X Ray Waveguides For High Resolution X Ray Analysis
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X Ray Waveguides For High Resolution X Ray Analysis
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Author :
language : en
Publisher:
Release Date : 1999
X Ray Waveguides For High Resolution X Ray Analysis written by and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1999 with categories.
The project goals were to model, synthesize, and characterize thin-film, x-ray waveguide structures to determine whether such nanostructurcs can be fabricated with the precision required for true waveguide operation at x-ray energies. In FY98, we designed, fabricated, and characterized (at the Stanford Synchrotron Radiation Laboratory) optimized. thin-film, x-ray waveguide structures (XWGs) as resonant concentrators of x-rays which may be applied as diffraction-limited, linear x-ray sources. We fabricated nine waveguide structures that were optimized to operate in the cavity modes m = 1,2,3 and tested them at x-ray energies of 6 to 10 keV. The observed performances were compared to the calculations based on the design structures and excellent agreement was demonstrated. This project plan is presented in TABLE 1 that includes all aspects of the development of these unique thin film x-ray optical devices. X-ray waveguide designs were made using a standard x-ray multilayer x-ray optic Fresnel code. Materials were selected on the basis of calculated performance as well as sputter deposition characteristics. Laboratory x-ray reflectivity measurements were made prior to the SSRL experimental run to assess the quality of the samples. Cross-section Transmission Electron Microscopy observations of selected sample were made to enable assessment of the relationship between the design structures and the fabricated structures. The cross-section TEM observations correlated well with the waveguide fabrication parameters supporting the observed agreement between the experimental and calculated grazing incidence reflectivities and fluorescence as functions of both x-ray energy and grazing angle of incidence.
X Ray Waveguide Optics
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Author : Sarah Hoffmann-Urlaub
language : en
Publisher: Göttingen University Press
Release Date : 2017
X Ray Waveguide Optics written by Sarah Hoffmann-Urlaub and has been published by Göttingen University Press this book supported file pdf, txt, epub, kindle and other format this book has been release on 2017 with categories.
Modern x-ray sources and analysis techniques such as lens less imaging combined with phase retrieval algorithms allow for resolving structure sizes in the nanometer range. For this purpose optics have to be employed, ensuring small focal spot dimensions simultaneously with high photon densities. Furthermore, the wave front behind the optics is required to be smooth enabling for high resolution imaging. Combining all these properties, x-ray waveguides are well suited to perform this task, since the intensity distribution behind the guide is restricted in two dimensions serving as a secondary quasi point-source without wave-front aberrations, showing also a high divergence, suitable for resolving fine features. Importantly, the radiation provided by the waveguide reveals a high degree of coherence, required by many imaging techniques. The waveguide itself consists of an air-filled channel embedded in a solid matrix; typical materials are silicon, germanium or quartz. While the entrance area is nano-sized, the channel length is in the millimeter-range, this way posing challenges to fabricate high aspect ratio geometries. Since the functioning of x-ray waveguides is based on the total reflection at small incident angles, the surface roughness of the channel walls must be as low as possible to avoid scattering and hence loss of intensity. To fulfill these demanding conditions, a process scheme involving spin-coating, electron beam lithography, wet development, reactive ion etching and wafer bonding is optimized within this work. To gain deeper insights into the principle of wave guiding finite difference simulations are performed, also opening access for advanced design considerations such as gratings, tapered and curved channels, or beamsplitters, enabling for constructing novel x-ray tools as for example time delay devices or interferometers. Waveguides in all geometries are tested at synchrotron sources, accomplishing new benchmarks in x-ray optical performance. Here, the x-ray beam leaving the channel, propagates out to a pixel array detector in the far-field region. From the recorded data the intensity distribution in the near-field directly behind the waveguide is reconstructed, revealing an outstanding agreement with the simulations and electron micrographs. Since the radiation field of the waveguide is well-characterized and also tunable to meet the requirements of both the measurement setup and the sample, they are suited of a broad field of applications in coherent x-ray imaging.
X Ray Waveguide Optics Beyond Straight Channels
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Author : Sarah Hoffmann-Urlaub
language : en
Publisher:
Release Date : 2016
X Ray Waveguide Optics Beyond Straight Channels written by Sarah Hoffmann-Urlaub and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2016 with categories.
Modern x-ray sources and analysis techniques such as lens less imaging combined with phase retrieval algorithms allow for resolving structure sizes in the nanometerrange. For this purpose optics have to be employed, ensuring small focal spot dimensions simultaneously with high photon densities. Furthermore, the wave front behind the optics is required to be smooth enabling for high-resolution imaging. Combining all these properties, x-ray waveguides are well suited to perform this task, since the intensity distribution behind the guide is restricted in two dimensions serving as a secondary ...
Optimization Of Waveguide Optics For Lensless X Ray Imaging
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Author : Sven Philip Krüger
language : en
Publisher: Universitätsverlag Göttingen
Release Date : 2011
Optimization Of Waveguide Optics For Lensless X Ray Imaging written by Sven Philip Krüger and has been published by Universitätsverlag Göttingen this book supported file pdf, txt, epub, kindle and other format this book has been release on 2011 with categories.
