Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction Patterns

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Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction Patterns

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Author : A. J. M. Hubert
language : en
Publisher:
Release Date : 2019

Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction Patterns written by A. J. M. Hubert and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019 with categories.

Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction

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Author : AJM Hubert
language : en
Publisher: University of Warwick
Release Date : 2019-09-25

Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction written by AJM Hubert and has been published by University of Warwick this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019-09-25 with Science categories.

We explore the capability of digital-large angle convergent beam electron diffraction (D-LACBED) data for the structural refinement of single crystals. To achieve this, we use three materials as test cases. We use corundum for atomic position refi nement, copper and gallium arsenide for Debye-Waller factor (DWF) re finement. D-LACBED patterns are found to be extremely sensitive to atomic position, within 0.4 pm of reference X-ray values. The patterns are less sensitive to DWF (using the independent atom model - IAM) but nonetheless give good agreement to X-ray and Mossbauer radiation values for copper. We find the IAM to be insufficient for accurate refinement of gallium arsenide due to the influence of previously suggested strong anharmonicity and bonding within the material. Finally, we use simulation to explore the sensitivity of D-LACBED patterns through most re fineable structural parameters, providing context to the aforementioned results. During the analysis we see that higher g-vector patterns within the D-LACBED data may be more sensitive to structural parameters in general.

Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction Patterns

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Author : Alexander James Morley Hubert
language : en
Publisher:
Release Date : 2019

Structural Refinement Of Single Crystals Using Digital Large Angle Convergent Beam Electron Diffraction Patterns written by Alexander James Morley Hubert and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2019 with Crystals categories.

Cumulated Index Medicus

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Author :
language : en
Publisher:
Release Date : 1989

Cumulated Index Medicus written by and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1989 with Medicine categories.

Transmission Electron Microscopy

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Author : C. Barry Carter
language : en
Publisher: Springer
Release Date : 2016-08-24

Transmission Electron Microscopy written by C. Barry Carter and has been published by Springer this book supported file pdf, txt, epub, kindle and other format this book has been release on 2016-08-24 with Technology & Engineering categories.

This text is a companion volume to Transmission Electron Microscopy: A Textbook for Materials Science by Williams and Carter. The aim is to extend the discussion of certain topics that are either rapidly changing at this time or that would benefit from more detailed discussion than space allowed in the primary text. World-renowned researchers have contributed chapters in their area of expertise, and the editors have carefully prepared these chapters to provide a uniform tone and treatment for this exciting material. The book features an unparalleled collection of color figures showcasing the quality and variety of chemical data that can be obtained from today’s instruments, as well as key pitfalls to avoid. As with the previous TEM text, each chapter contains two sets of questions, one for self assessment and a second more suitable for homework assignments. Throughout the book, the style follows that of Williams & Carter even when the subject matter becomes challenging—the aim is always to make the topic understandable by first-year graduate students and others who are working in the field of Materials Science Topics covered include sources, in-situ experiments, electron diffraction, Digital Micrograph, waves and holography, focal-series reconstruction and direct methods, STEM and tomography, energy-filtered TEM (EFTEM) imaging, and spectrum imaging. The range and depth of material makes this companion volume essential reading for the budding microscopist and a key reference for practicing researchers using these and related techniques.

Chemical Abstracts

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Author :
language : en
Publisher:
Release Date :

Chemical Abstracts written by and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on with Chemistry categories.

Industrial Applications Of Electron Microscopy

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Author : Zhigang Li
language : en
Publisher: CRC Press
Release Date : 2002-12-04

Industrial Applications Of Electron Microscopy written by Zhigang Li and has been published by CRC Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2002-12-04 with Science categories.

Providing proven strategies for solutions to research, development, and production dilemmas, this reference details the instrumentation and underlying principles for utilization of electron microscopy in the manufacturing, automotive, semiconductor, photographic film, pharmaceutical, chemical, mineral, forensic, glass, and pulp and paper industries

Physics Briefs

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Author :
language : en
Publisher:
Release Date : 1992

Physics Briefs written by and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1992 with Physics categories.

Structure Determination By X Ray Crystallography

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Author : M. F. C. Ladd
language : en
Publisher: Springer Science & Business Media
Release Date : 2012-12-06

Structure Determination By X Ray Crystallography written by M. F. C. Ladd and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2012-12-06 with Science categories.

Crystallography may be described as the science of the structure of materi als, using this word in its widest sense, and its ramifications are apparent over a broad front of current scientific endeavor. It is not surprising, therefore, to find that most universities offer some aspects of crystallography in their undergraduate courses in the physical sciences. It is the principal aim of this book to present an introduction to structure determination by X-ray crystal lography that is appropriate mainly to both final-year undergraduate studies in crystallography, chemistry, and chemical physics, and introductory post graduate work in this area of crystallography. We believe that the book will be of interest in other disciplines, such as physics, metallurgy, biochemistry, and geology, where crystallography has an important part to play. In the space of one book, it is not possible either to cover all aspects of crystallography or to treat all the subject matter completely rigorously. In particular, certain mathematical results are assumed in order that their applications may be discussed. At the end of each chapter, a short bibliog raphy is given, which may be used to extend the scope of the treatment given here. In addition, reference is made in the text to specific sources of information. We have chosen not to discuss experimental methods extensively, as we consider that this aspect of crystallography is best learned through practical experience, but an attempt has been made to simulate the interpretive side of experimental crystallography in both examples and exercises.

Ceramic Abstracts

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Author : American Ceramic Society
language : en
Publisher:
Release Date : 1991

Ceramic Abstracts written by American Ceramic Society and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1991 with Ceramic materials categories.