Thermal Methods Of Polymer Analysis

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Thermal Methods Of Polymer Analysis

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Author : T.R Crompton
language : en
Publisher: Smithers Rapra
Release Date : 2013-01-29

Thermal Methods Of Polymer Analysis written by T.R Crompton and has been published by Smithers Rapra this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-01-29 with Science categories.

This book reviews the various thermal methods used for the characterisation of polymer properties and composition. All these methods study the properties of polymers as they change with temperature. The methods discussed in this book are: differential photocalorimetry, differential scanning calorimetry, dielectric thermal analysis, differential thermal analysis, dynamic mechanical analysis, evolved gas analysis, gas chromatography, gas chromatography combined with mass spectrometry, mass spectrometry, microthermal analysis, thermal volatilisation, thermogravimetric analysis and thermomechanical analysis. Each technique is discussed in detail and examples of the use of each technique are also given. Each chapter has an extensive list of references so that the reader can follow up topics of interest. This book will be a useful reference for those who already use any of these thermal methods but will also be of interest to undergraduates and those who are just starting to use these techniques.

Thermal Analysis Of Polymers

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Author : Joseph D. Menczel
language : en
Publisher: John Wiley & Sons
Release Date : 2014-07-09

Thermal Analysis Of Polymers written by Joseph D. Menczel and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2014-07-09 with Science categories.

Presents a solid introduction to thermal analysis, methods, instrumentation, calibration, and application along with the necessary theoretical background. Useful to chemists, physicists, materials scientists, and engineers who are new to thermal analysis techniques, and to existing users of thermal analysis who wish expand their experience to new techniques and applications Topics covered include Differential Scanning Calorimetry and Differential Thermal Analysis (DSC/DTA), Thermogravimetry, Thermomechanical Analysis and Dilatometry, Dynamic Mechanical Analysis, Micro-Thermal Analysis, Hot Stage Microscopy, and Instrumentation. Written by experts in the various areas of thermal analysis Relevant and detailed experiments and examples follow each chapter.

Polymer Characterization By Thermal Methods Of Analysis

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Author : Jen Chiu
language : en
Publisher:
Release Date : 1974

Polymer Characterization By Thermal Methods Of Analysis written by Jen Chiu and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1974 with Detroit, MI categories.

1st published in Journal of Macromolecular Science (Chemistry) V.A8, no.1, 1974.

Principles And Applications Of Thermal Analysis

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Author : Paul Gabbott
language : en
Publisher: John Wiley & Sons
Release Date : 2008-04-30

Principles And Applications Of Thermal Analysis written by Paul Gabbott and has been published by John Wiley & Sons this book supported file pdf, txt, epub, kindle and other format this book has been release on 2008-04-30 with Science categories.

Thermal Analysis techniques are used in a wide range of disciplines, from pharmacy and foods to polymer science, materials and glasses; in fact any field where changes in sample behaviour are observed under controlled heating or controlled cooling conditions. The wide range of measurements possible provide fundamental information on the material properties of the system under test, so thermal analysis has found increasing use both in basic characterisation of materials and in a wide range of applications in research, development and quality control in industry and academia. Principles and Applications of Thermal Analysis is written by manufacturers and experienced users of thermal techniques. It provides the reader with sound practical instruction on how to use the techniques and gives an up to date account of the principle industrial applications. By covering basic thermogravimetric analysis (TGA), differential scanning calorimetry (DSC) including the new approach of Fast Scanning DSC, together with dynamic mechanical analysis (DMA /TMA) methods, then developing the discussion to encompass industrial applications, the book serves as an ideal introduction to the technology for new users. With a strong focus on practical issues and relating the measurements to the physical behaviour of the materials under test, the book will also serve as an important reference for experienced analysts.

Calorimetry And Thermal Analysis Of Polymers

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Author : Vincent B. F. Mathot
language : en
Publisher: Hanser Gardner Publications
Release Date : 1994-01

Calorimetry And Thermal Analysis Of Polymers written by Vincent B. F. Mathot and has been published by Hanser Gardner Publications this book supported file pdf, txt, epub, kindle and other format this book has been release on 1994-01 with Science categories.

Modulated Temperature Differential Scanning Calorimetry

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Author : Mike Reading
language : en
Publisher: Springer Science & Business Media
Release Date : 2006-02-22

Modulated Temperature Differential Scanning Calorimetry written by Mike Reading and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2006-02-22 with Medical categories.

