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Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction


Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction
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Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction


Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction
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Author : AJM Hubert
language : en
Publisher: University of Warwick
Release Date : 2019-09-25

Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction written by AJM Hubert and has been published by University of Warwick this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019-09-25 with Science categories.


We explore the capability of digital-large angle convergent beam electron diffraction (D-LACBED) data for the structural refinement of single crystals. To achieve this, we use three materials as test cases. We use corundum for atomic position refi nement, copper and gallium arsenide for Debye-Waller factor (DWF) re finement. D-LACBED patterns are found to be extremely sensitive to atomic position, within 0.4 pm of reference X-ray values. The patterns are less sensitive to DWF (using the independent atom model - IAM) but nonetheless give good agreement to X-ray and Mossbauer radiation values for copper. We find the IAM to be insufficient for accurate refinement of gallium arsenide due to the influence of previously suggested strong anharmonicity and bonding within the material. Finally, we use simulation to explore the sensitivity of D-LACBED patterns through most re fineable structural parameters, providing context to the aforementioned results. During the analysis we see that higher g-vector patterns within the D-LACBED data may be more sensitive to structural parameters in general.



Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction Patterns


Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction Patterns
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Author : A. J. M. Hubert
language : en
Publisher:
Release Date : 2019

Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction Patterns written by A. J. M. Hubert and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019 with categories.




Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction Patterns


Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction Patterns
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Author : Alexander James Morley Hubert
language : en
Publisher:
Release Date : 2019

Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction Patterns written by Alexander James Morley Hubert and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019 with Crystals categories.




Convergent Beam Electron Diffraction Ii


Convergent Beam Electron Diffraction Ii
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Author : Michiyoshi Tanaka
language : en
Publisher:
Release Date : 1988

Convergent Beam Electron Diffraction Ii written by Michiyoshi Tanaka and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1988 with Crystallography categories.




Cumulated Index Medicus


Cumulated Index Medicus
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Author :
language : en
Publisher:
Release Date : 1989

Cumulated Index Medicus written by and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1989 with Medicine categories.




International Tables For Crystallography Volume B


International Tables For Crystallography Volume B
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Author : U. Shmueli
language : en
Publisher: John Wiley & Sons
Release Date : 2008-08-25

International Tables For Crystallography Volume B written by U. Shmueli and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2008-08-25 with Science categories.


International Tables for Crystallography is the definitive resource and reference work for crystallography and structural science. Volume B presents accounts of the numerous aspects of reciprocal space in crystallographic research. This volume is a vital addition to the library of scientists engaged in crystal structure determination, crystallographic computing, crystal physics and other fields of crystallographic research. Graduate students specializing in crystallography will find much material suitable for self-study and a rich source of references to the relevant literature. New to this edition: A new chapter on modern extensions of the Ewald method for Coulomb interactions in crystals. Three new sections on electron diffraction and electron microscopy in structure determination, describing point-group and space-group determination by convergent-beam electron diffraction, three-dimensional reconstruction, and single-particle reconstruction. Substantial revisions to the chapters on space-group representations in reciprocal space, direct methods, Patterson and molecular replacement techniques, and disorder diffuse scattering More information on the series can be found at: http://it.iucr.org



International Tables For Crystallography Volume B


International Tables For Crystallography Volume B
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Author : Uri Shmueli
language : en
Publisher: Springer Science & Business Media
Release Date : 2008-08-27

International Tables For Crystallography Volume B written by Uri Shmueli and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2008-08-27 with Science categories.


International Tables for Crystallography are no longer available for purchase from Springer. For further information please contact Wiley Inc. (follow the link on the right hand side of this page). Volume B presents accounts of the numerous aspects of reciprocal space in crystallographic research. After an introductory chapter, Part 1 presents the reader with an account of structure-factor formalisms, an extensive treatment of the theory, algorithms and crystallographic applications of Fourier methods, and fundamental as well as advanced treatments of symmetry in reciprocal space. In Part 2, these general accounts are followed by detailed expositions of crystallographic statistics, the theory of direct methods, Patterson techniques, isomorphous replacement and anomalous scattering, and treatments of the role of electron microscopy and diffraction in crystal structure determination, including applications of direct methods to electron crystallography. Part 3 deals with applications of reciprocal space to molecular geometry and `best'-plane calculations, and contains a treatment of the principles of molecular graphics and modelling and their applications. A convergence-acceleration method of importance in the computation of approximate lattice sums is presented and the part concludes with a discussion of the Ewald method. Part 4 contains treatments of various diffuse-scattering phenomena arising from crystal dynamics, disorder and low dimensionality (liquid crystals), and an exposition of the underlying theories and/or experimental evidence. Polymer crystallography and reciprocal-space images of aperiodic crystals are also treated. Part 5 of the volume contains introductory treatments of the theory of the interaction of radiation with matter (dynamical theory) as applied to X-ray, electron and neutron diffraction techniques. The simplified trigonometric expressions for the structure factors in the 230 three-dimensional space groups, which appeared in Volume I of International Tables for X-ray Crystallography, are now given in Appendix 1.4.3 to Chapter 1.4 of this volume. Volume B is a vital addition to the library of scientists engaged in crystal structure determination, crystallographic computing, crystal physics and other fields of crystallographic research. Graduate students specializing in crystallography will find much material suitable for self-study and a rich source of references to the relevant literature.



Transmission Electron Microscopy


Transmission Electron Microscopy
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Author : C. Barry Carter
language : en
Publisher: Springer
Release Date : 2016-08-24

Transmission Electron Microscopy written by C. Barry Carter and has been published by Springer this book supported file pdf, txt, epub, kindle and other format this book has been release on 2016-08-24 with Technology & Engineering categories.


This text is a companion volume to Transmission Electron Microscopy: A Textbook for Materials Science by Williams and Carter. The aim is to extend the discussion of certain topics that are either rapidly changing at this time or that would benefit from more detailed discussion than space allowed in the primary text. World-renowned researchers have contributed chapters in their area of expertise, and the editors have carefully prepared these chapters to provide a uniform tone and treatment for this exciting material. The book features an unparalleled collection of color figures showcasing the quality and variety of chemical data that can be obtained from today’s instruments, as well as key pitfalls to avoid. As with the previous TEM text, each chapter contains two sets of questions, one for self assessment and a second more suitable for homework assignments. Throughout the book, the style follows that of Williams & Carter even when the subject matter becomes challenging—the aim is always to make the topic understandable by first-year graduate students and others who are working in the field of Materials Science Topics covered include sources, in-situ experiments, electron diffraction, Digital Micrograph, waves and holography, focal-series reconstruction and direct methods, STEM and tomography, energy-filtered TEM (EFTEM) imaging, and spectrum imaging. The range and depth of material makes this companion volume essential reading for the budding microscopist and a key reference for practicing researchers using these and related techniques.



Chemical Abstracts


Chemical Abstracts
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Author :
language : en
Publisher:
Release Date :

Chemical Abstracts written by and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on with Chemistry categories.




Electron Microdiffraction


Electron Microdiffraction
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Author : J. M. Zuo
language : en
Publisher:
Release Date : 2014-01-15

Electron Microdiffraction written by J. M. Zuo and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2014-01-15 with categories.