Solid Sample Analysis With The Mass Spectrometer
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Solid Sample Analysis With The Mass Spectrometer
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Author : Kellex Corporation
language : en
Publisher:
Release Date : 1951
Solid Sample Analysis With The Mass Spectrometer written by Kellex Corporation and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1951 with Mass spectrometers categories.
Trace Analysis By Mass Spectrometry
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Author : Arthur J. Ahearn
language : en
Publisher: Elsevier
Release Date : 2012-12-02
Trace Analysis By Mass Spectrometry written by Arthur J. Ahearn and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-02 with Science categories.
Trace Analysis by Mass Spectrometry deals with trace analysis of solids and liquids by mass spectrometric techniques. Topics include the physics and techniques of electrical discharge ion sources, transmission of ions through double focusing mass spectrometers, and detection and measurement of ions by ion-sensitive plates. The ion sources used are principally electrical discharge type sources. This book is comprised of 14 chapters. The first several chapters focus on the basic physics of electrical discharge ion sources, double focusing mass spectrometry, and the measurement of arrays of mass resolved ion beams by electrical detection methods and with ion sensitive emulsions. The discussion then shifts to the problem of obtaining the chemical composition of the recorded mass resolved ion sample and relating this composition to that of the original sample. The chapters that follow describe specific techniques for analyzing special samples such as insulators, powders, microsamples, biological materials, reactive and low melting point substances, radioactive materials, and gases in solids. The remaining chapters include the use of laser ion sources in the analysis of solids and the analysis of surfaces particularly with sputter ion sources. This book will be of interest to students and practitioners of physics and chemistry.
Symposium On Chemical Analysis Of Inorganic Solids By Means Of The Mass Spectrometer
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Author : American Society for Testing Materials
language : en
Publisher:
Release Date : 1953
Symposium On Chemical Analysis Of Inorganic Solids By Means Of The Mass Spectrometer written by American Society for Testing Materials and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1953 with Chemistry, Analytic categories.
Solid Sample Analysis
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Author : Ulrich Kurfürst
language : en
Publisher: Springer Science & Business Media
Release Date : 2013-04-17
Solid Sample Analysis written by Ulrich Kurfürst and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-04-17 with Science categories.
The analysis of solid materials by introducing solid test sampies directly into the graphite furnace of an atomic absorption spectrometer must be regarded as a powerful analytical approach. Even if it is - of course - not the "ultimate method". After three decades of development, the instrumentation and the methodology are available to apply solid sampling successfully for the analysis of almost every material. Moreover, several tasks cannot be solved using other analytical methods as neatly as they can using direct solid sampling. The conventional methods work more or less satisfactorily, so why do we sug gest applying solid sampling much more extensively than it is today? To begin with, the features pointed out time and again should be named: Rapidity of the analytical procedure, low susceptibility to analyte loss or contamination, very smallquantities can be analyzed, and expenditure on instrumentation and per sonell is also low. These properties are examined and the necessary conditions are discussed (Chapter 1) as are the analytical tasks (Chapter 6) for which use of this method is advantageous. Other features that are often overlooked are just as important: The simplicity of the analytical procedures allows the analyst to main tain an intimate relationship with the original scientific task that has to be solved with the analysis. Furthermore, the considerable reduction of working place haz ards and pollution by avoiding the use of chemical reagents must nowadays be assessed as a feature as important as the others.
Acceleration And Automation Of Solid Sample Treatment
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Author : J.L. Luque García
language : en
Publisher: Elsevier
Release Date : 2002-08-09
Acceleration And Automation Of Solid Sample Treatment written by J.L. Luque García and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2002-08-09 with Science categories.
This book aims to provide scientists with information about a series of techniques that can be used with a view to facilitating the transformation of the sample to an appropriate state for subsequent detection or quantitation of its components of interest. The techniques dealt with range from the very simple ones (e.g. freeze-drying) to other more complex ones (e.g. glow discharge and laser-induced breakdown sampling). This is the first compilation ever on the subjects of acceleration of solid sample pretreatment; automation of solid sample pretreatment; and integration of solid sample pretreatment and detection. Readers will find here the information required to compare and select the best choice for each sample treatment need and ways to facilitate or automate the most complex and time-consuming step of the analytical process when solid samples are involved.
Secondary Ion Mass Spectroscopy Of Solid Surfaces
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Author : V. T. Cherepin
language : en
Publisher: CRC Press
Release Date : 2020-04-28
Secondary Ion Mass Spectroscopy Of Solid Surfaces written by V. T. Cherepin and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2020-04-28 with Science categories.
This volume is devoted to the physics, instrumentation and analytical methods of secondary ion mass spectroscopy (SIMS) in relation to solid surfaces. It describes modern models of secondary ion formation and the factors influencing sensitivity of measurements and the range of applications. All the main parts of SIMS instruments are discussed in detail. Emphasising practical applications the book also considers the methods and analytical procedures for constitutional analysis of solids --- including metals, semiconductors, organic and biological samples. Methods of depth profiling, spatially multidimensional analysis and study of processes at the surface, such as adsorption, catalysis and oxidation, are given along with the application of SIMS in combination with other methods of surface analysis.
Solid Sample Analysis
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Author : Ulrich Kurfürst
language : en
Publisher: Springer Science & Business Media
Release Date : 1998-03-18
Solid Sample Analysis written by Ulrich Kurfürst and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 1998-03-18 with Science categories.
