixtures. It is fast, accurate and inexpensive, with a broad range of applications. It has however become very complex and involved: over 200 stationary phases, more than 10 detector principles and several very different column types are available from among the catalogs of over 100 manufacturers and major retailers. The progressive changes in the nature of gas chromatography have created new needs for information which are not satisfied by the literature presently available.This book provides a complete discussion of all the problems involved in the achievement of quantitative analysis by gas chromatography, whether in the research laboratory, in the routine analysis laboratory or in process control. For this reason the presentation of theoretical concepts has been limited to the essential, while extensive explanations have been devoted to the various steps involved in the derivation of precise and accurate data. This starts with the selection of the instrumentation and column, continues with the choice of optimum experimental conditions, then calibration and ends with the use of correct procedures for data acquisition and calculations. Finally, there is almost always a way to reduce errors and an entire chapter deals with this single issue. Numerous relevant examples are presented.The first part of the book presents the theoretical background, simple enough to be understood by all analytical chemists, but still complete and up-to-date. It discusses the problems of flow dynamics, retention and band broadening. The changes in band profile associated with column overloading are explained without much recourse to mathematics. The second part describes the gas chromatograph and discusses the properties of each of its parts: gas flow and pressure controller sampling system, oven, column switching valves, detectors. The different implementations, their advantages and drawbacks are discussed and compared. In addition, three chapters present packed column technology, open tubular column technology and some sophisticated new phase systems, respectively. The new phase systems described use adsorbents, modified by coating or grafting organic phase, and carrier gases containing vapors which are sorbed by the stationary phase and modify it, such as steam. The third part discusses the applications in qualitative and quantitative analysis. Calibration, peak integration, sources of errors arising from the various parts of the instrument as well as from the measurement process itself are carefully described in four detailed chapters. Methods to carry out accurate and precise analysis are presented. A last chapter is devoted to process control analysis and gives a number of detailed examples of applications. A lexicon explaining the most important chromatographic terms and a detailed index complete the book.This is a book which no chemical analyst should be without. It should be on the library shelf of all universities, instrument companies and any laboratory and plant where gas chromatography is used.
Quantitative Analysis By Gas Chromatography Second Edition
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Author : Josef P Novák
language : en
Publisher: CRC Press
Release Date : 1987-12-18
Quantitative Analysis By Gas Chromatography Second Edition written by Josef P Novák and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 1987-12-18 with Science categories.
Quantitative Analysis Using Chromatographic Techniques
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Author : Elena Katz
language : en
Publisher:
Release Date : 1987-02-27
Quantitative Analysis Using Chromatographic Techniques written by Elena Katz and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1987-02-27 with Science categories.
This is the only book that covers only quantitative techniques of all chromatography methods. Contributors, experts in the field, present general concepts applicable to all types of analyses performed by chromatographic techniques, and treat in detail principles of quantitative detection and sources of error in data processing procedures. Chapters cover liquid chromatography, gas chromatography, thin-layer chromatography, detection methods, detector performance, data handling procedures, and automation procedures. Included is discussion of chromatographic applications in physical chemistry and in pharmaceutical analysis.
Quantitative Analysis By Gas Chromatography
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Author : Josef P. Nov-Ak
language : en
Publisher: Marcel Dekker Incorporated
Release Date : 1975-06-01
Quantitative Analysis By Gas Chromatography written by Josef P. Nov-Ak and has been published by Marcel Dekker Incorporated this book supported file pdf, txt, epub, kindle and other format this book has been release on 1975-06-01 with Science categories.
Quantitative Analysis Using Chromatographic Techniques
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Author : Katz E.
language : en
Publisher:
Release Date : 1987
Quantitative Analysis Using Chromatographic Techniques written by Katz E. and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1987 with categories.
Chromatographic Analysis Of Pharmaceuticals
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Author : John A. Adamovics
language : en
Publisher: Routledge
Release Date : 2017-09-29
Chromatographic Analysis Of Pharmaceuticals written by John A. Adamovics and has been published by Routledge this book supported file pdf, txt, epub, kindle and other format this book has been release on 2017-09-29 with Science categories.
Updated and revised throughout. Second Edition explores the chromatographic methods used for the measurement of drugs, impurities, and excipients in pharmaceutical preparations--such as tablets, ointments, and injectables. Contains a 148-page table listing the chromatographic data of over 1300 drugs and related substances--including sample matrix analyzed, sample handling procedures, column packings, mobile phase, mode of detection, and more.
Practice Of High Performance Liquid Chromatography
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Author : Heinz Engelhardt
language : en
Publisher: Springer Science & Business Media
Release Date : 2012-12-06
Practice Of High Performance Liquid Chromatography written by Heinz Engelhardt and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-06 with Science categories.
During its short 20 year history High Performance Liquid Chro matography (HPLC) has won itself a firm place amongst the instrumental methods of analysis. HPLC has caused a revolution in biological and pharmaceutical chemistry. Approximately two thirds of the publications on HPLC are concerned with problems from this area of life science. Biotechnology, where it is necessary to isolate substances from complicated mixtures, is likely to give further impetus to the dissemination of modern liquid chromatog raphy in columns, particularly on the preparative scale. This book presents, by means of examples, the application of HPLC to various fields, as well as fundamental discussions of chromatographic methods. The quality of the analytical result is decisively dependent on the qualities of the equipment employed (by Colin, Guiochon, and Martin). Especially the demands are discussed that are placed on the components of the instrument including those for data acquisition and processing. The section on "quantitative analy sis" (by ABhauer, Ullner) covers besides the principles also the problems of ensuring the quality of the data in detail. The basic problems arising by enlarging the sample size to preparative di mensions and the requirements put on the aparatus are discussed in the section on "preparative applications" (by Wehrli).
Quantitative Analysis By Gas Chromatography
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Author : Josef Novak
language : en
Publisher:
Release Date : 1988
Quantitative Analysis By Gas Chromatography written by Josef Novak and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1988 with categories.
Lipid Chromatographic Analysis
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Author : Takayuki Shibamoto
language : en
Publisher: CRC Press
Release Date : 1993-12-14
Lipid Chromatographic Analysis written by Takayuki Shibamoto and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 1993-12-14 with Science categories.
Focusing on state-of-the-art gas chromatography (GC) and high-performance liquid chromatography, this guide discusses the theories behind, and applications of, the latest developments in chromatographic techniques - assessing the strengths and limitations of each methodology.;Presenting many detection methods for the first time, Lipid Chromatographic Analysis: provides a review of conventional column and thin-layer chromatography; examines a new GC technique to detect plasmalogen phospholipids; outlines a supercritical fluid chromatography for lipids; details the first systematic description of a microanalytical procedure for cholesterol and related compounds; explains a GC analysis of lipid breakdown products for monitoring biological processes such as ageing, carcinogenesis and mutagenesis; and describes techniques that allow for the simultaneous analysis of non-polar and polar lipids.