MTDSC provides a step-change increase in the power of calorimetry to characterize virtually all polymer systems including curing systems, blends and semicrystalline polymers. It enables hidden transitions to be revealed, miscibility to be accurately assessed, and phases and interfaces in complex blends to be quantified. It also enables crystallinity in complex systems to be measured and provides new insights into melting behaviour. All of this is achieved by a simple modification of conventional DSC. In 1992 a new calorimetric technique was introduced that superimposed a small modulation on top of the conventional linear temperature program typically used in differential scanning calorimetry. This was combined with a method of data analysis that enabled the sample’s response to the linear component of the temperature program to be separated from its response to the periodic component. In this way, for the first time, a signal equivalent to that of conventional DSC was obtained simultaneously with a measure of the sample’s heat capacity from the modulation. The new information this provided sparked a revolution in scanning calorimetry by enabling new insights to be gained into almost all aspects of polymer characteristics. This book provides both a basic and advanced treatment of the theory of the technique followed by a detailed exposition of its application to reacting systems, blends and semicrystalline polymers by the leaders in all of these fields. It is an essential text for anybody interested in calorimetry or polymer characterization, especially if they have found that conventional DSC cannot help them with their problems.

Thermal Methods Of Analysis

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Author : P.J. Haines
language : en
Publisher: Springer
Release Date : 1995

Thermal Methods Of Analysis written by P.J. Haines and has been published by Springer this book supported file pdf, txt, epub, kindle and other format this book has been release on 1995 with Gardening categories.

This book provides a unique introduction to all the thermal methods of analysis which are currently growing in importance by laying a special emphasis on worked examples and graded problems. Part I covers principles, modern instrumentation and interpretation of results whilst Part II consists entirely of thoroughly worked examples and problems of gradually increasing complexity. Analytical chemists, physical chemists, polymer chemists, bio-analytical chemists, material scientists and physicists at undergraduate level and in industry will find this step-by-step guide an invaluable learning tool and entry to the subject.

Thermal Methods In Polymer Analysis

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Author : Shalaby W. Shalaby
language : en
Publisher: Lawrence Erlbaum Associates
Release Date : 1978

Thermal Methods In Polymer Analysis written by Shalaby W. Shalaby and has been published by Lawrence Erlbaum Associates this book supported file pdf, txt, epub, kindle and other format this book has been release on 1978 with Science categories.

Introduction To Thermal Analysis

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Author : Michael Ewart Brown
language : en
Publisher: Springer Science & Business Media
Release Date : 2001-12-31

Introduction To Thermal Analysis written by Michael Ewart Brown and has been published by Springer Science & Business Media this book supported file pdf, txt, epub, kindle and other format this book has been release on 2001-12-31 with Technology & Engineering categories.

to Thermal Analysis Techniques and Applications Edited by Michael E. Brown Chemistry Department, Rhodes University, Grahamstown, South Africa KLUWER ACADEMIC PUBLISHERS NEW YORK, BOSTON, DORDRECHT, LONDON, MOSCOW eBook ISBN: 0-306-48404-8 Print ISBN: 1-4020-0472-9 ©2004 Kluwer Academic Publishers New York, Boston, Dordrecht, London, Moscow Print ©2001 Kluwer Academic Publishers Dordrecht All rights reserved No part of this eBook may be reproduced or transmitted in any form or by any means, electronic, mechanical, recording, or otherwise, without written consent from the Publisher Created in the United States of America Visit Kluwer Online at: http://kluweronline. com and Kluwer's eBookstore at: http://ebooks. kluweronline. com CONTENTS Preface to the First Edition, Chapman & Hall, London, 1988 ix About the First Edition of this Book x Preface to the Second Edition xi 1. INTRODUCTION 1. 1 Definition and History 1 1. 2 Thermal Analysis Instruments 4 References 11 2. THERMAL EVENTS 2. 1 Introduction 13 2. 2 The Solid State 13 2. 3 Reactions of Solids 14 2. 4 Decomposition of Solids 15 2. 5 Reaction with the Surrounding Atmosphere 16 2. 6 Solid-Solid Interactions 16 References 17 3. THERMOGRAVIMETRY (TG) Introduction 3. 1 19 3. 2 The Balance 19 3. 3 Heating the Sample 21 3. 4 The Atmosphere 24 3. 5 The Sample 26 3. 6 Temperature Measurement 26 3. 7 Temperature Control 28 Sample Controlled Thermal Analysis (SCTA) 29 3. 8 3. 9 Calibration 36 3. 10 Presentation of TG Data 37 3.