The direct determination of elements in solid samples by atomspectrometric methods without prior digestion is in many cases more efficient and reliable, faster, easier, more cost-effective and less time-consuming than other methods. In this first book on the topic the authors describe concisely all instrumental and methodological features, including calibration, influences from the matrix or sample inhomogeneities, optimization, data analysis and measurement uncertainty. Special chapters deal with GF-AAS, slurry injection, ETV-ICP-AES/MS coupling. The authors' aim to deliver all their experience in a way that enables the spectroscopists to develop their own solid sampling based methods makes this book an unvaluable source for AAS- and AES-practitioners.
Medical Applications Of Mass Spectrometry
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Author : Karoly Vekey
language : en
Publisher: Elsevier
Release Date : 2011-08-11
Medical Applications Of Mass Spectrometry written by Karoly Vekey and has been published by Elsevier this book supported file pdf, txt, epub, kindle and other format this book has been release on 2011-08-11 with Science categories.
Mass spectrometry is fast becoming an indispensable field for medical professionals. The mass spectrometric analysis of metabolites and proteins promises to revolutionize medical research and clinical diagnostics. As this technology rapidly enters the medical field, practicing professionals and students need to prepare to take full advantage of its capabilities. Medical Applications of Mass Spectrometry addresses the key issues in the medical applications of mass spectrometry at the level appropriate for the intended readership. It will go a long way to help the utilization of mass spectrometry in medicine.The book comprises five parts. A general overview is followed by a description of the basic sampling and separation methods in analytical chemistry. In the second part a solid foundation in mass spectrometry and modern techniques of data analysis is presented. The third part explains how mass spectrometry is used in exploring various classes of biomolecules, including proteins and lipids. In the fourth section mass spectrometry is introduced as a diagnostic tool in clinical treatment, infectious pathogen research, neonatal diagnostics, cancer, brain and allergy research, as well as in various fields of medicine: cardiology, pulmonology, neurology, psychiatric diseases, hemato-oncology, urologic diseases, gastrointestinal diseases, gynecology and pediatrics. The fifth part covers emerging applications in biomarker discovery and in mass spectrometric imaging. * Provides a broad look at how the medical field is benefiting from advances in mass spectrometry.* Guides the reader from basic principles and methods to cutting edge applications.* There is NO comparable book on the market to fill this fast growing field.
Organic Trace Analysis
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Author : Reinhard Nießner
language : en
Publisher: Walter de Gruyter GmbH & Co KG
Release Date : 2017-08-07
Organic Trace Analysis written by Reinhard Nießner and has been published by Walter de Gruyter GmbH & Co KG this book supported file pdf, txt, epub, kindle and other format this book has been release on 2017-08-07 with Science categories.
"Organic Trace Analysis" presents the basics of trace analysis, from sample preparation to the measurement: Students are introduced to statistical evaluation, quality control technologies, sampling and preparation of organic traces, as well as to enrichment and separation of samples. Spectroscopic techniques as chromatography, capillary electrophoresis, mass spectrometry, and receptor-based bioanalysis are presented in detail.
Sample Preparation In Lc Ms Bioanalysis
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Author : Wenkui Li
language : en
Publisher: John Wiley & Sons
Release Date : 2019-03-12
Sample Preparation In Lc Ms Bioanalysis written by Wenkui Li and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019-03-12 with Science categories.
Revised and Expanded Handbook Provides Comprehensive Introduction and Complete Instruction for Sample Preparation in Vital Category of Bioanalysis Following in the footsteps of the previously published Handbook of LC-MS Bioanalysis, this book is a thorough and timely guide to all important sample preparation techniques used for quantitative Liquid Chromatography–Mass Spectrometry (LC-MS) bioanalysis of small and large molecules. LC-MS bioanalysis is a key element of pharmaceutical research and development, post-approval therapeutic drug monitoring, and many other studies used in human healthcare. While advances are continually being made in key aspects of LC-MS bioanalysis such as sensitivity and throughput, the value of research/study mentioned above is still heavily dependent on the availability of high-quality data, for which sample preparation plays the critical role. Thus, this text provides researchers in industry, academia, and regulatory agencies with detailed sample preparation techniques and step-by-step protocols on proper extraction of various analyte(s) of interest from biological samples for LC-MS quantification, in accordance with current health authority regulations and industry best practices. The three sections of the book with a total of 26 chapters cover topics that include: Current basic sample preparation techniques (e.g., protein precipitation, liquid-liquid extraction, solid-phase extraction, salting-out assisted liquid-liquid extraction, ultracentrifugation and ultrafiltration, microsampling, sample extraction via electromembranes) Sample preparation techniques for uncommon biological matrices (e.g., tissues, hair, skin, nails, bones, mononuclear cells, cerebrospinal fluid, aqueous humor) Crucial aspects of LC-MS bioanalytical method development (e.g., pre-analytical considerations, derivation strategies, stability, non-specific binding) in addition to sample preparation techniques for challenging molecules (e.g., lipids, peptides, proteins, oligonucleotides, antibody-drug conjugates) Sample Preparation in LC-MS Bioanalysis will prove a practical and highly valuable addition to the reference shelves of scientists and related professionals in a variety of fields, including pharmaceutical and biomedical research, mass spectrometry, and analytical chemistry, as well as practitioners in clinical pharmacology, toxicology, and therapeutic drug monitoring.