Lensless x-ray imaging is a promising method to determine the three-dimensional structure of material science and biological specimens at the nanoscale. The development of this technique is strongly related to the optimization of x-ray optics since the image formation and object reconstruction depend significantly on the properties of the illumination wave-field. Waveguide optics act as quasi-point sources and enable the spatial and coherent filtering of x-ray beams. Up to now, x-ray waveguides were severely limited in transmission and flux, restricting their use to high-contrast test structures with moderate resolution and long accumulation times. To overcome these limitations, a novel waveguide design with an optimized refractive index profile is presented which significantly minimizes the absorption of the modes propagating inside the waveguide. Experimental results along with simulations show that these two-component planar x-ray waveguides provide small beam cross-sections along with a high photon flux at the exit. By a serial arrangement of two waveguide slices an optimized illumination source has been developed for high-resolution microscopy, as demonstrated in proof-of-concept imaging experiments.
A Dedicated Endstation For Waveguide Based X Ray Imaging
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Author : Sebastian Kalbfleisch
language : en
Publisher: Universitätsverlag Göttingen
Release Date : 2013
A Dedicated Endstation For Waveguide Based X Ray Imaging written by Sebastian Kalbfleisch and has been published by Universitätsverlag Göttingen this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013 with categories.
High Resolution X Ray Diffraction And Imaging
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Author : Tilo Baumbach
language : en
Publisher:
Release Date : 2007
High Resolution X Ray Diffraction And Imaging written by Tilo Baumbach and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 2007 with categories.
Nanoscale Photonic Imaging
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Author : Tim Salditt
language : en
Publisher: Springer Nature
Release Date : 2020-06-09
Nanoscale Photonic Imaging written by Tim Salditt and has been published by Springer Nature this book supported file pdf, txt, epub, kindle and other format this book has been release on 2020-06-09 with Science categories.
This open access book, edited and authored by a team of world-leading researchers, provides a broad overview of advanced photonic methods for nanoscale visualization, as well as describing a range of fascinating in-depth studies. Introductory chapters cover the most relevant physics and basic methods that young researchers need to master in order to work effectively in the field of nanoscale photonic imaging, from physical first principles, to instrumentation, to mathematical foundations of imaging and data analysis. Subsequent chapters demonstrate how these cutting edge methods are applied to a variety of systems, including complex fluids and biomolecular systems, for visualizing their structure and dynamics, in space and on timescales extending over many orders of magnitude down to the femtosecond range. Progress in nanoscale photonic imaging in Göttingen has been the sum total of more than a decade of work by a wide range of scientists and mathematicians across disciplines, working together in a vibrant collaboration of a kind rarely matched. This volume presents the highlights of their research achievements and serves as a record of the unique and remarkable constellation of contributors, as well as looking ahead at the future prospects in this field. It will serve not only as a useful reference for experienced researchers but also as a valuable point of entry for newcomers.
X Ray Diffraction Methods
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Author : E. W. Nuffield
language : en
Publisher:
Release Date : 1966
X Ray Diffraction Methods written by E. W. Nuffield and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1966 with Science categories.
1. Introduction 1; 2. The nature and generation of X-rays 29; 3. The diffraction of X-rays 46; 4. Systematically absent X-ray reflections and the determination of space group 87; 5. Polycrystal or powder methods 105; 6. Orientation and projection of morphological crystals 208; 7. The Laue method 226; 8. The reciprocal lattice 239; 9. The Buerger precession method 253; 10. The rotation and oscillation methods 283; 11. The equi-inclination Weissenberg method 302; 12. Single-crystal X-ray diffractometry 343; 13. A general method for orienting a crystal 351; Appendix : 1. The 230 space groups 365; 2. The six permutation of the orthorhombic space groups 370; 3. Space-group determinative tables 372; 4. Table of 1/2 (cos2 phi/sin phi + cos2 phi/phi) 385; 5. Data for constructing stereographic scales 388; 6. Mathematical relations between reciprocal- and direct-lattice constants 391; Index 405.
Handbook Of X Rays
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Author : Emmett Frank Kaelble
language : en
Publisher:
Release Date : 1967
Handbook Of X Rays written by Emmett Frank Kaelble and has been published by this book supported file pdf, txt, epub, kindle and other format this book has been release on 1967 with Science categories.
X Ray Standing Wave Technique The Principles And Applications
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Author : Jorg Zegenhagen
language : en
Publisher: World Scientific
Release Date : 2013-01-30
X Ray Standing Wave Technique The Principles And Applications written by Jorg Zegenhagen and has been published by World Scientific this book supported file pdf, txt, epub, kindle and other format this book has been release on 2013-01-30 with Science categories.
The X-ray standing wave (XSW) technique is an X-ray interferometric method combining diffraction with a multitude of spectroscopic techniques. It is extremely powerful for obtaining information about virtually all properties of surfaces and interfaces on the atomic scale. However, as with any other technique, it has strengths and limitations. The proper use and necessary understanding of this method requires knowledge in quite different fields of physics and technology. This volume presents comprehensively the theoretical background, technical requirements and distinguished experimental highlights of the technique. Containing contributions from the most prominent experts of the technique, such as Andre Authier, Boris Batterman, Michael J Bedzyk, Jene Golovchenko, Victor Kohn, Michail Kovalchuk, Gerhard Materlik and D Phil Woodruff, the book equips scientists with all the necessary information and knowledge to understand and use the XSW technique in practically all applications.